Optimization in strength-ductility of heterogeneous Mg-13Gd alloy via small extrusion ratio combined with pre-aging

Author(s):  
Shuaishuai Liu ◽  
Jingjing Zhang ◽  
Hong Yang ◽  
Xiang Chen ◽  
Guangsheng Huang ◽  
...  
Keyword(s):  
Author(s):  
S. Wisutmethangoon ◽  
T. F. Kelly ◽  
J.E. Flinn

Vacancies are introduced into the crystal phase during quenching of rapid solidified materials. Cavity formation occurs because of the coalescence of the vacancies into a cluster. However, because of the high mobility of vacancies at high temperature, most of them will diffuse back into the liquid phase, and some will be lost to defects such as dislocations. Oxygen is known to stabilize cavities by decreasing the surface energy through a chemisorption process. These stabilized cavities, furthermore, act as effective nucleation sites for precipitates to form during aging. Four different types of powders with different oxygen contents were prepared by gas atomization processing. The atomized powders were then consolidated by hot extrusion at 900 °C with an extrusion ratio 10,5:1. After consolidation, specimens were heat treated at 1000 °C for 1 hr followed by water quenching. Finally, the specimens were aged at 600 °C for about 800 hrs. TEM samples were prepared from the gripends of tensile specimens of both unaged and aged alloys.


2011 ◽  
Vol 291-294 ◽  
pp. 1082-1086
Author(s):  
Yao Jin Wu ◽  
Zhi Ming Zhang ◽  
Bao Cheng Li ◽  
Bao Hong Zhang ◽  
Jian Min Yu ◽  
...  

In the present research, the influences of different extrusion ratios (15, 30, 45, 60, and 75) and extrusion temperature (300°C, 330°C, 360°C, 390°C, 420°C) on the mechanical properties and microstructure changes of AZ80 magnesium alloy have been investigated through tensile test and via ZEISS digital metallographic microscope observation. Research indicates that the alloy’s plasticity gradually decreases as the temperature increases, and that the alloy’s tensile strength varies with the extrusion ratio. At 330°C, the alloy’s particle grain is small and a small amount of black hard and brittle second-phase β (Mg17Al12) are precipitated uniformly along the grain boundary causing the gradual increase of the alloy’s tensile strength. When the extrusion temperature is up to 390°C, the grain size increases significantly, but the second phase precipitation along grain boundaries transforms into continuous and uniform-distribution precipitation within the grain. In this case, when the extrusion ratio is 60, the alloy’s tensile strength reaches its peak 390 Mpa. As the extrusion temperature increases, inhomogeneous precipitation of the second-phase along grain boundaries increases, causing the decrease of the alloy’s strength. At the same temperature, both the tensile strength and plasticity increases firstly and then decreases as extrusion ratio increases. With the gradual increase of the refinement grain, the dispersed precipitates increase and the alloy’s tensile strength and plasticity reach their peaks when the extrusion temperature is 390°C. As the grain grows, the second phase becomes inhomogeneous distribution, and the alloy’s strength and plasticity gradually decrease.


1997 ◽  
Author(s):  
Joseph P. Domblesky ◽  
Frank Kraft ◽  
Matt Guzowski ◽  
Charles Downing

2010 ◽  
Vol 139-141 ◽  
pp. 180-184
Author(s):  
Yong Xue ◽  
Zhi Min Zhang ◽  
Li Hui Lang

In the present research, the influences of different extrusion ratios (15, 30, 45, 60, and 75) and extrusion temperatures (300°C, 330°C, 360°C, 390°C, 420°C) on the mechanical properties and microstructure of homogenized AZ80 alloy have been investigated through the tensile tests and via metallographic microscope observation. The results show that the alloy’s grain is small and small amounts of black hard and brittle second-phase β (Mg17Al12) are precipitated uniformly along the grain boundary causing the gradual increase of the alloy’s tensile strength at 330°C. When the extrusion temperature is up to 390°C, the grain size increases significantly, but the second phase precipitation along grain boundaries transforms into continuous and uniform-distribution precipitation within the grain. In this case, when the extrusion ratio is 60, the alloy’s tensile strength reaches its peak 390Mpa. As the extrusion temperature increases, inhomogeneous precipitation of the second-phase along grain boundaries increases, causing the decrease of the alloy’s strength. At the same temperature, the tensile strength increases firstly and then decreases as extrusion ratio increases. With the gradual increase of the refinement grain, the dispersed precipitates increase and the alloy’s tensile strength and plasticity reach their peaks when the extrusion temperature is 390°C. As the grain grows, the second phase becomes inhomogeneous distribution, and the alloy’s strength and plasticity gradually decrease.


1975 ◽  
Vol 97 (1) ◽  
pp. 25-31 ◽  
Author(s):  
K. M. Kulkarni ◽  
J. A. Schey

Hydrostatic extrusion of annealed 1100 aluminum was investigated experimentally at ambient temperature. The principal variables studied were lubricant viscosity which was varied from less than 100 to over 76,000 SUS at 100 deg F and the diametral clearance between the follower block and the extrusion cylinder which ranged from 0.0005 to 0.0030 in. for the 1.026 in. dia. cylinder. The specimen diameter was 0.97 or 1.00 in. corresponding to an extrusion ratio of 4.75 or 5.00, respectively. The included die angle was either 60 deg or 90 deg. The results show that with a proper combination of the lubricant viscosity and the follower block clearance, hydrostatic extrusion can be accomplished without the necessity of any sealing of the container on the follower block side. The optimum clearance for minimum breakthrough pressure increases as the lubricant viscosity increases. The extrusion force increases with die angle. The paper discusses the various factors that affect the magnitude of the breakthrough pressure and the occasional uneven bamboo-type appearance of the surface. Processing conditions must be selected carefully since the lowest extrusion force does not necessarily lead to a product with the best surface finish.


2006 ◽  
Vol 503-504 ◽  
pp. 865-870 ◽  
Author(s):  
Yongjun Chen ◽  
Qu Dong Wang ◽  
Jianguo Peng ◽  
Chun Quan Zhai

Experiments were conducted both to evaluate the potential for grain refinement, the subsequent mechanical properties at room temperature in samples of AZ31 Mg alloy and also to investigate the relationship between one-step and two-step high ratio extrusion (HRE). The one-step HRE was undertaken using a high extrusion ratio of 70:1 at 250, 300 and 350°C. And the two-step HRE was conducted with an extrusion ratio of 7 for the first step at 250, 300 and 350°C, followed by a second-step extrusion with an extrusion ratio of 10 at 250, 300 and 350°C. The initial grain size in the AZ31 ingot was 100μm and that after one-step HRE became similar to 5μm, after two-step HRE at 250, 300 and 350°C were 2, 4, 7μm, respectively, resulting in superior mechanical properties at ambient temperature. The microstructure of two-step HRE was finer and uniformer than that of one-step HRE and the strength of one-step and two-step HRE were similar, moreover, the elongation of one-step HRE was improved markedly than that of two-step HRE. Dynamic recrystallization and adjacent grain broking during HRE is introduced to explain the effects of one-step and two-step HRE on the microstructure and mechanical properties of AZ31 Mg alloy. The current results imply that the simple HRE method might be a feasible processing method for industry applications, and the multiply steps extrusion are effective to fabricate high strength of fine grained hcp metals.


1972 ◽  
Vol 94 (4) ◽  
pp. 1225-1230 ◽  
Author(s):  
A. H. Shabaik

A procedure for smoothing the experimental values of the flow function ψ in axisymmetric extrusion through curved boundaries was developed. The analysis was applied to a 45 deg conical die with a 6:1 extrusion ratio and a circular arc of 0.33-in. radius and 0.033-in. land at the exit section. An analytical expression of ψ in terms of r and z was obtained and used in the calculation of velocity and strain rate components in axisymmetric extrusion of a superplastic of the eutectic of lead–tin. The stress components were obtained from the known values of the strain rates by considering equilibrium and plasticity equations and material properties.


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