Thermal Stability of Quasi-1D NbS3 Nanoribbons and Their Transformation to 2D NbS2: Insights from in Situ Electron Microscopy and Spectroscopy

2021 ◽  
Author(s):  
Eric V. Formo ◽  
Jordan A. Hachtel ◽  
Yassamin Ghafouri ◽  
Matthew A. Bloodgood ◽  
Tina T. Salguero
Keyword(s):  
Electron Microscopy ◽  
Thermal Stability ◽  
In Situ Electron Microscopy ◽  
Thermal Stability Of

Grain Growth Behaviour Of Nanocrystalline Nickel

1991 ◽  
Vol 238 ◽  
Author(s):  
A. M. El-Sherik ◽  
K. Boylan ◽  
U. Erb ◽  
G. Palumbo ◽  
K. T. Aust
Keyword(s):  
Electron Microscopy ◽  
Thermal Stability ◽  
Grain Size ◽  
Grain Boundary ◽  
Grain Growth ◽  
Thermal Stabilization ◽  
Growth Behaviour ◽  
In Situ Electron Microscopy ◽  
Thermal Stability Of

ABSTRACTThe thermal stability of electrodeposited nanocrystalline Ni-1.2%P and Ni-0.12%S alloys is evaluated by in-situ electron microscopy studies. Isothermal grain size versus annealing time curves at 573K and 623K show an unexpected thermal stabilization in form of a transition from rapid initial grain growth to negligible grain growth. This behaviour is discussed in terms of the various grain boundary drag mechanisms which may be operative in these alloys.

Thermal stability of laser-induced modified volumes in Si as studied by in situ and ex situ heating experiments

Microscopy ◽  
2018 ◽  
Vol 67 (2) ◽  
pp. 112-120
Author(s):  
Hiroyasu Saka ◽  
Hiroyuki Iwata ◽  
Daisuke Kawaguchi
Keyword(s):  
Electron Microscopy ◽  
Thermal Stability ◽  
Transmission Electron Microscopy ◽  
Laser Beam ◽  
Ex Situ ◽  
Dislocation Theory ◽  
Tail Region ◽  
Transmission Electron ◽  
Thermal Stability Of

Abstract Radiation of a permeable laser beam into Si induces considerable modification of structures. Thermal stability of the laser-induced modified volumes (LIMV’s) was studied comprehensively by means of in situ and ex situ heating experiments using transmission electron microscopy. The behavior in the tail region of a LIMV can be understood by dislocation theory, while that of a void formed at the very focus of a laser beam cannot be understood easily.

Effects of Polyaniline Doped by Different Acids on Thermal Stability of Epoxy Resin

2010 ◽  
Vol 160-162 ◽  
pp. 1405-1408 ◽  
Author(s):  
Qing Ming Jia ◽  
Shao Yun Shan ◽  
Li Hong Jiang ◽  
Ya Ming Wang
Keyword(s):  
Electron Microscopy ◽  
Thermal Stability ◽  
Scanning Electron Microscopy ◽  
Sulfuric Acid ◽  
Epoxy Resin ◽  
Inert Atmosphere ◽  
Pani Nanofibers ◽  
Thermal Stability Of ◽  
Scanning Electron

Polyaniline(PANI) nanofibers were firstly prepared by rapid mixture method, EP/PANI nanocomposite was obtained by in-situ adding the PANI nanofibers to epoxy resin(EP). Scanning electron microscopy(SEM) proves that the type of doped acids has a little effect on the morphologies of PANI, and the PANI doped by different acids present nanofiber structures with the diameter of about 50 nm. The thermal behaviour of EP/PANI nanocomposites were investigated in detail by using a dynamic rate mode of thermogravimetric analyser (TGA) in inert atmosphere, and the results show that the PANI nanofibers obviously improve thermal stability of pure EP. Compared with EP/PANI doped by nitric acid or sulfuric acid, EP/PANI doped by phosphoric acid has best thermal stability.

scholarly journals Thermal stability of CsPbBr3 perovskite as revealed by in situ transmission electron microscopy

APL Materials ◽  
2019 ◽  
Vol 7 (7) ◽  
pp. 071110 ◽  
Author(s):  
Chao Zhang ◽  
Joseph F. S. Fernando ◽  
Konstantin L. Firestein ◽  
Joel E. von Treifeldt ◽  
Dumindu Siriwardena ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Thermal Stability ◽  
Transmission Electron Microscopy ◽  
Transmission Electron ◽  
Thermal Stability Of

Synthesis, Characterization and Thermal Analysis of Rod-Shaped Polyaniline-Barium Ferrites Nanocomposites

2010 ◽  
Vol 150-151 ◽  
pp. 386-390
Author(s):  
Yuan Xun Li ◽  
Ying Li Liu ◽  
Huai Wu Zhang ◽  
Wei Wei Ling
Keyword(s):  
Electron Microscopy ◽  
Thermal Stability ◽  
Barium Ferrite ◽  
In Situ Polymerization ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Barium Ferrites ◽  
Thermal Stability Of

The rod-shaped polyaniline (PANI)-barium ferrite nanocomposites were synthesized by in situ polymerization of aniline in the presence of BaFe12O19 nanoparticles with diameters of 60-80 nm. The composites obtained were characterized by infrared spectra (IR), X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The thermal stability and the composition of the composites were investigated by TG-DTG analysis. The results indicate that the thermal stability of the composites is higher than that of the pure PANI which can be attributed to the interactions existed between PANI chains and ferrite particles.

scholarly journals Properties of carbon black-PEDOT composite prepared via in-situ chemical oxidative polymerization

e-Polymers ◽  
2019 ◽  
Vol 19 (1) ◽  
pp. 61-69 ◽  
Author(s):  
Yong Xie ◽  
Shi-Hao Zhang ◽  
Hai-Yun Jiang ◽  
Hui Zeng ◽  
Ruo-Mei Wu ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Thermal Stability ◽  
Carbon Black ◽  
In Situ Polymerization ◽  
Oxidative Polymerization ◽  
Gravimetric Analysis ◽  
Transmission Electron ◽  
The One ◽  
Thermal Stability Of

AbstractA new conductive composite composed of nanoscale carbon black (CB) and poly(3,4-ethylenedioxythiophene) (PEDOT) was prepared by a simple in-situ polymerization. The morphology of the composite was characterized by scanning electron microscopy and transmission electron microscopy. The structure and thermal stability were examined by Fourier transform infrared spectroscopy and thermal gravimetric analysis, respectively. The results indicated that the addition of CB improved the agglomerated state of PEDOT. On the one hand, CB effectively hindered the agglomeration of PEDOT during the polymerization. Thus, the obtained CB-PEDOT composite dispersed well in solution, which can facilitate the reprocessing of CB-PEDOT. On the other hand, CB covered most of the surface of PEDOT, which enhanced the electrical conductivity of CB-PEDOT. Furthermore, the interfacial interaction between CB and PEDOT improved the thermal stability of CB-PEDOT. The findings of this research suggest that CB can replace polyelectrolyte poly(styrenesulfonic acid) (PSS) to achieve reprocessable materials for certain applications.

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