scholarly journals Nanostructured silver vanadate decorated with silver particles and their applicability in dental materials: a scope review

Heliyon ◽  
2021 ◽  
pp. e07168
Author(s):  
Murilo Rodrigues de Campos ◽  
André Luís Botelho ◽  
Andréa Cândido dos Reis
Author(s):  
C. F. Oster

Although ultra-thin sectioning techniques are widely used in the biological sciences, their applications are somewhat less popular but very useful in industrial applications. This presentation will review several specific applications where ultra-thin sectioning techniques have proven invaluable.The preparation of samples for sectioning usually involves embedding in an epoxy resin. Araldite 6005 Resin and Hardener are mixed so that the hardness of the embedding medium matches that of the sample to reduce any distortion of the sample during the sectioning process. No dehydration series are needed to prepare our usual samples for embedding, but some types require hardening and staining steps. The embedded samples are sectioned with either a prototype of a Porter-Blum Microtome or an LKB Ultrotome III. Both instruments are equipped with diamond knives.In the study of photographic film, the distribution of the developed silver particles through the layer is important to the image tone and/or scattering power. Also, the morphology of the developed silver is an important factor, and cross sections will show this structure.


Author(s):  
H. Seiler ◽  
U. Haas ◽  
K.H. Körtje

The physical properties of small metal particles reveal an intermediate position between atomic and bulk material. Especially Ag has shown pronounced size effects. We compared silver layers evaporated in high vacuum with cluster layers of small silver particles, evaporated in N2 at a pressure of about 102 Pa. The investigations were performed by electron optical methods (TEM, SEM, EELS) and by Photoacoustic (PA) Spectroscopy (gas-microphone detection).The observation of cluster layers with TEM and high resolution SEM show small silver particles with diameters of about 50 nm (Fig. 1 and Figure 2, respectively). The electron diffraction patterns of homogeneous Ag layers and of cluster layers are similar, whereas the low loss EELS spectra due to plasmon excitation are quite different. Fig. 3 and Figure 4 show first results of EELS spectra of a cluster layer of small silver particles on carbon foil and of a homogeneous Ag layer, respectively.


1973 ◽  
Vol 37 (2) ◽  
pp. 39-42
Author(s):  
JB Moser ◽  
EP Lautenschlager ◽  
BK Moore ◽  
EH Greener

2020 ◽  
Vol 9 (4) ◽  
pp. e27942662
Author(s):  
Patrícia Capellato ◽  
Cláudia Eliana Bruno Marino ◽  
Gilbert Silva ◽  
Lucas Victor Benjamim Vasconcelos ◽  
Rodrigo Perito Cardoso ◽  
...  

During the last decades, researchers have been growing the interest in surface treatment with an antimicrobial agent. Silver nanoparticles (AgNPs) are widely used in biomedical fields due to their potent antimicrobial activity. So, in this study was investigated silver particles (isles) coated on titanium surface for dental and orthopedic application. Silver particles coating process on titanium surface were performed via sputtering that is a plasma-assisted deposition technique with and titanium without treatment was applied as comparing standard. Plasma treatment parameters were optimized so that the result was not a thin film of Ag but dispersed particles of Ag on the Ti-cp surface. The alloy surfaces were investigated using scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDS). In order to investigate antibacterial potential Staphylococcus aureus and Escherichia coli have been used at Agar diffusion assay. The results were analyzed by analysis of variance (ANOVA) in order to verify significant difference antimicrobial activity between samples that have shown no difference between the surfaces studied treatments. For silver deposition scattered particles (isles) over titanium surface for a 10-minute treatment, EDS revealed by silver clusters that the particles were not properly scattered onto surface, hence, the low effectiveness in antibacterial activity.


2020 ◽  
Vol 33 (2) ◽  
pp. 102-105
Author(s):  
Joanna Bialowska ◽  
Witold Bojar ◽  
Tomasz Zareba ◽  
Stefan Tyski ◽  
Barbara Tymczyna-Borowicz

AbstractCross-infection involves the transmission of microorganisms through secretions, bodily fluids and excreta, as well as undisinfected surfaces and medical equipment. In the dental office, diseases are transmitted via various routes, e.g. from patient to dentist or other member of dental team, from doctor or dental team member to patient, from patient to another patient, from dental office to community and from community to patient. The study was conducted to evaluate the effectiveness of infection control in dental practices based on the qualitative and quantitative assessment of microbiological contaminants detected on the surface of filling material packaging used in dental offices. The material for research were 9 packages containing dental materials during their use in 3 dental settings. The packages were placed in sterile flasks and rinsed to wash microorganisms from the surfaces. The washes were filtered through membrane filters and cultured under proper aerobic and anaerobic conditions, and at elevated CO2 concentration. Microbial growth on TIO and TSB media was observed. The contamination of most samples remained low as indicated by the growth from one to a maximum of five colonies on TSA. The contamination remained at the level of 10-50 CFU/package, i.e. <100 CFU/single package. The tests evaluating the contamination of dental package surfaces with aerobic bacteria confirmed high hygiene standards observed in dental offices from which the packages were brought.


Author(s):  
Жанна Владимировна Вечеркина ◽  
Наталия Владимировна Чиркова ◽  
Михаил Анатольевич Крючков ◽  
Виктор Сергеевич Калиниченко

Развитие технологий, основанных на использовании низкотоксичных материалов, позволит в скором будущем начать их применение в медицине. Применение наночастиц серебра, меди, кремния, цинка, титана, кобальта в качестве модифицирующей добавки позволит оказать активное влияние на структуру исходных материалов и изменение их свойств, а именно улучшение физико-механических, физико-химических и токсико-гигиенических свойств материалов. Наноразмерные частицы кремния, введенные в фиксирующие стоматологические материалы, приводят к улучшению физико-химических, физико-механических свойств кристаллизующихся материалов, а малая теплопроводность кремния может увеличить его рабочее время и снизить выделение тепла при реакции кристаллизации. Так как от этих характеристик зависит объем манипуляций, при фиксации ортопедических конструкций на опорных зубах целесообразно было бы привести рабочее время твердения к чистому времени твердения, что позволит увеличить объем манипуляций приготовленной массой без ухудшения ее свойств. Разработка высокопрочных, биосовместимых, высокотехнологичных нанопластмасс для базисов съемных пластиночных протезов является актуальной проблемой повышения качества жизни пациентов. Модификация наноразмерными частицами серебра, кремния акрилового полимера позволит улучшить такие физико-механические свойства, как ударную вязкость, прочность, температуростойкость, барьерные свойства, уменьшить усадку полимера на этапе полимеризации, в отличие от уже известных отечественных и дорогостоящих импортных полимеров. Наноразмерные частицы кремния, серебра являются сокатализаторами метилметакрилата, влияющими на уменьшение количества остаточного мономера после процесса полимеризации, тем самым повышая санитарно-химические и токсико-гигиенические характеристики полимера. Все вышеизложенное позволило сформулировать цель исследований по наноструктурированным материалам под руководством профессора …посвящается памяти профессора, д.м.н. Каливраджияна Э.С. The development of technologies based on the use of low-toxic materials will make it possible to begin their application in medicine in the near future. The use of nanoparticles of silver, copper, silicon, zinc, titanium, cobalt as a modifying additive will make it possible to actively influence the structure of the starting materials and change their properties, namely, improve the physicomechanical, physicochemical and toxicohygienic properties of materials. Nanosized silicon particles introduced into fixing dental materials lead to an improvement in the physicochemical, physicomechanical properties of crystallizing materials, and the low thermal conductivity of silicon can increase its working time and reduce heat generation during the crystallization reaction. Since the volume of manipulations depends on these characteristics, when fixing orthopedic structures on abutment teeth, it would be advisable to bring the working time of hardening to a pure hardening time, which will increase the volume of manipulations with the prepared mass without deteriorating its properties. The development of high-strength, biocompatible, high-tech nanoplastics for the bases of removable plate prostheses is an urgent problem to improve the quality of life of patients. Modification of acrylic polymer with nano-sized particles of silver and silicon will improve such physical and mechanical properties as impact strength, strength, temperature resistance, barrier properties, and reduce polymer shrinkage at the stage of polymerization, in contrast to the already known domestic and expensive imported polymers. Nanosized particles of silicon, silver are cocatalysts of methyl methacrylate, affecting the reduction of the amount of residual monomer after the polymerization process, thereby increasing the sanitary-chemical and toxic-hygienic characteristics of the polymer. All of the above made it possible to formulate the goal of research on nanostructured materials under the guidance of the professor …dedicated to the memory of the professor, d.m.s. Kalivrajiyan E.S.


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