scholarly journals Effect of surface roughness on the angular acceleration for a droplet on a super-hydrophobic surface

Friction ◽  
2020 ◽  
Author(s):  
Longyang Li ◽  
Jingfang Zhu ◽  
Zhixiang Zeng ◽  
Eryong Liu ◽  
Qunji Xue
Keyword(s):  
Contact Angle ◽  
High Speed ◽  
Adhesion Force ◽  
Angular Acceleration ◽  
Hydrophobic Surface ◽  
Adhesive Force ◽  
Industrial Applications ◽  
Contact Angles ◽  
Etching Time ◽  
Receding Contact

Abstract The motion of droplets on a super-hydrophobic surface, whether by sliding or rolling, is a hot research topic. It affects the performance of super-hydrophobic materials in many industrial applications. In this study, a super-hydrophobic surface with a varied roughness is prepared by chemical-etching. The adhesive force of the advancing and receding contact angles for a droplet on a super-hydrophobic surface is characterized. The adhesive force increases with a decreased contact angle, and the minimum value is 0.0169 mN when the contact angle is 151.47°. At the same time, the motion of a droplet on the super-hydrophobic surface is investigated by using a high-speed camera and fluid software. The results show that the droplet rolls instead of sliding and the angular acceleration increases with an increased contact angle. The maximum value of the angular acceleration is 1,203.19 rad/s2 and this occurs when the contact angle is 151.47°. The relationship between the etching time, roughness, angular acceleration, and the adhesion force of the forward and backward contact angle are discussed.

Degradation of Hydrophobic Surface Coatings Under Water Exposure

2018 ◽  
Author(s):  
Matthew A. Trapuzzano ◽  
Rasim Guldiken ◽  
Andrés Tejada-Martínez ◽  
Nathan B. Crane
Keyword(s):  
Contact Angle ◽  
Material Selection ◽  
Contact Angle Hysteresis ◽  
Hydrophobic Surface ◽  
Contact Angles ◽  
Water Exposure ◽  
Angle Measurements ◽  
Degradation Rates ◽  
Contact Angle Measurements ◽  
Receding Contact

Many important processes depend on the wetting of liquids on surfaces. Wetting is commonly controlled through material selection, coatings, and/or surface texture, however these means are sensitive to environmental conditions. Some “hydrophobic” fluoropolymer coatings are sensitive to extended water exposure as evidenced by declining contact angles and increasing contact angle hysteresis. Understanding degradation of these coatings is critical to processes that employ them. To accomplish this, contact angle measurements were taken before, during, and after slides coated with FluoroSyl 3750 or Cytop were submerged in water, or vibrated while covered in water. Both methods demonstrated similar changes in advancing contact angle though vibration increased degradation rates significantly. However, it does not simply accelerate the process as different trends are apparent in receding contact angles. The FluoroSyl 3750 showed no clear degradation under either condition. Surface profilometry did not detect any surface morphology differences that might cause contact angle change.

Wetting and Capillarity Effects On Bubble Formation From Orifice Plates Submerged in Pools of Water

2021 ◽  
Author(s):  
Sanjivan Manoharan ◽  
Raj M. Manglik ◽  
Milind A. Jog
Keyword(s):  
Contact Angle ◽  
Bubble Growth ◽  
High Speed ◽  
Bubble Formation ◽  
Minimum Energy ◽  
Hydrophobic Surface ◽  
Contact Angles ◽  
Orifice Diameter ◽  
Capillary Length ◽  
Critical Contact

Abstract An experimental study of bubble growth from submerged orifice plates in pools of water is carried out to scale and correlate the effects of surface wettability and orifice diameter D0 on ebullience. Measurements of bubble growth on surfaces with nine different contact angles (38° ≤ θ ≤ 128°) with varying air flow rates (1 to 300 ml/min) were made using high speed videography and image processing. In the static or constant-volume regime, below a critical contact angle θc, the bubble base remains attached to the orifice and the equivalent departure diameter Db is independent of contact angle θ. On the other hand, above the critical contact angle, the bubble base spreads on the surface resulting in larger Db. For θ > θc, Db is strongly dependent on θ and increases with it. Using minimum energy method, it is shown that the wettability effects can be scaled and correlated by a modified capillary length, defined as a function of the Laplace length and contact angle. The proposed correlation provides predictions of Db that agree with experimental data of this study as well as those available in the literature to within ±15 %. Moreover, for a hydrophobic surface when D0 > twice the modified capillary length, the bubble grows inside the orifice; for a hydrophilic surface this scales with twice the capillary length and effect of θ is not seen.

The Effects of Asymmetric Micro Ratchets on Dynamic Contact Angle and Pool Boiling Performance

2012 ◽  
Author(s):  
Lance Austin Brumfield ◽  
Sunggook Park
Keyword(s):  
Contact Angle ◽  
High Speed ◽  
Pool Boiling ◽  
Dynamic Contact Angle ◽  
Dynamic Contact ◽  
Contact Angles ◽  
Equilibrium Contact Angle ◽  
Droplet Impingement ◽  
Receding Contact ◽  
Receding Contact Angle

The dynamic advancing and receding contact angles of 5μl water droplets were experimentally measured via the droplet impingement technique on a polished brass surface, one brass symmetric micro ratchet, and five brass asymmetric micro ratchet samples of varying dimensions. Droplets were released from varying heights (Weber number) and the impacts studied via high speed camera. Equilibrium advancing and receding contact angles were measured by placing a water droplet on the surfaces and tilting it. Contact angle values were then compared to an existing pool boiling model which incorporates the dynamic receding contact angle, surface roughness ratio, and equilibrium contact angle.

The Surface Modification with Fluorocarbon Thin Films for the Prevention of Stiction in Mems

1998 ◽  
Vol 518 ◽  
Author(s):  
Sang-Ho Lee ◽  
Myong-Jong Kwon ◽  
Jin-Goo Park ◽  
Yong-Kweon Kim ◽  
Hyung-Jae Shin
Keyword(s):  
Contact Angle ◽  
Contact Angle Hysteresis ◽  
Contact Angles ◽  
Fluorocarbon Films ◽  
Perfluorodecanoic Acid ◽  
Large Hysteresis ◽  
Static Contact ◽  
Receding Contact ◽  
Highly Hydrophobic ◽  
Receding Contact Angle

AbstractHighly hydrophobic fluorocarbon films were prepared by the vapor phase (VP) deposition method in a vacuum chamber using both liquid (3M's FC40, FC722) and solid sources (perfluorodecanoic acid (CF3(CF2)8COOH), perfluorododecane (C12F26)) on Al, Si and oxide coated wafers. The highest static contact angles of water were measured on films deposited on aluminum substrate. But relatively lower contact angles were obtained on the films on Si and oxide wafers. The advancing and receding contact angle analysis using a captive drop method showed a large contact angle hysteresis (ΔH) on the VP deposited fluorocarbon films. AFM study showed poor film coverage on the surface with large hysteresis. FTIR-ATR analysis positively revealed the stretching band of CF2 groups on the VP deposited substrates. The thermal stability of films was measured at 150°C in air and nitrogen atmospheres as a function of time. The rapid decrease of contact angles was observed on VP deposited FC and PFDA films in air. However, no decrease of contact angle on them was observed in N2.

Surface Topography Induced Ultrahydrophobic Behavior: Effect of Three-Phase Contact Line Topology

2006 ◽  
Author(s):  
Neeharika Anantharaju ◽  
Mahesh Panchagnula ◽  
Wayne Kimsey ◽  
Sudhakar Neti ◽  
Svetlana Tatic-Lucic
Keyword(s):  
Contact Angle ◽  
Contact Line ◽  
Anomalous Behavior ◽  
Contact Angles ◽  
Wet Etching ◽  
Surface Geometry ◽  
Wetting Behavior ◽  
Void Fractions ◽  
Three Phase ◽  
Receding Contact

The wettability of silicon surface hydrophobized using silanization reagents was studied. The advancing and receding contact angles were measured with the captive needle approach. In this approach, a drop under study was held on the hydrophobized surface with a fine needle immersed in it. The asymptotic advancing and receding angles were obtained by incrementally increasing the volume added and removed, respectively, until no change in angles was observed. The values were compared with the previously published results. Further, the wetting behavior of water droplets on periodically structured hydrophobic surfaces was investigated. The surfaces were prepared with the wet etching process and contain posts and holes of different sizes and void fractions. The surface geometry brought up a scope to study the Wenzel (filling of surface grooves) and Cassie (non filling of the surface grooves) theories and effects of surface geometry and roughness on the contact angle. Experimental data point to an anomalous behavior where the data does not obey either Wenzel or Cassie type phenomenology. This behavior is explained by an understanding of the contact line topography. The effect of contact line topography on the contact angle was thus parametrically studied. It was also inferred that, the contact angle increased with the increase in void fraction. The observations may serve as guidelines in designing surfaces with the desired wetting behavior.

An Easy Approach for Obtaining Superhydrophobic Surfaces and their Applications

2019 ◽  
Vol 813 ◽  
pp. 37-42
Author(s):  
Amani Khaskhoussi ◽  
Luigi Calabrese ◽  
Edoardo Proverbio
Keyword(s):  
Surface Morphology ◽  
Large Scale ◽  
Adhesion Force ◽  
Industrial Applications ◽  
Contact Angles ◽  
Boiling Water ◽  
Superhydrophobic Surfaces ◽  
Acid Mixture ◽  
Short Term Treatment ◽  
Water Contact

Three different methods were used to obtain nature-inspired superhydrophobic surfaces on aluminum alloys: short-term treatment with boiling water, HF/HCl and HNO3/HCl concentrated solution etching. Afterwards a thin octadecylsilane film was deposited on all pre-treated surfaces. The surface morphology analysis showed that each method allow to obtain a specific dual nano/micro-structure. The corresponding water contact angles ranged from 160° to nearly 180°. The adhesion force between the water droplets and superhydrophobic surfaces were evaluated. The specimen etched with HF/HCl acid mixture solution showed the lowest adhesion. However, the boiling water treatment sample was characterized by the highest adhesion. Furthermore, the relationship between hydrophobic behavior and surface morphology was discussed compressively. In addition, the electrochemical measurements show that the different superhydrophobic surfaces have an excellent anti-corrosion performance evidencing promising results suitable to obtain large-scale nature-inspired superhydrophobic surfaces for several industrial applications.

The Effect of Surface Wettability on Viscous Film Deposition

2009 ◽  
Author(s):  
Alexandru Herescu ◽  
Jeffrey S. Allen
Keyword(s):  
Contact Angle ◽  
Film Thickness ◽  
Capillary Number ◽  
High Speed ◽  
Glass Tube ◽  
Contact Angles ◽  
Film Deposition ◽  
Surface Wettability ◽  
Working Fluid ◽  
Uniqueness Of The Solution

The viscous deposition of a liquid film on the inside of a capillary has been experimentally investigated with a focus on the relationship between the film thickness and surface wettability. With distilled water as a working fluid tests were run in a 622 microns diameter glass tube with contact angles of 30° and 105°, respectively. In the first set of experiments the tube was uncoated while in the second set a fluoropolymer coating was applied to increase the contact angle. A film thickness dependence with the contact angle θ (surface wettability) as well as the Capillary number in the form hR ∼ Ca2/3/cosθ is inferred from scaling arguments. For partial wetting it may explain the existence of a thicker film for nonzero contact angle. It was further found that the non-wetting case of 105° contact angle deviates significantly from the existing theories, the film thickness presenting a weak dependence with the Capillary number. This deviation as well as the apparent non-uniqueness of the solution is thought to be caused by the film instability (rupture) observed during the tests. The thickness of the deposited film as a function of the Capillary number was estimated from the liquid mass exiting the capillary and the gas-liquid interface (meniscus) velocity, and compared to Bretherton’s data and a correlation proposed by Quere. The film thickness measurements as well as the meniscus velocity were determined with the aid of a Photron high speed camera with 10000 frames per second sampling capability coupled with a Nikon TE-2000 inverted microscope and a Precisa electronic balance.

scholarly journals The adhesion model considering capillarity for gecko attachment system

2007 ◽  
Vol 5 (20) ◽  
pp. 319-327 ◽  
Author(s):  
Tae Wan Kim ◽  
Bharat Bhushan
Keyword(s):  
Capillary Force ◽  
Adhesion Force ◽  
Adhesive Force ◽  
Contact Angles ◽  
Adhesion Forces ◽  
Real Area Of Contact ◽  
Wide Range ◽  
Elliptical Integral ◽  
Gecko Adhesion ◽  
Surface Construction

Geckos make use of approximately a million microscale hairs (setae) that branch off into hundreds of nanoscale spatulae to cling to different smooth and rough surfaces and detach at will. This hierarchical surface construction gives the gecko the adaptability to create a large real area of contact with surfaces. It is known that van der Waals force is the primary mechanism used to adhere to surfaces, and capillary force is a secondary effect that can further increase adhesive force. To investigate the effects of capillarity on gecko adhesion, we considered the capillary force as well as the solid-to-solid interaction. The capillary force expressed in terms of elliptical integral is calculated by numerical method to cope with surfaces with a wide range of contact angles. The adhesion forces exerted by a single gecko spatula in contact with planes with different contact angles for various relative humidities are calculated, and the contributions of capillary force to total adhesion force are evaluated. The simulation results are compared with experimental data. Finally, using the three-level hierarchical model recently developed to simulate a gecko seta contacting with random rough surface, the effect of the relative humidity and the hydrophobicity of surface on the gecko adhesion is investigated.

Dynamics of Contact Angle During Growth and Liftoff of Bubbles at a Single Nucleation Site in Flow Boiling

2004 ◽  
Author(s):  
Wangcun Jia ◽  
Vijay K. Dhir
Keyword(s):  
Contact Angle ◽  
High Speed ◽  
Flow Boiling ◽  
Nucleation Site ◽  
Contact Angles ◽  
Working Fluid ◽  
Wafer Surface ◽  
Photographic Images ◽  
Flow Boiling Heat Transfer ◽  
Processing Program

Contact angle is a critical parameter needed in the mechanistic models for the prediction of flow boiling heat transfer. In this paper, variations of upstream and downstream contact angles for a single vapor bubble in flow boiling on horizontal and vertical surfaces were investigated experimentally. The nucleation site is a well-characterized cavity, which was etched on a highly polished silicon wafer surface using micro-fabrication techniques. Water at one atmosphere pressure was used as the working fluid. Photographic images of the bubble were recorded during its inception, growth and liftoff by using high-speed video system and analyzed by an image-processing program. The results provide clean data on the dependence of upstream and downstream contact angles on surface orientation and flow velocity.

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