Comparison of different etch-and-rinse adhesive systems based on shear fatigue dentin bond strength and morphological features the interface

ABSTRACT Introduction One of the possible mechanisms for the gradual destruction of bond strength in dentin-resin interface, could be due to the demineralized unstable collagen matrix. Use of protease inhibitors, such as tannic acid (TA) could prevent destruction of collagen fibers. The aim of this study was to compare the TA effect on bond strength of etch and rinse and self-etch adhesive systems in the dentin of primary teeth. Materials and methods This in vitro study was done on 40 extracted primary molar teeth. The teeth were sectioned in the mesiodistal direction, and enamel of buccal and lingual surfaces was removed. Samples were randomly divided into four groups: Single bond (SB) + TA, SB, Clearfil SE Bond (CSB) + TA, and CSB. Then, Z250 and Clearfil AP-X composites were cured on the surfaces of SB and CSB groups respectively. After that, all samples were divided into aging and non-aging groups. For 3 months, samples were placed under 1,000 thermal cycles in aging group. Subsequently, the shear bond strengths of all groups were measured by the International testing machine, and failure mode was evaluated by an optical stereomicroscope. Data were analyzed with paired t-test and independent t-test. Results Tannic acid induced a significant reduction in the immediate bond strength of adhesive SB. Meanwhile, TA had no significant effect on shear bond strength of the CSB system. Conclusion Based on our findings, use of TA is not recommended with SB and CSB adhesives on primary teeth. Clinical significance Tannic acid may not be considered in resin restorations of primary teeth. How to cite this article Ebrahimi M, Sarraf Shirazi A, Abdolhoseinpour F, Abdollahi M. Effect of Tannic Acid on Bond Strength of Etch and Rinse and Self-etch Adhesive Systems in Dentin of Primary Teeth. J Contemp Dent Pract 2017;18(1):34-38.

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Co-Blend Application Mode of Bulk Fill Composite Resin

Materials ◽

10.3390/ma12162504 ◽

2019 ◽

Vol 12 (16) ◽

pp. 2504

Author(s):

Mohammad Al-Nabulsi ◽

Alaa Daud ◽

Cynthia Yiu ◽

Hanan Omar ◽

Salvatore Sauro ◽

...

Keyword(s):

Bond Strength ◽

Composite Resin ◽

Degree Of Conversion ◽

Adhesive Systems ◽

Bonding Agents ◽

Force Microscopy ◽

Flowable Composite ◽

Etch And Rinse ◽

Significant Difference ◽

Nanoindentation Hardness

Objective: To evaluate the effect of a new application method of bulk-fill flowable composite resin material on bond-strength, nanoleakage, and mechanical properties of dentine bonding agents. Materials and methods: Sound extracted human molars were randomly divided into: manufacturer’s instructions (MI), manual blend 2 mm (MB2), and manual blend 4 mm (MB4). Occlusal enamel was removed and flattened, dentin surfaces were bonded by Prime & Bond universal (Dentsply and Optibond FL, Kerr). For the MI group, adhesives were applied following the manufacturer’s instructions then light-cured. For MB groups, SDR flow+ bulk-fill flowable composite resin was applied in 2- or 4-mm increment then manually rubbed by a micro brush for 15 s with uncured dentine bonding agents and the mixture was light-cured. Composite buildup was fabricated incrementally using Ceram.X One, Dentsply nanohybrid composite resin restorative material. After 24-h water storage, the teeth were sectioned to obtain beams of about 0.8 mm2 for 24-h and thermocycled micro-tensile bond strength at 0.5 mm/min crosshead speed. Degree of conversion was evaluated with micro-Raman spectroscopy. Contraction gaps at 24 h after polymerization were evaluated and atomic force microscopy (AFM) nano-indentation processes were undertaken for measuring the hardness across the interface. Depth of resin penetration was studied using a scanning electron microscope (SEM). Bond strength data was expressed using two-way ANOVA followed by Tukey’s test. Nanoindentation hardness was separately analyzed using one-way ANOVA. Results: Factors “storage F = 6.3” and “application F = 30.11” significantly affected the bond strength to dentine. For Optibond FL, no significant difference in nanoleakage was found in MI/MB4 groups between baseline and aged specimens; significant difference in nanoleakage score was observed in MB2 groups. Confocal microscopy analysis showed MB2 Optibond FL and Prime & Bond universal specimens diffusing within the dentine. Contraction gap was significantly reduced in MB2 specimens in both adhesive systems. Degree of conversion (DC) of the MB2 specimens were numerically more compared to MS1 in both adhesive systems. Conclusion: Present study suggests that the new co-blend technique might have a positive effect on bond strengths of etch-and-rinse adhesives to dentine.

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Effect of Chitosan as a Cross-Linker on Matrix Metalloproteinase Activity and Bond Stability with Different Adhesive Systems

Marine Drugs ◽

10.3390/md18050263 ◽

2020 ◽

Vol 18 (5) ◽

pp. 263 ◽

Cited By ~ 1

Author(s):

Eugenia Baena ◽

Sandra R Cunha ◽

Tatjana Maravić ◽

Allegra Comba ◽

Federica Paganelli ◽

...

Keyword(s):

Matrix Metalloproteinase ◽

Bond Strength ◽

Adhesive Systems ◽

Microtensile Bond Strength ◽

Bond Stability ◽

Etch And Rinse ◽

Mechanical Durability ◽

Human Dentine ◽

Self Etch ◽

Metalloproteinase Activity

The aim of the present study was to evaluate the effect of 0.1% chitosan (Ch) solution as an additional primer on the mechanical durability and enzymatic activity on dentine using an etch-and-rinse (E&R) adhesive and a universal self-etch (SE) adhesive. Microtensile bond strength and interfacial nanoleakage expression of the bonded interfaces for all adhesives (with or without pretreatment with 0.1% Ch solution for 1 min and air-dried for 5 s) were analyzed immediately and after 10,000 thermocycles. Zymograms of protein extracts from human dentine powder incubated with Optibond FL and Scotchbond Universal on untreated or Ch-treated dentine were obtained to examine dentine matrix metalloproteinase (MMP) activities. The use of 0.1% Ch solution as an additional primer in conjunction with the E&R or SE adhesive did not appear to have influenced the immediate bond strength (T0) or bond strength after thermocycling (T1). Zymography showed a reduction in MMP activities only for mineralized and demineralized dentine powder after the application of Ch. Application of 0.1% Ch solution does not increase the longevity of resin–dentine bonds. Nonetheless, the procedure appears to be proficient in reducing dentine MMP activities within groups without adhesive treatments. Further studies are required to comprehend the cross-linking of Ch with dentine collagen.

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Bond Strength Comparison of Orthodontic Bonding Systems: A Systematic Review

Bangladesh Journal of Orthodontics and Dentofacial Orthopedics ◽

10.3329/bjodfo.v7i1.43691 ◽

2019 ◽

pp. 20-26

Author(s):

Tubayesha Hassan ◽

MH Sattar

Keyword(s):

Bond Strength ◽

Shear Bond Strength ◽

Dental Treatment ◽

Enamel Surface ◽

Adhesive Systems ◽

Scientific Review ◽

Bonding System ◽

Etch And Rinse ◽

Bonding Systems ◽

Self Etch

As a means of regular practice in orthodontics and aesthetic dentistry, resin based adhesive systems are being used exclusively. Keeping up with the ever-increasing demand for aesthetic dental treatment all over the world, newer and more improved adhesive systems have been developed. However, regarding the comparison as to which bonding system performs better in clinical perspective, there is lack of existing scientific review articles. In this review, we tend to explore the conventional etch and rinse bonding system and the self-etch primer bonding system. The different tests to assess and compare bond strength between these two types of adhesives from various bibliography are discussed. The results of shear bond strength test, adhesive remnant index (ARI), enamel-adhesive interface using scanning electron microscope (SEM) and the effect of saliva contamination and time are discussed. Interestingly, each system has its strengths and weaknesses. In shear bond strength, self-etch bonding systems clearly exhibits less strength than conventional bonding systems. Resin tags into enamel surface are shorter in self-etch primer adhesives which results from milder etching to enamel compared to the conventional aid-etch and rinse adhesives. Contrarily, the irreversible changes to enamel surface is more aggressive in conventional acid-etching which states that self-etching systems are better according to the principles of minimal intervention dentistry. Ban J Orthod & Dentofac Orthop, April 2017; Vol-7 (1-2), P.20-26

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Determining the Effects of Eugenol on the Bond Strength of Resin-Based Restorative Materials to Dentin: A Meta-Analysis of the Literature

Applied Sciences ◽

10.3390/app10031070 ◽

2020 ◽

Vol 10 (3) ◽

pp. 1070

Author(s):

Isadora M. Garcia ◽

Vicente C. B. Leitune ◽

Maria S. Ibrahim ◽

Mary Anne S. Melo ◽

Vicente Faus Matoses ◽

...

Keyword(s):

Bond Strength ◽

Global Analysis ◽

Meta Analysis ◽

Negative Influence ◽

Accurate Information ◽

Publication Date ◽

Adhesive Systems ◽

Hand Search ◽

Etch And Rinse ◽

Restorative Materials

The aim of this study was to determine whether the residual presence of eugenol in coronal dentin may compromise the bond strength of resin-based restorative materials. A search was performed on MEDLINE/Pubmed, Scopus, and by hand search for relevant papers. No restriction was applied for language and publication date. The studies selected for analysis tested specimens with reduced size (micro-shear bond strength (µSBS) and micro-tensile bond strength (µTBS)) of adhesive systems and resin-based restorative materials applied to coronary dentin “contaminated” with eugenol-based materials. The search provided 335 articles, but only 10 studies met the inclusion criteria. The pooled global analysis showed a significant influence of eugenol, as it negatively influenced the bond strength of resin-based restorations (5.79 (3.31–8.28) MPa, p < 0.00001). The subgroup analyses for conventional etch-and-rinse (p = 0.003) and self-etch (p < 0.0004) adhesive systems, as well as for µSBS (p = 0.01) and µTBS (p < 0.0001), showed a negative influence of eugenol on the bond strength. Data were statistically heterogeneous. However, it was possible to observe that eugenol could negatively affect the bonding of resin-based restorative materials to dentin. Further evidence is necessary in order to acquire more accurate information about this issue and confirm that the residual presence of eugenol in dentin compromises the bond strength of resin-based materials.

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Bond Strength of Two-Step Etch-and-Rinse Adhesive Systems to the Dentin of Primary and Permanent Teeth

Journal of Clinical Pediatric Dentistry ◽

10.17796/jcpd.35.2.958893530534m503 ◽

2010 ◽

Vol 35 (2) ◽

pp. 163-168 ◽

Cited By ~ 6

Author(s):

Hérica Adad Ricci ◽

Mariane Emi Sanabe ◽

Carlos Alberto de Souza Costa ◽

Josimeri Hebling

Keyword(s):

Bond Strength ◽

Adhesive System ◽

Permanent Tooth ◽

Permanent Teeth ◽

Adhesive Systems ◽

Microtensile Bond Strength ◽

Human Teeth ◽

Cross Sectional ◽

Etch And Rinse ◽

The Mean

Objective: The purpose of this study was to compare the immediate microtensile bond strength (µTBS) of two-step etch-and-rinse adhesive systems to the dentin of primary and permanent teeth. Study Design: Non-carious human teeth (12 primary molars and 12 premolars) were assigned to 3 groups according to the adhesive system. The adhesive systems were applied to flat superficial coronal dentin surfaces etched with phosphoric acid and composite resin blocks were built up. The teeth were sectioned to produce beam-shaped specimens with 0.81 mm2 cross-sectional area subjected to µTBS testing. µTBS data were analyzed statistically by ANOVA and Tukey’s test (a= 0.05). Results: The adhesive systems produced statistically similar mean µTBS to each other (p>0.05) and no significant differences (p>0.05) were found when the same material was applied to primary or permanent tooth dentin. The mean µTBS values (MPa) obtained were: Prime& Bond NT: 41.7±14.4 (permanent) and 40.8±13.4 (primary); Single Bond: 42.9±8.6 (permanent) and 41.4±11.9 (primary); Excite DSC: 46.3±11.3 (permanent teeth) and 43.4±12.0 (primary). Conclusion:There was no difference in the immediate µTBS of two-step etch-and-rinse adhesive systems when applied to the dentin of primary and permanent teeth.

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Effect of Enamel Etching Time on Roughness and Bond Strength

Operative Dentistry ◽

10.2341/08-72 ◽

2009 ◽

Vol 34 (2) ◽

pp. 217-222 ◽

Cited By ~ 49

Author(s):

W. W. Barkmeier ◽

R. L. Erickson ◽

N. S. Kimmes ◽

M. A. Latta ◽

T. M. Wilwerding

Keyword(s):

Phosphoric Acid ◽

Bond Strength ◽

Clinical Relevance ◽

Etching Time ◽

Application Time ◽

Adhesive Systems ◽

Etch And Rinse

Clinical Relevance Traditionally, etch-and-rinse adhesive systems have used phosphoric acid to condition enamel surfaces and successfully create a strong, durable bond to resin-based materials. Newer adhesive systems now use acid monomers to bond resin materials to both enamel and dentin. These newer adhesives do not provide the same degree of bonding to enamel as etch-and-rinse systems, and extending the application time does not improve their performance.

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Effect of Ethanol Wet Bonding Technique on the Durability of Resin- Dentin Bond with Contemporary Adhesive Systems

Journal of Clinical Pediatric Dentistry ◽

10.17796/jcpd.39.2.p14u4x3q14272452 ◽

2015 ◽

Vol 39 (2) ◽

pp. 133-142 ◽

Cited By ~ 6

Author(s):

R Nagpal ◽

N Manuja ◽

IK Pandit

Keyword(s):

Bond Strength ◽

Shear Bond Strength ◽

Sem Analysis ◽

Adhesive Systems ◽

Etch And Rinse ◽

Two Samples ◽

Significant Difference ◽

Permanent Molars ◽

Bonding Technique

Objective: To evaluate the effect of ethanol wet bonding technique on the immediate and long term bond strength of simplified etch and rinse adhesive systems to dentin. Study Design: 96 extracted human permanent molars were ground to expose the flat dentin surface. The teeth were divided into four groups (n=24) according to the adhesives used, either Tetric N Bond or Solobond M and bonding techniques i.e. water wet bonding or ethanol wet bonding (EWB). Composite cylinder was bonded to each specimen using the respective adhesive technique. Ten samples from each group were then tested immediately for shear bond strength evaluation and two samples for SEM analysis. The remaining samples (12) were tested after 6 month storage in distilled water. Results: Upon immediate testing, there was no significant difference in the mean shear bond strength of the groups regardless of the bonding technique or adhesive used. The bond strength fell dramatically in the water wet bonded specimens after 6 months water storage, while the bond strength of both the adhesives was maintained when EWB technique was used. SEM observation revealed good interfacial adaptation in EWB groups even after six months. Conclusion: For both simplified etch and rinse adhesives used, ethanol wet bonding technique led to significant preservation of the resin dentin bond over 6 months.

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Adhesive Temperature: Effects on Adhesive Properties and Resin-Dentin Bond Strength

Operative Dentistry ◽

10.2341/10-218l ◽

2011 ◽

Vol 36 (3) ◽

pp. 293-303 ◽

Cited By ~ 14

Author(s):

AD Loguercio ◽

D Salvalaggio ◽

AE Piva ◽

CA Klein-Júnior ◽

M de LR Accorinte ◽

...

Keyword(s):

Bond Strength ◽

Temperature Effects ◽

Adhesive Layer ◽

Adhesive Systems ◽

Adhesive Properties ◽

Fourier Transformed Infrared Spectroscopy ◽

Etch And Rinse ◽

Water Based ◽

Demineralized Dentin ◽

Scanning Electron

SUMMARY Objectives To evaluate the effect of adhesive temperature on the resin-dentin bond strength (μTBS), nanoleakage (NL), adhesive layer thickness (AL), and degree of conversion (DC) of ethanol/water- (SB) and acetone-based (PB) etch-and-rinse adhesive systems. Methods The bottles of the two adhesives were kept at each temperature (5°C, 20°C, 37°C, and 50°C) for 2 hours before application to demineralized dentin surfaces of 40 molars. Specimens were prepared for μTBS testing. Bonded sticks (0.8 mm2) were tested under tension (0.5 mm/min). Three bonded sticks from each tooth were immersed in silver nitrate and analyzed by scanning electron microscopy. The DC of the adhesives was evaluated by Fourier transformed infrared spectroscopy. Results Lower μTBS was observed for PB at 50°C. For SB, the μTBS values were similar for all temperatures. DC was higher at 50°C for PB. Higher NL and thicker AL were observed for both adhesives in the 5°C and 20°C groups compared to the 37°C and 50°C groups. The higher temperatures (37°C or 50°C) reduced the number of pores within the adhesive layer of both adhesive systems. Conclusions It could be useful to use an ethanol/water-based adhesive at 37°C or 50°C and an acetone-based adhesive at 37°C to improve adhesive performance.

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