Microstructural analysis and characterization of lime mortar of seventeenth century Raigad hill fort from western India

Author(s):  
M. R. Singh ◽  
Rajendra Yadav
Author(s):  
R.T. Blackham ◽  
J.J. Haugh ◽  
C.W. Hughes ◽  
M.G. Burke

Essential to the characterization of materials using analytical electron microscopy (AEM) techniques is the specimen itself. Without suitable samples, detailed microstructural analysis is not possible. Ultramicrotomy, or diamond knife sectioning, is a well-known mechanical specimen preparation technique which has been gaining attention in the materials science area. Malis and co-workers and Glanvill have demonstrated the usefulness and applicability of this technique to the study of a wide variety of materials including Al alloys, composites, and semiconductors. Ultramicrotomed specimens have uniform thickness with relatively large electron-transparent areas which are suitable for AEM anaysis.Interface Analysis in Type 316 Austenitic Stainless Steel: STEM-EDS microanalysis of grain boundaries in austenitic stainless steels provides important information concerning the development of Cr-depleted zones which accompany M23C6 precipitation, and documentation of radiation induced segregation (RIS). Conventional methods of TEM sample preparation are suitable for the evaluation of thermally induced segregation, but neutron irradiated samples present a variety of problems in both the preparation and in the AEM analysis, in addition to the handling hazard.


Materials ◽  
2021 ◽  
Vol 14 (11) ◽  
pp. 2911
Author(s):  
Margarida Gonçalves ◽  
Inês Silveirinha Vilarinho ◽  
Marinélia Capela ◽  
Ana Caetano ◽  
Rui Miguel Novais ◽  
...  

Ordinary Portland Cement is the most widely used binder in the construction sector; however, a very high carbon footprint is associated with its production process. Consequently, more sustainable alternative construction materials are being investigated, namely, one-part alkali activated materials (AAMs). In this work, waste-based one-part AAMs binders were developed using only a blast furnace slag, as the solid precursor, and sodium metasilicate, as the solid activator. For the first time, mortars in which the commercial sand was replaced by two exhausted sands from biomass boilers (CA and CT) were developed. Firstly, the characterization of the slag and sands (aggregates) was performed. After, the AAMs fresh and hardened state properties were evaluated, being the characterization complemented by FTIR and microstructural analysis. The binder and the mortars prepared with commercial sand presented high compressive strength values after 28 days of curing-56 MPa and 79 MPa, respectively. The mortars developed with exhausted sands exhibit outstanding compressive strength values, 86 and 70 MPa for CT and CA, respectively, and the other material’s properties were not affected. Consequently, this work proved that high compressive strength waste-based one-part AAMs mortars can be produced and that it is feasible to use another waste as aggregate in the mortar’s formulations: the exhausted sands from biomass boilers.


2016 ◽  
Vol 97 (3) ◽  
pp. 694-705 ◽  
Author(s):  
Rongala Laxmivandana ◽  
Sarah S. Cherian ◽  
Prasanna Yergolkar ◽  
Shobha D. Chitambar

Author(s):  
Roger Ariew

Aristotelians in the seventeenth century comprised a group of mostly anonymous textbook writers whose chief claim to fame is that their philosophy was opposed by such early moderns as Descartes and Galileo. In line with the characterization of them by their opponents, their philosophy has generally been depicted as conservative, monolithic and moribund. However, it is difficult to ratify such judgments. As Aristotelians, these philosophers do not seem particularly conservative; they appear to have assimilated many of the scientific developments of the seventeenth century, and the diversity and range of their views is quite broad. Some of the doctrines peculiar to them, or their particular developments of older views, can be seen as the background against which modern philosophy developed.


2017 ◽  
Vol 7 (1.1) ◽  
pp. 78
Author(s):  
C. Thiruvasagam ◽  
S. Prabagaran ◽  
P. Suresh

The research paper involves fiber composites form a special category materials that are contributing to present swaping of manufactured  hybrid  which finds traditional and non traditional applications. The study explains which are accentuates and optimizing for the recently recognized snake grass standard materials. In this article, the prospecting performance characterization of SG fiber is selected and contrasted as per the ASTM standard. This study additionally manages the examination apply different phenomena of this stages in Jute and snake as fortifications utilized index ended a try. Experiments have been conducted on normal Filaments, snake grass, Glass Fiber and Jute to analyse their Mechanical properties. The common strands are orchestrated in the flat and vertical heading as transferred quality on all sides. Microstructural analysis of these hybrid composite is observed using Scanning  Electron Microscope that reveals bonding and Filament breaksge, Voids and Fiber decover which are further investigated.


2013 ◽  
Vol 594-595 ◽  
pp. 29-33
Author(s):  
Rohaya Abdul Malek ◽  
Yeoh Chieh Hang

A Co-Cr-Mo (ASTM CoF-75) alloy is normally used because of their good in physical, mechanical, wear and as well as biocompatibility. In order to obtain similarity chemical structure of bone, addition of HAP or TCP into CoF-75 alloy is required. The samples were fabricated using powder metallurgy (P/M) technique under pressure of 350 MPa and sintered at 1200 °C under argon atmosphere. The results on the effect of different additives were studied in terms of shrinkage, bulk density, apparent porosity and microstructural analysis.


2014 ◽  
Vol 1618 ◽  
pp. 153-160
Author(s):  
Leticia Jiménez ◽  
Diana E. Arano ◽  
José L. Ruvalcaba ◽  
Fanny Unikel

ABSTRACTThe altarpiece dedicated to San Antonio de Padua was made of wood assembled and self-supporting structure attached to the wall. It is a straight plant altarpiece designed to withstand sculptures. This master piece belongs to the a set of Baroque altarpieces preserved in the state of Campeche and is located in San Roque Church in the City of San Francisco de Campeche, Mexico. This altarpiece was decorated following the traditional technique of the seventeenth century in Mexico, a technique derived from Spain. According to literature sources we know that the strata are the wood, the imprimatura, the pictorial strata and metal sheets that make the golden color and corladuras. The characterization of the constituent materials was of great importance for the interpretation of the constructions system and manufacture of the decoration. The present study shows the results of analysis techniques such as optical microscopy, Particle Induce X Ray Emission (PIXE), and X Ray Florescence Spectroscopy (XRF) and interpretation of the different layers constituting the altarpiece of San Antonio.


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