scholarly journals Evaluation of pH, Calcium Ion Release, and Dimensional Stability of an Experimental Silver Nanoparticle-Incorporated Calcium Silicate-Based Cement

2021 ◽  
Vol 2021 ◽  
pp. 1-6
Author(s):  
Teena Sheethal Dsouza ◽  
Aditya Shetty ◽  
Neevan Dsouza
Keyword(s):  
Physicochemical Properties ◽  
Dimensional Stability ◽  
Calcium Ion ◽  
Calcium Silicate ◽  
Filling Material ◽  
Ion Release ◽  
Filling Materials ◽  
Sample Test ◽  
Initial Ph ◽  
Experimental Group

An experimental calcium silicate-based root-end filling material incorporated with silver nanoparticles intended for use in periapical surgeries was developed with the purpose to overcome the drawbacks of existing materials and to satisfy the ideal requirements of root-end filling materials. This study was designed to evaluate the physicochemical properties, pH, calcium ion release, and dimensional stability of the experimental cement, and compare the results with commercially available ProRoot MTA (Dentsply). An independent sample test was used to analyze the data. Mean initial pH (immediately after mixing) of the experimental cement was 10.42 ± 0.04 which was higher than that of MTA. However, there was a significant increase in pH of MTA at 1 day, 2 days, and 7 days. Presence of calcium chloride favored the release of calcium ions which was significantly increased in the experimental group at 24 hours. At the end of 30 days, MTA showed a significant expansion when compared to the experimental cement p < 0.001 . In conclusion, the experimental nanoparticle-incorporated calcium silicate-based cement showed clinically acceptable physicochemical properties.

scholarly journals Evaluation of Physicochemical Properties of New Calcium Silicate-Based Sealer

2018 ◽  
Vol 29 (6) ◽  
pp. 536-540 ◽  
Author(s):  
Aline Teixeira Mendes ◽  
Paula Barcellos da Silva ◽  
Bruna Barcelos Só ◽  
Lina Naomi Hashizume ◽  
Rodrigo Ricci Vivan ◽  
...  
Keyword(s):  
Physicochemical Properties ◽  
Calcium Ion ◽  
Calcium Silicate ◽  
Calcium Release ◽  
Setting Time ◽  
Porto Alegre ◽  
Ion Release ◽  
Ph Values ◽  
Time Flow ◽  
Ah Plus

Abstract This study aimed to evaluate the physicochemical properties of a calcium silicate-based sealer (Sealer Plus BC; MK Life, Porto Alegre, Brazil) compared with an epoxy-resin sealer (AH Plus; Dentsply DeTrey GmbH, Konstanz, Germany). Initial and final setting time was assessed based on ISO 6876:2012 and ASTM C266:03. Calcium ion release and pH were evaluated by filling polyethylene tubes with sealers and then immersing them in 10 mL of deionized water. Following experimental periods of 1, 24, 72 and 168 hours, the samples were measured regarding pH and calcium ion release with a pH meter and a colorimetric spectrophotometer, respectively. The flow was examined based on ISO 6876:2012. Rings of 10 mm in diameter with 1 mm thickness were prepared to analyze the radiopacity (ISO 6876:2012 and ADA n.57) and solubility (ISO 6876:2012). The data were analyzed by variance analysis, Student-T and Tukey tests (p<0.05). The calcium ion release and pH values were significantly higher for the Sealer Plus BC compared with the AH Plus (p<0.05). Lower setting time, flow and radiopacity were observed for the bioceramic sealer than for AH Plus (p<0.05). Sealer Plus BC exhibited higher solubility compared with AH Plus (p<0.05). Sealer Plus BC showed physicochemical properties as setting time, pH, calcium release, flow, and radiopacity following the required standards, but higher solubility than the minimum values required by ISO 6876:2012.

Evaluation of pH and Calcium Ion Release of a Dual-cure Bisphenol A Ethoxylate Dimethacrylate/Mineral Trioxide Aggregate–based Root-end Filling Material

2013 ◽  
Vol 39 (12) ◽  
pp. 1603-1606 ◽  
Author(s):  
Giane da Silva Linhares ◽  
Maximiliano Sérgio Cenci ◽  
César Blaas Knabach ◽  
Camila Mizette Oliz ◽  
Mariana Antunes Vieira ◽  
...  
Keyword(s):  
Bisphenol A ◽  
Calcium Ion ◽  
Mineral Trioxide Aggregate ◽  
Filling Material ◽  
Ion Release

scholarly journals The use of bioceramic root canal sealers for obturation of the root canal system: A review

2021 ◽  
Vol 2 (1) ◽  
pp. 14-25
Author(s):  
Musliana Mustaffa
Keyword(s):  
Physicochemical Properties ◽  
Root Canal ◽  
Scientific Evidence ◽  
Filling Material ◽  
Flow Properties ◽  
Filling Materials ◽  
System A ◽  
Root Canal System ◽  
Root Canal Sealers ◽  
Selection Of

The use of bioceramic root canal sealers in endodontics is a promising approach because of the advantages such as improved flow properties, biocompatible and could promote the formation of hard tissue. Due to the recent technology and limited scientific evidence, the effectiveness of bioceramic root canal sealers remains unclear. This article focuses on the physicochemical properties, biocompatibility, biomineralisation, retreatability, 3D obturation and current practice of using bioceramic root canal sealers. The relevant articles for this review were searched manually from Google Scholar and PubMed using keywords ‘bioceramic root filling material AND endodontics’, ‘bioceramic root canal sealers AND endodontics’, ‘cytotoxicity AND bioceramic root canal sealers’, ‘bioceramic root canal sealers AND physicochemical properties’, ‘biomineralisation AND bioceramic root canal sealers’ and ‘retreatment efficacy AND bioceramic root filling materials’. Since the clinical data concerning the obturation with bioceramic root canal sealers is lacking, the selection of materials should be made based on the available scientific evidence, individual cases, material availability and operator’s preference.

scholarly journals A New Calcium Silicate-Based Root Canal Dressing: Physical and Chemical Properties, Cytotoxicity and Dentinal Tubule Penetration

2020 ◽  
Vol 31 (6) ◽  
pp. 598-604
Author(s):  
Natália Villa ◽  
Vanessa Valgas Dos Santos ◽  
Ubirajara Maciel da Costa ◽  
Aline Teixeira Mendes ◽  
Pedro Henrique Marks Duarte ◽  
...  
Keyword(s):  
Calcium Hydroxide ◽  
Calcium Ion ◽  
Calcium Silicate ◽  
Chemical Properties ◽  
Dentinal Tubule ◽  
Ion Release ◽  
Tukey Test ◽  
Physical And Chemical ◽  
Tubule Penetration ◽  
And Chemical Properties

Abstract The aims of this study were to evaluate the physical and chemical properties, cytotoxicity and dentinal tubule penetration of a new calcium silicate-based root canal dressing. For pH and calcium ion release evaluation (1, 24, 72 and 168 h) were used a pH meter and colorimetric spectrophotometer, respectively. Radiopacity evaluation followed the ISO 6876:2012. Cytotoxicity was evaluated by the percentage of cell viability using MTT assay. Illustrative images of dentinal tubule penetration were obtained using confocal laser scanning microscopy (CLSM). Data from pH and calcium ion release were statistically analyzed by two-way analysis of variance and Tukey test. Radiopacity was analyzed using the Student t-test. The statistical tests for cytotoxicity results were the one-way analysis of variance and Tukey test. Both materials showed alkaline pH in all experimental times. The pH values for calcium hydroxide paste were higher than bioceramic paste at 1, 24, and 72 h (p<0.05). The calcium ion release of bioceramic was lower than the calcium hydroxide paste only at 24 h (p<0.05). The bioceramic was more radiopaque than the calcium hydroxide paste (p<0.05). Bioceramic paste presented a dose and time-dependent cytotoxic effect after MTT assay. CLSM images showed absence of tubule penetration for both pastes. The new calcium silicate-based canal dressing presented alkaline pH, high calcium release, and acceptable radiopacity. Bio C Temp showed a dose and time-dependent cytotoxic and absence of dentinal tubule penetration.

Biodentine: um substituto ao MTA?

2019 ◽  
Vol 9 (3) ◽  
pp. 29-36
Author(s):  
Maíra do Prado ◽  
Carolina Oliveira de Lima ◽  
Hugo Gonçalves Dutra ◽  
Jefferson Marion ◽  
Maria Das Graças Afonso Miranda Chaves ◽  
...  
Keyword(s):  
Compressive Strength ◽  
Bond Strength ◽  
Physicochemical Properties ◽  
Calcium Silicate ◽  
Setting Time ◽  
Filling Material ◽  
Retrograde Filling

Objetivo: o objetivo desse estudo é realizar uma revisão de literatura em relação às propriedades físico- -químicas e biológicas do Biodentine, seu emprego na Endodontia e discutir, com base nas evidências científicas encontradas na literatura, se esse material poderá ser um substituto ao MTA. Métodos: foi realizada uma busca na literatura na base de dados PubMed, usando os termos em inglês: Biodentine, calcium silicate, MTA, properties, setting time, radiopacity, solubility, physicochemical properties, porosity, hydration, biocompatibility, bioactivity, microhardness, compressive strength, bond strength, irrigants, furcal perforation, retrograde filling material, revitalization, revascularization, endodontics, apexification. Cinquenta artigos foram incluídos. Resultados: os artigos revisados sugerem que o Biodentine tem características favoráveis e que tem alcançado resultados promissores em relação ao MTA. Conclusão: o Biodentine pode ser considerado um eventual substituto ao MTA.

Evaluation of pH and calcium ion release of new root-end filling materials

2009 ◽  
Vol 108 (1) ◽  
pp. 135-139 ◽  
Author(s):  
Bruno Carvalho de Vasconcelos ◽  
Ricardo Affonso Bernardes ◽  
Suyane M. Luna Cruz ◽  
Marco Antonio Húngaro Duarte ◽  
Pedro de Magalhães Padilha ◽  
...  
Keyword(s):  
Calcium Ion ◽  
Ion Release ◽  
Filling Materials

scholarly journals Examination of Calcium Silicate Cements with Low-Viscosity Methyl Cellulose or Hydroxypropyl Cellulose Additive

2016 ◽  
Vol 2016 ◽  
pp. 1-6 ◽  
Author(s):  
Toshiaki Baba ◽  
Yasuhisa Tsujimoto
Keyword(s):  
Calcium Ion ◽  
Calcium Silicate ◽  
Zirconium Oxide ◽  
Setting Time ◽  
Mineral Trioxide Aggregate ◽  
Methyl Cellulose ◽  
Hydroxypropyl Cellulose ◽  
Ion Release ◽  
Low Viscosity ◽  
Calcium Silicate Cements

The purpose of this study was to improve the operability of calcium silicate cements (CSCs) such as mineral trioxide aggregate (MTA) cement. The flow, working time, and setting time of CSCs with different compositions containing low-viscosity methyl cellulose (MC) or hydroxypropyl cellulose (HPC) additive were examined according to ISO 6876-2012; calcium ion release analysis was also conducted. MTA and low-heat Portland cement (LPC) including 20% fine particle zirconium oxide (ZO group), LPC including zirconium oxide and 2 wt% low-viscosity MC (MC group), and HPC (HPC group) were tested. MC and HPC groups exhibited significantly higher flow values and setting times than other groups (p<0.05). Additionally, flow values of these groups were higher than the ISO 6876-2012 reference values; furthermore, working times were over 10 min. Calcium ion release was retarded with ZO, MC, and HPC groups compared with MTA. The concentration of calcium ions was decreased by the addition of the MC or HPC group compared with the ZO group. When low-viscosity MC or HPC was added, the composition of CSCs changed, thus fulfilling the requirements for use as root canal sealer. Calcium ion release by CSCs was affected by changing the CSC composition via the addition of MC or HPC.

scholarly journals Experimental Resin-Based Monoblock Endodontic Obturation System

2019 ◽  
Vol 2019 ◽  
pp. 1-6
Author(s):  
Thiago Machado Pereira ◽  
Evandro Piva ◽  
Carlos Enrique Cuevas-Suárez ◽  
Luiz Evaristo Ricci Volpato ◽  
Manoel dos Santos da Silva Neto ◽  
...  
Keyword(s):  
Film Thickness ◽  
Dimensional Stability ◽  
Calcium Ion ◽  
Experimental System ◽  
Cohesive Strength ◽  
National Standards ◽  
Ion Release ◽  
Gutta Percha ◽  
Ah Plus

Objective. The aim of the present study was to characterize a novel resin-based monoblock endodontic obturation system consisting of a polymeric cone and a resin-based endodontic sealer. Methods. The preliminary tests performed for the experimental cone were as follows: cohesive strength, dimensional stability, standardization of the diameter and taper, calcium ion release, and radiopacity, for the characterization of the experimental sealer, film thickness and flow tests were performed. Tests were performed according to the American National Standards Institute/American Dental Association (ANSI/ADA) Standards Nos. 57 and 78. The experimental cone was compared to gutta-percha, whereas the experimental sealer was compared to AH Plus. Data were analyzed by Student’s t-test (α = 0.05). Results. The experimental cone had superior values for cohesive strength and dimensional stability compared to gutta-percha. Regarding calcium ion release, the experimental system continued to release calcium ions after 30 days. Film thickness was similar for both endodontic sealers; conversely, the experimental resin-based sealer achieved higher values for flow compared to AH Plus. Conclusion. The experimental resin-based monoblock obturation system fully met the requirements of the ANSI/ADA Standard No. 78 and the ANSI/ADA Standard No. 57, except for radiopacity. Considering this, further studies are still needed to evaluate other radiopacifiers and the effect of their incorporation on the physicochemical properties of this novel resin-based monoblock endodontic obturation system.

Variation of the bone forming ability with the physicochemical properties of calcium phosphate bone substitutes

2018 ◽  
Vol 6 (1) ◽  
pp. 136-145 ◽  
Author(s):  
Rongquan Duan ◽  
Davide Barbieri ◽  
Xiaoman Luo ◽  
Jie Weng ◽  
Chongyun Bao ◽  
...  
Keyword(s):  
Calcium Phosphate ◽  
Physicochemical Properties ◽  
Surface Structure ◽  
Protein Adsorption ◽  
Calcium Ion ◽  
Bone Substitutes ◽  
Ion Release ◽  
Adsorption Surface

The submicron-scaled surface structure triggers osteoinduction in CaPs via mechanotransduction, rather than protein adsorption, surface mineralization and calcium ion release.

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