Evaluation of pH and Calcium Ion Release of a Dual-cure Bisphenol A Ethoxylate Dimethacrylate/Mineral Trioxide Aggregate–based Root-end Filling Material

2013 ◽  
Vol 39 (12) ◽  
pp. 1603-1606 ◽  
Author(s):  
Giane da Silva Linhares ◽  
Maximiliano Sérgio Cenci ◽  
César Blaas Knabach ◽  
Camila Mizette Oliz ◽  
Mariana Antunes Vieira ◽  
...  
2006 ◽  
Vol 32 (12) ◽  
pp. 1194-1197 ◽  
Author(s):  
E ANTUNESBORTOLUZZI ◽  
N JUAREZBROON ◽  
M ANTONIOHUNGARODUARTE ◽  
A DEOLIVEIRADEMARCHI ◽  
C MONTEIROBRAMANTE

2021 ◽  
Vol 2021 ◽  
pp. 1-6
Author(s):  
Teena Sheethal Dsouza ◽  
Aditya Shetty ◽  
Neevan Dsouza

An experimental calcium silicate-based root-end filling material incorporated with silver nanoparticles intended for use in periapical surgeries was developed with the purpose to overcome the drawbacks of existing materials and to satisfy the ideal requirements of root-end filling materials. This study was designed to evaluate the physicochemical properties, pH, calcium ion release, and dimensional stability of the experimental cement, and compare the results with commercially available ProRoot MTA (Dentsply). An independent sample test was used to analyze the data. Mean initial pH (immediately after mixing) of the experimental cement was 10.42 ± 0.04 which was higher than that of MTA. However, there was a significant increase in pH of MTA at 1 day, 2 days, and 7 days. Presence of calcium chloride favored the release of calcium ions which was significantly increased in the experimental group at 24 hours. At the end of 30 days, MTA showed a significant expansion when compared to the experimental cement p < 0.001 . In conclusion, the experimental nanoparticle-incorporated calcium silicate-based cement showed clinically acceptable physicochemical properties.


2016 ◽  
Vol 2016 ◽  
pp. 1-6 ◽  
Author(s):  
Toshiaki Baba ◽  
Yasuhisa Tsujimoto

The purpose of this study was to improve the operability of calcium silicate cements (CSCs) such as mineral trioxide aggregate (MTA) cement. The flow, working time, and setting time of CSCs with different compositions containing low-viscosity methyl cellulose (MC) or hydroxypropyl cellulose (HPC) additive were examined according to ISO 6876-2012; calcium ion release analysis was also conducted. MTA and low-heat Portland cement (LPC) including 20% fine particle zirconium oxide (ZO group), LPC including zirconium oxide and 2 wt% low-viscosity MC (MC group), and HPC (HPC group) were tested. MC and HPC groups exhibited significantly higher flow values and setting times than other groups (p<0.05). Additionally, flow values of these groups were higher than the ISO 6876-2012 reference values; furthermore, working times were over 10 min. Calcium ion release was retarded with ZO, MC, and HPC groups compared with MTA. The concentration of calcium ions was decreased by the addition of the MC or HPC group compared with the ZO group. When low-viscosity MC or HPC was added, the composition of CSCs changed, thus fulfilling the requirements for use as root canal sealer. Calcium ion release by CSCs was affected by changing the CSC composition via the addition of MC or HPC.


2013 ◽  
Vol 47 (2) ◽  
pp. 120-126 ◽  
Author(s):  
B. C. Cavenago ◽  
T. C. Pereira ◽  
M. A. H. Duarte ◽  
R. Ordinola-Zapata ◽  
M. A. Marciano ◽  
...  

2009 ◽  
Vol 35 (10) ◽  
pp. 1418-1421 ◽  
Author(s):  
Mário Tanomaru-Filho ◽  
Frederico Bordini Chaves Faleiros ◽  
Juliana Nogueira Saçaki ◽  
Marco Antonio Hungaro Duarte ◽  
Juliane Maria Guerreiro-Tanomaru

2011 ◽  
Vol 37 (6) ◽  
pp. 844-846 ◽  
Author(s):  
Santiago Massi ◽  
Mário Tanomaru-Filho ◽  
Guilherme Ferreira Silva ◽  
Marco Antonio Hungaro Duarte ◽  
Larissa Tercilia Grizzo ◽  
...  

2020 ◽  
Vol 44 (1) ◽  
Author(s):  
Manar Galal ◽  
Dalia Y. Zaki ◽  
Mohamed I. Rabie ◽  
Samia M. El-Shereif ◽  
Tamer M. Hamdy

Materials ◽  
2021 ◽  
Vol 14 (7) ◽  
pp. 1693
Author(s):  
Tae-Yun Kang ◽  
Ji-Won Choi ◽  
Kyoung-Jin Seo ◽  
Kwang-Mahn Kim ◽  
Jae-Sung Kwon

Commercial mineral trioxide aggregate (MTA) materials such as Endocem MTA (EC), Dia-Root Bio MTA (DR), RetroMTA (RM), and ProRoot MTA (PR) are increasingly used as root-end filling materials. The aim of this study was to assess and compare the physicochemical and mechanical properties and cytotoxicity of these MTAs. The film thicknesses of EC and DR were considerably less than that of PR; however, RM’s film thickness was greater than that of PR. In addition, the setting times of EC, DR, and RM were shorter than that of PR (p < 0.05). The solubility was not significantly different among all groups. The three relatively new MTA groups (EC, DR, and RM) exhibited a significant difference in pH variation and calcium ion release relative to the PR group (p < 0.05). The radiopacity of the three new MTAs was considerably less than that of PR. The mechanical strength of RM was not significantly different from that of PR (p > 0.05); however, the EC and DR groups were not as strong as PR (p < 0.05). All MTA groups revealed cytocompatibility. In conclusion, the results of this study confirmed that EC, RM, DR, and PR exhibit clinically acceptable physicochemical and mechanical properties and cell cytotoxicity.


Materials ◽  
2021 ◽  
Vol 14 (2) ◽  
pp. 340
Author(s):  
Sivaprakash Rajasekharan ◽  
Chris Vercruysse ◽  
Luc Martens ◽  
Ronald Verbeeck

The authors wish to make the following correction to the paper [...]


Materials ◽  
2021 ◽  
Vol 14 (9) ◽  
pp. 2139
Author(s):  
Bilal Marie ◽  
Raymond Clark ◽  
Tim Gillece ◽  
Seher Ozkan ◽  
Michael Jaffe ◽  
...  

A series of bio-based hydrophobically modified isosorbide dimethacrylates, with para-, meta-, and ortho- benzoate aromatic spacers (ISBGBMA), are synthesized, characterized, and evaluated as potential dental restorative resins. The new monomers, isosorbide 2,5-bis(4-glyceryloxybenzoate) dimethacrylate (ISB4GBMA), isosorbide 2,5-bis(3-glyceryloxybenzoate) dimethacrylate (ISB3GBMA), and isosorbide 2,5-bis(2-glyceryloxybenzoate) dimethacrylate (ISB2GBMA), are mixed with triethylene glycol dimethacrylate (TEGDMA) and photopolymerized. The resulting polymers are evaluated for the degree of monomeric conversion, polymerization shrinkage, water sorption, glass transition temperature, and flexural strength. Isosorbide glycerolate dimethacrylate (ISDGMA) is synthesized, and Bisphenol A glycerolate dimethacrylate (BisGMA) is prepared, and both are evaluated as a reference. Poly(ISBGBMA/TEGDMA) series shows lower water sorption (39–44 µg/mm3) over Poly(ISDGMA/TEGDMA) (73 µg/mm3) but higher than Poly(BisGMA/TEGDMA) (26 µg/mm3). Flexural strength is higher for Poly(ISBGBMA/TEGDMA) series (37–45 MPa) over Poly(ISDGMA/TEGDMA) (10 MPa) and less than Poly(BisGMA/TEGDMA) (53 MPa) after immersion in phosphate-buffered saline (DPBS) for 24 h. Poly(ISB2GBMA/TEGDMA) has the highest glass transition temperature at 85 °C, and its monomeric mixture has the lowest viscosity at 0.62 Pa·s, among the (ISBGBMA/TEGDMA) polymers and monomer mixtures. Collectively, this data suggests that the ortho ISBGBMA monomer is a potential bio-based, BPA-free replacement for BisGMA, and could be the focus for future study.


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