Ultra-fine nickel sulfide nanoclusters @ nickel sulfide microsphere as enzyme-free electrode materials for sensitive detection of lactic acid

2020 ◽  
Vol 874 ◽  
pp. 114465
Author(s):  
Mani Arivazhagan ◽  
Govindhan Maduraiveeran
2021 ◽  
Author(s):  
C. Sambathkumar ◽  
R. Ranjithkumar ◽  
S. Ezhil Arasi ◽  
A. Manikandan ◽  
N. Nallamuthu ◽  
...  

Abstract High-performance energy storage electrode materials are emerging demand in near future for the construction of supercapacitor with high energy and power densities. Herein, Nickel (II) Diethyldithiocarbamate was used as single source precursor for Nickel Sulfide (Ni9S8) two dimensional (2D) nanosheets preparation and hexadecylamine as shape directing agent via simple solvothermal method. The orthorhombic structure of Ni9S8 nanosheets was confirmed by X-ray diffraction (XRD) pattern. Scanning electron microscopy (SEM) and high resolution transmission electron microscopy (HRTEM) images revealed that as-prepared Ni9S8 nanoparticles possess sheet-like morphology. Besides, the thermal stability of Ni(DTC)2 complex was studied by Thermo-gravimetric/Derivative thermo gravimetric(TG/DTG) with Differential scanning calorimetric (DSC) analysis. The electrochemical properties of Ni9S8 nanosheets was studied using galvanostatic charge-discharge (GCD) and cyclic voltammetry (CV) techniques. From the charge-discharge study of Ni9S8 nanosheets, a high specific capacitance of 281 Fg− 1 was obtained at a current density of 1 Ag− 1, and up to 82 % retentivity was achieved after 5000 cycles. Thus, the prepared Ni9S8 nanosheets could be one of the attractive potential active electrode materials for the application of supercapacitor.


2020 ◽  
Vol 12 (32) ◽  
pp. 4097-4099
Author(s):  
Xuyue Chen ◽  
Rui Shen ◽  
Sidi Liu ◽  
Xiang Xiao ◽  
Jun Yan ◽  
...  

Correction for ‘The sensitive detection of single-cell secreted lactic acid for glycolytic inhibitor screening with a microdroplet biosensor’ by Xuyue Chen et al., Anal. Methods, 2020, 12, 3250–3259, DOI: 10.1039/D0AY00633E.


2020 ◽  
Vol 12 (25) ◽  
pp. 3250-3259 ◽  
Author(s):  
Xuyue Chen ◽  
Rui Shen ◽  
Sidi Liu ◽  
Xiang Xiao ◽  
Jun Yan ◽  
...  

Lactic acid (LA) plays an important role in the tumor metabolism and malignant progression of various cancers.


2013 ◽  
Vol 712-715 ◽  
pp. 760-763
Author(s):  
Min Tang ◽  
Bao Liang Ge ◽  
Shu Ming Wen

It is known that oxidation is one of the most common ways for penlandite to be introducted into tailing during traditional coarse-particle sulfide flotation. However, it could become much more complicated and challenging problems for the low-grade, fine-disseminated Cu-Ni sulfides containing Pt and Pd in Yunnan Mine, accompanied with more than 75% of the content of MgO in the ore sample is. Direct flotation tests had been conducted to extract the metallic values as much as possible by adding traditional depressants and collectors, such as carboxylmethyl cellulose, starch, sodium silicate, butyl xanthate, (BX), butyl ammonium dithophosphate (BA) and etc., the relatively satisfied recoveries of Cu, Ni, Pt and Pd in the concentrate from bench flotation tests were obtained, however, more than 30% of metallic values still lost in the slime. In this study, bench flotation tests for the ore sample fromYunnan Mine, micro-flotation tests of serpentines and pentlandite from Jinchuan Mine and their settling rate tests were conducted to figure out how the oxidation influence the recovery of the ultra-fine nickel sulfide. All the tests results pointed to the presence of over-oxidation on the ultra-fine nickel sulfide surface and lead to the loss of Ni containing Pt and Pd in the slime tailing. Some methods which tried to slow the speed of oxidation on mineral surface during grinding and flotation were introduced in order to recover the values before over-oxidation of sulfides; however, the slime coating of serpentines also may play an important role in disturbing the floatability of ultra-fine sulfide.


2015 ◽  
Vol 163 (3) ◽  
pp. H159-H170 ◽  
Author(s):  
Rajeev Jain ◽  
Nimisha Jadon ◽  
Kshiti Singh

2021 ◽  
Vol 2021 ◽  
pp. 1-11
Author(s):  
Jiezeng Chen ◽  
Hongying Shu ◽  
Pingping Niu ◽  
Pinghua Chen ◽  
Hualin Jiang

Due to the abuse application of antibiotics in the recent decades, a high level of antibiotics has been let out and remains in our environment. Electrochemical sensing is a useful method to sensitively detect antibiotics, and the key factor for a successful electrochemical sensor is the active electrode materials. In this study, a sensitive electrochemical sensing platform based on a metal-organic framework (MOF) of MIL-53 (Fe) was facilely fabricated. It shows highly selective and sensitive detection performance for trace tetracycline. Differential pulse voltammetry (DPV) was applied to analyze the detection of tetracycline. The linear range of tetracycline detection was 0.0643 μmol/L-1.53 μmol/L, and the limit of detection (LOD) is 0.0260 μmol/L. Furthermore, the MOF-enabled sensor can be effectively used in actual water bodies. The results indicate that the electrochemical sensor is a high potential sensing platform for tetracycline.


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