Characterization of iron oxide-based pigments by synchrotron-based micro X-ray diffraction

2008 ◽  
Vol 42 (1-2) ◽  
pp. 57-62 ◽  
Author(s):  
L.K. Herrera ◽  
M. Cotte ◽  
M.C. Jimenez de Haro ◽  
A. Duran ◽  
A. Justo ◽  
...  
Keyword(s):  
Iron Oxide ◽  
X Ray Diffraction ◽  
X Ray

scholarly journals Production and characterization of iron-chromium-zinc pigment based ceramic stain colour of red-brown shade

2013 ◽  
Vol 48 (3) ◽  
pp. 213-216 ◽  
Author(s):  
S Parveen ◽  
SA Jahan ◽  
S Ahmed
Keyword(s):  
Zinc Oxide ◽  
Iron Oxide ◽  
Chemical Durability ◽  
X Ray Diffraction ◽  
X Ray ◽  
Exposure Limit ◽  
Substitute Material ◽  
Pure Chromium ◽  
Iron Chromium

Considering the demand of ceramic stain colours in Bangladesh, an attempt has been taken to develop iron-chromium-zinc pigment based ceramic stain colour of red-brown shade which could be used as an import substitute material in the local ceramic industries. The desired shade of red-brown stain was synthesized from an equimolar mixture of pure chromium oxide (Cr2O3), iron oxide (Fe2O3) and zinc oxide (ZnO). The developed stain was characterized by X-ray diffraction (XRD) technique. The characteristic of the stain complied with the chemical durability. Moreover, chromium leaching was below the permissible exposure limit which makes it as a promising ceramic stain to be used in our ceramic industries. DOI: http://dx.doi.org/10.3329/bjsir.v48i3.17334 Bangladesh J. Sci. Ind. Res. 48(3), 213-216, 2013

scholarly journals Phosphate adsorption onto bagasse iron oxide biochar: Parameter optimization, kinetic analysis, and study of mechanism

BioResources ◽  
2021 ◽  
Vol 16 (1) ◽  
pp. 1335-1357
Author(s):  
Qing Zhang ◽  
Yan-mei Ding ◽  
Lin Lu ◽  
Jing-xi Li ◽  
Mei-na Liang ◽  
...  
Keyword(s):  
Iron Oxide ◽  
Photoelectron Spectroscopy ◽  
Phosphate Adsorption ◽  
Phosphorus Concentration ◽  
X Ray Diffraction ◽  
Phosphorus Adsorption ◽  
X Ray ◽  
Bet Specific Surface Area ◽  
Ph Range

This study combined chemical ultrasonic modifications and microwave oven heating to prepare a novel adsorbent, bagasse iron oxide biochar, (BIBC) to remove phosphate from aqueous solutions. The characterization of BIBC was made by energy dispersive spectrometry (EDS), Brunauer–Emmett–Teller (BET), Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), and X-ray photoelectron spectroscopy (XPS) analyses, and the mechanism of phosphorus adsorption on BIBC was researched by adsorption batch experiments with emphasis on pH, dosages of BIBC, initial phosphorus concentration, and adsorption time. The BIBC’s BET specific surface area and pore volumes were 81.94 m2 g−1 and 26.74 cm3 g−1, respectively. The pH for the optimal phosphorus adsorption by BIBC ranged from 5.0 to 7.0. The maximum adsorption capacities of phosphorus (according to the Langmuir model) were 3.62, 4.06, and 4.32 mg g-1 at temperatures of 25, 35, and 45 °C, respectively. Electrostatic interaction, surface adsorption of phosphorus on BIBC, and ion exchange were the main mechanisms of phosphorus adsorption. According to XPS results, Fe2p was involved in the adsorption reaction. The adsorption of phosphorus by BIBC is considered to be mainly chemical adsorption. The BIBC was stable under a pH range from 4.0 to 10.0 and secondary pollution did not result.

Characterization of iron oxide nanoparticles from the leaf extract of piper betle by green synthesis method

2020 ◽  
Vol 3 (1) ◽  
Author(s):  
Gowri Manohari N ◽  
Mohanapriya N
Keyword(s):  
Iron Oxide ◽  
Leaf Extract ◽  
Synthesis Method ◽  
Nano Particles ◽  
Piper Betle ◽  
X Ray Diffraction ◽  
Green Method ◽  
X Ray ◽  
Uv Visible

In this present study, Iron Oxide nano particles were synthesized by using Green method. For this synthesis on Iron oxide, the leaf extract of piper betle was used as a reducing agent and FeCl3 as a precursor. Thus, they were characterized by XRD, SEM,EDX and FTIR. The parity of Fe2O3 nano particles was confirmed by EDX. The crystalline size of Iron Oxide nano particles was analyzed using X-ray Diffraction (XRD) spectrum. The functional groups are identified in Fourier Transform Infrared Spectroscopy (FTIR). The surface morphology of the Iron Oxide Nano particles is found from Scanning Electron Microscopy (SEM). The optical properties are determined by using UV-Visible Spectroscopy. Thus, the so-formed nano particles were Fe2O3.

Synthesis and Characterization of Super Paramagnetic Iron Oxide Nanoparticles

2020 ◽  
Vol 10 (2) ◽  
pp. 123-126
Author(s):  
Debasish Aich ◽  
Pijus Kanti Samanta ◽  
Satyajit Saha ◽  
Tapanendu Kamilya
Keyword(s):  
Iron Oxide ◽  
Room Temperature ◽  
Synthesis And Characterization ◽  
Oxide Nanoparticles ◽  
Fe2o3 Nanoparticles ◽  
X Ray Diffraction ◽  
X Ray ◽  
Paramagnetic Behavior ◽  
Diffraction Peaks

Background: Iron oxide (γ-Fe2O3) nanoparticles have been prepared by a simplified coprecipitation method. Methods: X-ray diffraction peaks of the prepared nanoparticles match well with the characteristic peaks of crystalline g-Fe2O3 as per JCPDS data (JCPDS Card No. 39-1346) and absorption peak at 369 nm along with band gap 2.10 eV suggesting the formation of (γ-Fe2O3) nanoparticles. Results: The γ-Fe2O3 nanoparticles are spherical in nature with a diameter around ~10 nm. Conclusion: The crystalline g-Fe2O3 nanoparticles exhibit excellent super-paramagnetic behavior not only at room temperature (300K) but also at a temperature as low as 100K.

scholarly journals Synthesis of Iron Oxide Nanoparticles Using Isobutanol

2016 ◽  
Vol 2016 ◽  
pp. 1-9 ◽  
Author(s):  
Diana Kostyukova ◽  
Yong Hee Chung
Keyword(s):  
Iron Oxide ◽  
Iron Oxide Nanoparticles ◽  
Ammonium Hydroxide ◽  
Oxide Nanoparticles ◽  
X Ray Diffraction ◽  
Ferrous Chloride ◽  
X Ray ◽  
Superparamagnetic Properties

Iron oxide nanoparticles were synthesized by precipitation in isobutanol with sodium hydroxide and ammonium hydroxide. The isobutanol played a role of a surfactant in the synthesis. The nanoparticles were calcined for 100 min to 5 hours in the range of 300 to 600°C. The characterization of the samples by FTIR (Fourier-transform infrared) and XRD (X-ray diffraction) confirmed the formation ofγ-Fe2O3(maghemite) from Fe3O4(magnetite) at calcination at 300°C. The morphology and particle size were studied by SEM (scanning electron microscope). Nanoparticles in the range of 11–22 nm prepared at 0.09 M of ferrous chloride exhibited superparamagnetic properties. Nanoparticles synthesized with ferrous chloride and ammonium hydroxide at 75°C and calcined at 530°C for 2 h wereα-Fe2O3(hematite).

Characterization of Fe2O3 Nanowires and its Solar Cell Applications

2018 ◽  
Vol 766 ◽  
pp. 217-222
Author(s):  
Suphaporn Daothong
Keyword(s):  
Solar Cell ◽  
Iron Oxide ◽  
Oxidation Process ◽  
X Ray Diffraction ◽  
Sem Images ◽  
Xrd Pattern ◽  
Oxide Nanowires ◽  
X Ray ◽  
Dye Sensitized

Iron oxide nanowires were synthesized on stainless steel mesh substrate using the thermal oxidation process at the varying temperature of 750°C for 60 min. The samples were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The XRD pattern showed that the iron oxide nanowires exhibited the structure of alpha-Fe2O3 (hematite). SEM images indicated that the diameter and the length of the nanowires were 80 to 285 nm and more than 5 μm, respectively. The dye-sensitized solar cell (DSC) properties based on the nanowires substrate was also studied. It was found that the power conversion efficiency (η) of the device was 0.11%.

Preparation and Characterization of Iron-Oxide-Coated-Zeolite Adsorbent

2014 ◽  
Vol 941-944 ◽  
pp. 216-220
Author(s):  
Li Zhu ◽  
Yan Qin Lu ◽  
Zhao Ju He
Keyword(s):  
Iron Oxide ◽  
Phosphorus Removal ◽  
Removal Rate ◽  
Adsorption Properties ◽  
Ferric Nitrate ◽  
X Ray Diffraction ◽  
X Ray ◽  
Infrared Spectrometer ◽  
Zeolite Adsorbent

In this paper, Iron-Oxide-Coated-Zeolite has been prepared by using natural zeolite and ferric nitrate. The morphology and structure of the adsorbent were Characterized by Scanning electron microscopy (SEM), powder X-ray diffraction (XRD), and Fourier transform infrared spectrometer (FTIR). The results show that the adsorption properties of zeolite were improved by modified with ferric nitrate. The phosphorus removal rate on IOCZ50was above 80%.

Characterization of iron oxide compounds in soils by Mössbauer and other methods

1977 ◽  
Vol 14 (1) ◽  
pp. 1-15 ◽  
Author(s):  
H. Kodama ◽  
J. A. McKeague ◽  
R. J. Tremblay ◽  
J. R. Gosselin ◽  
M. G. Townsend
Keyword(s):  
Iron Oxide ◽  
Infrared Absorption ◽  
Thermal Analyses ◽  
Detection Limits ◽  
X Ray Diffraction ◽  
Iron Compounds ◽  
Thermal Methods ◽  
X Ray ◽  
Forms Of Iron Compounds

Iron oxide compounds in 12 selected Canadian soil samples have been characterized by Mössbauer, X-ray, chemical, infrared absorption, and differential thermal methods. Chemical differentiation provides useful information about the forms of iron compounds present such as crystalline, amorphous, inorganic, and organic complexed iron compounds. X-ray diffraction methods can generally identify mineral species of crystalline iron compounds. However, detection limits of goethite and hematite, which are iron oxide minerals commonly present in soils, are about 7% and 10%, respectively. The Mössbauer method is especially useful for identification of small amounts of these iron oxide compounds which are far beyond X-ray detection limits. In addition, information about grain size of hematite and goethite, the Fe3+/Fe2+ ratio and characterization of the 'amorphous' fraction are also available from Mössbauer spectra. Infrared absorption and differential thermal analyses provide supplementary data concerning organic complexed iron compounds.Hematite content in the soils examined is always lower than 10%, but goethite content varies widely and coexistence of both minerals appears to be common.

scholarly journals Structural and Band Structure Investigation of Iron Oxide Nanoparticles Incorporated PVA Nanocomposite Films

2021 ◽  
Author(s):  
Muhammad Aslam ◽  
Muhammad Basit ◽  
Muhammad Ahmad ◽  
Zulfiqar Ali Raza
Keyword(s):  
Iron Oxide ◽  
Analytical Techniques ◽  
Nanocomposite Films ◽  
X Ray Diffraction ◽  
Band Tail ◽  
X Ray ◽  
Vis Spectroscopy ◽  
Uv Visible ◽  
Fabrication And Characterization

Abstract The work reported here deals with the fabrication and characterization of iron oxide (Fe3O4) nanoparticles (NPs – IONPs) incorporated polyvinyl alcohol (PVA)-based nanocomposite films. The nanocomposite films, fabricated via solution casting route, have been characterized using advanced analytical techniques including x-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), and UV-visible (vis.) spectroscopy. There observed notable changes in the structural phases, crystallite size (2.3 to 2.1 nm), d-spacing (0.131 to 0.134 Å), optical absorption edge (5.12 to 4.84 eV), indirect bandgap (4.99 to 4.68 eV), direct bandgap (5.35 to 5.20 eV), and band tail (0.57 to 0.89 eV) from native PVA to nanocomposite films. The refractive index and optical conductivity enhancements were also observed on incorporating IONPs into the PVA matrix. It could be inferred that a minute loading of IONPs might induce significant alternation in opto-structural properties of the PVA-based nanocomposites for potential optoelectronic applications.

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