An X-ray diffraction (XRD) and Fourier transform infrared spectroscopic (FT-IR) investigation of the long-term effect on the solidification/stabilization (S/S) of arsenic(V) in Portland cement type-V

Polyaniline (PANI) is synthesized by chemical oxidative polymerization method. The, characterization were made using XRD (X-ray diffraction), FT-IR (Fourier transform spectroscopy), UV -vis (ultra-violet visible spectrophotometer) technique which confirms the synthesis of the Polyaniline. The surface morphology of Polyaniline was studied with scanning electron microscope (SEM).

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Synthesis of Triethynylborazine-Polyhydromethylsiloxane Copolymers and its Ceramization

Advanced Materials Research ◽

10.4028/www.scientific.net/amr.774-776.629 ◽

2013 ◽

Vol 774-776 ◽

pp. 629-633

Author(s):

Ji Feng Jiang ◽

Kang Kang Guo ◽

Ya Ping Zhu ◽

Fan Wang ◽

Hui Min Qi

Keyword(s):

Electron Microscopy ◽

Scanning Electron Microscopy ◽

Nuclear Magnetic Resonance ◽

Fourier Transform ◽

Thermogravimetric Analysis ◽

X Ray Diffraction ◽

Hydrosilylation Reaction ◽

X Ray ◽

Ft Ir ◽

Scanning Electron

Triethynylborazine-polyhydromethylsiloxane copolymers (TEB-PHMSs) were prepared through hydrosilylation reaction between -C≡CH attached to boron and ≡Si-H. The structures of TEB-PHMSs were characterized by Fourier transform Infrared (FT-IR) and Nuclear Magnetic Resonance (NMR) spectroscopy. Their cure behavior were examined by Differential Scanning Calorimeter (DSC) and FT-IR, and then thermostability and ceramization of cured TEB-PHMS were investigated by Thermogravimetric analysis (TGA), pyrolysis-GC-MS, X-ray diffraction (XRD) and Scanning Electron Microscopy (SEM). The results indicated that TEB-PHMSs could be cured and converted into an outstanding thermostable SiBCN ceramics.

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Dissolution and Regeneration of Reed Leaf Fibers in Imidazole-Based Ionic Liquids

Advanced Materials Research ◽

10.4028/www.scientific.net/amr.652-654.1539 ◽

2013 ◽

Vol 652-654 ◽

pp. 1539-1542

Author(s):

Hou Jie Zhao ◽

Chun Yan Wei ◽

Yong Zhu Cui ◽

Li Hua Lv ◽

Xiao Wang

Keyword(s):

Fourier Transform ◽

Ionic Liquids ◽

Infrared Spectroscopy ◽

Chloride Solution ◽

X Ray Diffraction ◽

Cellulose I ◽

X Ray ◽

High Temperature And Pressure ◽

Ft Ir ◽

Temperature And Pressure

In this paper, regeneration of reed leaf fibers that have been degummed pretreatment in high temperature and pressure dissolved in 1-butyl-3-methylimidazolium chloride ionic liquids was studied. The samples containing 5% or 10%(wt/wt)reed leaf fibers in the ionic liquids, at 90°C for 7h.The dissolution process was viewed by polarizing microscope. Fourier-transform infrared spectroscopy(FT-IR) and X-ray diffraction were used to visualize the crystalline of reed leaf fiber transformed completely from cellulose I to cellulose Ⅱ after regenerated directly from 1-butyl-3-methylimidazolium chloride solution.

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SINTESIS DAN KARAKTERISASI N DOPED TiO2 (N/TiO2) NANOTUBE SERTA UJI AKTIVITAS FOTOKATALISIS TERHADAP ZAT WARNA RHODAMIN B

Jurnal Teknologi dan Manajemen ◽

10.52330/jtm.v19i1.21 ◽

2021 ◽

Vol 19 (1) ◽

pp. 27-32

Author(s):

Ida Nur Apriani Apriani ◽

Jarnuzi Gunlazuardi

Keyword(s):

Fourier Transform ◽

Tio2 Nanotube ◽

X Ray Diffraction ◽

Linear Sweep ◽

Doped Tio2 ◽

X Ray ◽

Infra Red ◽

Ft Ir ◽

Rhodamin B ◽

Scanning Electron

Telah dilakukan sintesis fotokatalis N/TiO2 bermofologi nanotube dengan metode anodisasi menggunakan ammonium nitrat (NH4NO3) sebagai sumber dopan pada berbagai variasi konsentrasi (0,5M , 1M, 2M), dilanjutkan dengan kalisinasi pada suhu 4500C selama 2 jam untuk mendapatkan fasa kristal anatase. Karakterisasi dilakukan menggunakan Scanning Electron Miscroscopy (SEM), Fourier Transform Infra Red (FT-IR), X-ray Diffraction (XRD), dan DRS (Diffused Reflectant Spectrometry) UV-Vis. Pengujian Linear Sweep Voltametri dan Multi Pulse Anperiometri pada fotokatalis N/TiO2 telah berhasil diterapkan untuk degradasi senyawa Rhodamin B menggunakan sinar UV maupun sinar tampak. Aplikasi dari uji fotoelektrokatalisis menggunakan sinar tampak untuk N/TiO2-NT memberikan hasil eliminasi sebesar 47,86%, sedangkan bila menggunakan TiO2 nanotube tanpa dopan eleminasi hanya sebesar 25,49%. Hal ini menunjukkan bahwa proses doping yang dilakukan telah berhasil menyisipkan nitrogen kedalam matrik TiO2 nanotube dan memperbaiki kinerja fotokatalisis nya di daerah sinar tampak.

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Ciprofloxacin Based on Carrier Double Layered Hydroxide Nano-particles of Fe+3/Fe+2, Fe+3/Ni+2, Al+3/Fe+2, and Al+3/Ni+2 Ions

International Journal of Drug Delivery Technology ◽

10.25258/ijddt.v10i1.26 ◽

2020 ◽

Vol 10 (01) ◽

pp. 119-126

Author(s):

Noor M. Mohammed ◽

Farah AH. Kadhim ◽

Aseel A. Hammood ◽

Ashour H. Dawood

Keyword(s):

Fourier Transform ◽

Electron Microscope ◽

Nano Particles ◽

X Ray Diffraction ◽

X Ray ◽

Atomic Force ◽

Ft Ir ◽

Double Layered Hydroxide ◽

Scanning Electron ◽

Ft Ir Spectroscopy

The double-layered hydroxide nano-particles compounds with ciprofloxacin drug were carried out by preparation of the double layered hydroxide (DLH) of M+3/M+2 ions for selective ions. The ciprofloxacin drug was inserted between them. The resulted compounds were characterized by X-Ray diffraction (XRD), scanning electron microscope (SEM), atomic force microscope (AFM), and Fourier Transform Infrared (FT-IR) spectroscopy; the antibacterial studied done by using the gram (+) and gram (-) pigments.

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Influence of Organoclay on the Physical Properties of Polyethylene Nanocomposites

Materials Science Forum ◽

10.4028/www.scientific.net/msf.530-531.709 ◽

2006 ◽

Vol 530-531 ◽

pp. 709-714 ◽

Cited By ~ 5

Author(s):

Edcleide Maria Araújo ◽

Amanda D. de Oliveira ◽

Renata Barbosa ◽

Tomás Jefférson Alves de Mélo

Keyword(s):

Mechanical Properties ◽

Fourier Transform ◽

Infrared Spectroscopy ◽

Quaternary Ammonium Salts ◽

Ammonium Salts ◽

Clay Nanocomposites ◽

X Ray Diffraction ◽

Polyethylene Matrix ◽

X Ray ◽

Ft Ir

In this work, polyethylene/montmorillonite clay nanocomposites were produced by melt intercalation. The clays were treated with quaternary ammonium salts and then treated and untreated clays were introduced in polyethylene. The clays were characterized by X-Ray Diffraction (XRD) and Fourier Transform Infrared Spectroscopy (FT-IR). The nanocomposites were characterized by mechanical and flammability properties. The results showed that the mechanical properties were improved by introduction of organoclay in polyethylene matrix. By adding only 3wt% montmorillonite, the burning rate of the nanocomposites was reduced by 17% in relation to PE matrix.

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Comparison of FT-IR, Thermal Analysis and XRD for Determination of Products of Cement Hydration

Advanced Materials Research ◽

10.4028/www.scientific.net/amr.168-170.518 ◽

2010 ◽

Vol 168-170 ◽

pp. 518-522 ◽

Cited By ~ 6

Author(s):

Zhi Hua Ou ◽

Bao Guo Ma ◽

Shou Wei Jian

Keyword(s):

Thermal Analysis ◽

Fourier Transform ◽

Cement Hydration ◽

Hydration Products ◽

X Ray Diffraction ◽

Cement Pastes ◽

X Ray ◽

Degree Of Hydration ◽

Ft Ir

Fourier Transform Infrared Spectroscopy (FT-IR), thermal analysis and X-Ray Diffraction (XRD) are commonly performed to study the hydration products in cement pastes. The three methods were compared in this frame to detect products of cement hydration at different ages, especially at early ages (before 24h ages). The results indicate from the present experiment that CH (Calcium hydroxide) can be detected by three methods at all ages; C-S-H can be distinguished by FT-IR at all ages; ettringite may be detected by FT-IR before 24h ages and by XRD at all ages; and monosulphate can be detected by FT-IR before 24h ages. The process of cement hydration, characterized by formation and development of some hydration products, can be clearly observed by three methods. FT-IR is suggested for detecting the major hydration products before 24h ages, FT-IR and XRD are suggested for detecting the major hydration products after 24h ages, and thermal analysis is suggested for analyzing the degree of hydration quantitatively.

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