A comprehensive study on the synthesis, characterization and mathematical modeling of nanostructured Co-based catalysts using different support materials for AB hydrolysis

2021 ◽  
Author(s):  
Hilal Çelik Kazıcı ◽  
Mehmet Sait İzgi ◽  
Ömer Şahin
2016 ◽  
Vol 22 (3) ◽  
pp. 434-476 ◽  
Author(s):  
Michael Wolff ◽  
Michael Böhm

The subject of this comprehensive study is the general (mathematical) modeling of sharp (i.e. two-dimensional) interfaces without and with their own thermodynamical activity. We provide essential tools for the modeling of body-interface systems. Important items of the kinematics of singular (moving) interfaces as well as balance equations at interfaces will be addressed. Problems connected with material representation will be discussed. Special interfacial balances for mass, impulse, angular momentum, energy, mass of a tracer and of entropy will be considered including the discussion of special cases. As an illustrative example, a continuous model for a body with loss of material (e.g. due to mechanical treatment) will be developed in the framework presented.


Author(s):  
Manuel Malaver ◽  
Hamed Kasmaei ◽  
Umair Khan ◽  
Aurang Zaib

In the presented paper, a comprehensive study will be done on shape factor analysis of MoS2-GO in H2O-C2H6O2 based hybrid nanoliquids associated with effect and influence of transverse magnetic field and thermal radiation. The effect of variation in different parameters and nanoliquids shapes under temperature and velocity distribution is explored and also non-linear thermal radiation will be analyzed. Algorithms are introduced in proportion to mathematical modeling based on their numerical results and comparative curves for further explanation. In addition, it will be done research for influence and effect of new significant parameters emerged to the model to do sensitivity analysis and also their output results are demonstrated, examined and compared together by presenting graphs and tables. Based on detailed discussions, authentication of attained results designates the high accuracy of applied methods deployed to solve presented model in the paper. Our results satisfy that our used approach is accurate, highly reliable and also effective. All mentioned steps will be described throughout the literature.


2014 ◽  
Vol 15 (4) ◽  
pp. 313-326 ◽  
Author(s):  
Anup Anurag ◽  
Satarupa Bal ◽  
Suman Sourav

Abstract This paper provides a detailed and comprehensive study of various models of photovoltaic (PV) array which have been formulated previously in the literature, using the datasheet parameters. In this paper, comparisons of the models have been made on basis of the MPP tracking, the root mean square deviation (RMSD) from the experimental data, the Fill Factor (FF), the efficiency of the model and the time required for simulation. Further, the resemblance with the actual P–V and I–V curves, as obtained on the basis of experimental data, has also been included in this analysis. On the basis of all these, the best model that can be used for simulation purposes, keeping in mind the necessary factors for a particular application, can be selected. It is envisaged that the work can be very useful for professionals who require simple and accurate PV simulators for their design. This paper is also intended to be a useful tool for the beginners who require a clear and logical insight regarding the working and modeling of PV cells. All the systems here are modeled and simulated in MATLAB/Simulink environment.


Author(s):  
F. A. Heckman ◽  
E. Redman ◽  
J.E. Connolly

In our initial publication on this subject1) we reported results demonstrating that contrast is the most important factor in producing the high image quality required for reliable image analysis. We also listed the factors which enhance contrast in order of the experimentally determined magnitude of their effect. The two most powerful factors affecting image contrast attainable with sheet film are beam intensity and KV. At that time we had only qualitative evidence for the ranking of enhancing factors. Later we carried out the densitometric measurements which led to the results outlined below.Meaningful evaluations of the cause-effect relationships among the considerable number of variables in preparing EM negatives depend on doing things in a systematic way, varying only one parameter at a time. Unless otherwise noted, we adhered to the following procedure evolved during our comprehensive study:Philips EM-300; 30μ objective aperature; magnification 7000- 12000X, exposure time 1 second, anti-contamination device operating.


Author(s):  
A. Singh ◽  
A. Dykeman ◽  
J. Jarrelf ◽  
D. C. Villeneuve

Hexachlorobenzene (HCB), a persistent and mobile organochlorine pesticide, occurs in environment. HCB has been shown to be present in human follicular fluid. An objective of the present report, which is part of a comprehensive study on reproductive toxicity of HCB, was to determine the cytologic effects of the compound on ovarian follicles in a primate model.Materials and Methods. Eight Cynomolgus monkeys were housed under controlled conditions at Animal facility of Health and Welfare, Ottawa. Animals were orally administered gelatin capsules containing HCB mixed with glucose in daily dosages of 0.0 or 10 mg/kg b.w. for 90 days; the former was the control group. On the menstrual period following completion of dosing, the monkeys underwent an induction cycle of superovulation. At necropsy, one-half of an ovary from each animal was diced into ca. 2- to 3-mm cubed specimens that were fixed by immersion in 2.5% glutaraldehyde in 0.1 M cacodylate buffer (pH 7.3). Subsequent procedures followed to obtain thin sections that were examined in a Hitachi H-7000 electron microscope have been described earlier.


Author(s):  
D. L. Rohr ◽  
S. S. Hecker

As part of a comprehensive study of microstructural and mechanical response of metals to uniaxial and biaxial deformations, the development of substructure in 1100 A1 has been studied over a range of plastic strain for two stress states.Specimens of 1100 aluminum annealed at 350 C were tested in uniaxial (UT) and balanced biaxial tension (BBT) at room temperature to different strain levels. The biaxial specimens were produced by the in-plane punch stretching technique. Areas of known strain levels were prepared for TEM by lapping followed by jet electropolishing. All specimens were examined in a JEOL 200B run at 150 and 200 kV within 24 to 36 hours after testing.The development of the substructure with deformation is shown in Fig. 1 for both stress states. Initial deformation produces dislocation tangles, which form cell walls by 10% uniaxial deformation, and start to recover to form subgrains by 25%. The results of several hundred measurements of cell/subgrain sizes by a linear intercept technique are presented in Table I.


Author(s):  
F.E. Hossler ◽  
M.I. McKamey ◽  
F.C. Monson

A comprehensive study of the microvasculature of the normal rabbit bladder, revealed unusual "capillary glomeruli" along the lateral walls. Here they are characterized as hemal lymph nodes using light microscopy, SEM, TEM, ink injection, and vascular casting.Bladders were perfused via a cannula placed in the abdominal aorta with either 2% glutaraldehyde in 0.1M cacodylate buffer (pH 7.4) for fixation, 10% India ink in 0.9% saline and 0.1M phosphate (pH 7.4) for vessel tracing, or resin (Mercoximethylmethacrylate: catalyst, 4:1:0.3; Ladd Research Industries) for vascular corrosion casting. Infusion pressure was 100mm Hg. Fixed tissue was sectioned from epon-araldyte resin, and stained with toluidine blue for light microscopy, and lead and uranium for TEM. Ink injected tissue was photographed directly from saline-filled bladders illuminated from below. Resin-filled tissue was macerated in 5% KOH and distilled water. Casts were critical point dried, sputter coated with goldpalladium, and examined by routine SEM at 10 KV.


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