Vacuum Arc Cathode Spot Characterization on Graphite Materials Using Field Emission Gun Scanning Electron Microscopy (FEGSEM)

1997 ◽  
Vol 3 (S2) ◽  
pp. 1225-1226
Author(s):  
M. Kandah ◽  
J.-L. Meunier ◽  
R. Gauvin

Vacuum arcs on graphite cathodes are currently used as sources of carbon ions for the production of diamond-like films in the arc ion-plating (AIP) deposition process. Emission from these cathode sources is concentrated in very localized “cathode spots” having typically 10 (i.m in diameter for graphite cathodes. These spots carry the totality of the arc current, the remaining of the surface being unaffected by the discharge. For electron emission falling in the thermo-field emission mode, extremely high current densities up to 108 -109 Am-2 are induced generating a high localized heat flux to the surface during the spot lifetime. On metallic electrodes, this strong heat flux generates localized surface melting during the microsecond scale spot lifetime. High localized plasma pressures (>10 Atm in the case of copper) were found to exist in the cathode spot volume, leading to the co-emission of micro-droplets of the liquid metal along with the ion beam.

1999 ◽  
Vol 593 ◽  
Author(s):  
W.I. Milne ◽  
B.S. Satyanarayana ◽  
J. Robertson

ABSTRACTCarbon films with variable sp3/sp2 bonding ratio can be deposited on a variety of substrates at room temperature, using the cathodic vacuum arc deposition process. The variation in their surface morphology as a function of He and N2partial pressure during growth have been investigated and it has been shown that the morphology of the films can be varied from the mirror like smooth tetrahedrally bonded carbon (ta-C) films through nanocluster to fibrous type carbon. This paper reviews the work carried out on Field Emission from these various carbon films. Threshold fields as low as 1 V/μm for emission current densities of 1 μA/cm2 and emission site densities of up to 104 -105/cm2 have been obtained.


1997 ◽  
Vol 471 ◽  
Author(s):  
W. I. Milne ◽  
J. Robertson ◽  
B. S. Satyanarayanan ◽  
A. Hart

ABSTRACTA series of tetrahedrally bonded carbon (ta-C) films have been produced using a Filtered Cathodic Vacuum Arc System. The threshold field and current densities achievable have been investigated as a function of sp3/sp2 bonding ratio and nitrogen content. Typical undoped ta-C films have a threshold field of 15–20V/μm and optimally nitrogen doped films exhibit threshold fields as low as ∼ 5 V/μm. Current densities of typically 10-4 A/cm2 at an applied field of 20V/micron were also obtained.


2017 ◽  
Vol 4 (1) ◽  
pp. 99-103
Author(s):  
B. Tezenas du Montcel ◽  
P. Chapelle ◽  
A. Jardy ◽  
C. Creusot

The distribution of cathode spots in a CuCr25 vacuum arc controlled by an axial magnetic field and ignited on the lateral surface of the cathode is investigated for long gap distances, from the processing of high-speed video images. The processing method includes also estimating the current carried by a single spot and reconstructing the distribution of the current density at the cathode. Various distributions depending partly on the arc current are described.


Author(s):  
G. V. Markov ◽  
A. T. Volochko ◽  
V. G. Zaleski ◽  
N. Yu. Melnik

The simple relation to estimate the cathode spot radius of a vacuum arc of pure metals is obtained. On its basis, is established between the cathode spot radius and the size of droplets generated by the cathode spot a correlation. This enables to find ways to reduce droplets in the plasma flow, which forms coatings by the vacuum electric arc method. The paper presents the results of experimental study of the droplet sizes depending on the vacuum arc current iд. The size and amount of the droplets on an area of 1 mm2 of the coating surface are determined using the ImageSP program. As the initial data, the microstructures of the coatings are used with an increase of: ç100, ç200, ç500, ç1000, ç1500. The droplets have been generated by a cathode spot of a vacuum arc for the alloy of the composition, at.%: 68Al–8Cr–4Nb–20Si. It is established that the number of droplets with a diameter of < 2 μm is generated most of all, and the number of droplets with a diameter > 10 μm is generated least of all. The number of generated droplets with a diameter from 2 to 10 μm slightly depends on the arc current iд. It is noted that the diameter of the alloy droplet is smaller than the diameter of the droplets generated by the cathode spot on its components due to the fact that the radius of the cathode spot on the alloy is smaller than the radius of the cathode spot on its pure components.


1998 ◽  
Vol 509 ◽  
Author(s):  
Dihu Chen ◽  
S. P. Wong ◽  
W.Y. Cheung ◽  
E.Z. Luo ◽  
W. Wu ◽  
...  

AbstractPlanar SiC/Si heterostructures were formed by high dose carbon implantation using a metal vapor vacuum arc ion source. The variations of the field emission properties with the implant dose and annealing conditions were studied. A remarkably low turn-on field of IV/μm was observed from a sample implanted at 35 keV to a dose of 1.0×1018 cm−2 with subsequent annealing in nitrogen at 1200°C for 2h. The chemical composition depth profiles were determined from x-ray photoelectron spectroscopy and the surface morphology was observed by atomic force microscopy. The formation of a thin surface stoichiometric SiC layer and the formation of densely distributed small protrusions on the surface are believed to be the two factors responsible for the efficient electron field emission.


Author(s):  
W.R. Bottoms ◽  
G.B. Haydon

There is great interest in improving the brightness of electron sources and therefore the ability of electron optical instrumentation to probe the properties of materials. Extensive work by Dr. Crew and others has provided extremely high brightness sources for certain kinds of analytical problems but which pose serious difficulties in other problems. These sources cannot survive in conventional system vacuums. If one wishes to gather information from the other signal channels activated by electron beam bombardment it is necessary to provide sufficient current to allow an acceptable signal-to-noise ratio. It is possible through careful design to provide a high brightness field emission source which has the capability of providing high currents as well as high current densities to a specimen. In this paper we describe an electrode to provide long-lived stable current in field emission sources.The source geometry was based upon the results of extensive computer modeling. The design attempted to maximize the total current available at a specimen.


Author(s):  
L. Wan ◽  
R. F. Egerton

INTRODUCTION Recently, a new compound carbon nitride (CNx) has captured the attention of materials scientists, resulting from the prediction of a metastable crystal structure β-C3N4. Calculations showed that the mechanical properties of β-C3N4 are close to those of diamond. Various methods, including high pressure synthesis, ion beam deposition, chemical vapor deposition, plasma enhanced evaporation, and reactive sputtering, have been used in an attempt to make this compound. In this paper, we present the results of electron energy loss spectroscopy (EELS) analysis of composition and bonding structure of CNX films deposited by two different methods.SPECIMEN PREPARATION Specimens were prepared by arc-discharge evaporation and reactive sputtering. The apparatus for evaporation is similar to the traditional setup of vacuum arc-discharge evaporation, but working in a 0.05 torr ambient of nitrogen or ammonia. A bias was applied between the carbon source and the substrate in order to generate more ions and electrons and change their energy. During deposition, this bias causes a secondary discharge between the source and the substrate.


1978 ◽  
Vol 125 (8) ◽  
pp. 665-706 ◽  
Author(s):  
G.A. Lyubimov ◽  
V.I. Rakhovskii
Keyword(s):  

2019 ◽  
Vol 139 (5) ◽  
pp. 302-308 ◽  
Author(s):  
Shinji Yamamoto ◽  
Soshi Iwata ◽  
Toru Iwao ◽  
Yoshiyasu Ehara

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