Little Adjustments Significantly Simplify the Gram-Scale Synthesis of High-Quality Iron Oxide Nanocubes

Langmuir ◽  
2021 ◽  
Author(s):  
Michael Kampferbeck ◽  
Lea R. Klauke ◽  
Horst Weller ◽  
Tobias Vossmeyer
Keyword(s):  
2020 ◽  
Vol 3 (9) ◽  
pp. 5699-5707
Author(s):  
Katsunori Tamura ◽  
Tatsuki Kunoh ◽  
Noriyuki Nagaoka ◽  
Jun Takada

Minerals ◽  
2019 ◽  
Vol 9 (2) ◽  
pp. 124 ◽  
Author(s):  
Arash Tohry ◽  
Reza Dehghan ◽  
Saeed Chehreh Chelgani ◽  
Jan Rosenkranz ◽  
Omid Rahmani

Demand for high-quality iron concentrate is significantly increasing around the world. Thus, the development of the techniques for a selective separation and rejection of typical associated minerals in the iron oxide ores, such as phosphorous minerals (mainly apatite group), is a high priority. Reverse anionic flotation by using sodium silicate (SS) as an iron oxide depressant is one of the techniques for iron ore processing. This investigation is going to present a synthesized reagent “sodium co-silicate (SCS)” for hematite depression through a reverse anionic flotation. The main hypothesis is the selective depression of hematite and, simultaneously, modification of the pulp pH by SCS. Various flotation experiments, including micro-flotation, and batch flotation of laboratory and industrial scales, were conducted in order to compare the depression selectivity of SS versus SCS. Outcomes of flotation tests at the different flotation scales demonstrated that hematite depression by SCS is around 3.3% higher than by SS. Based on flotation experiment outcomes, it was concluded that SCS can modify the pH of the process at ~9.5, and the plant reagents (including NaOH, Na2CO3, and SS gel) can be replaced by just SCS, which can also lead to a higher efficiency in the plant.


Nanoscale ◽  
2015 ◽  
Vol 7 (19) ◽  
pp. 8995-9003 ◽  
Author(s):  
T. Tsoufis ◽  
Z. Syrgiannis ◽  
N. Akhtar ◽  
M. Prato ◽  
F. Katsaros ◽  
...  

We report a facile approach for the in situ synthesis of very small iron oxide nanoparticles on the surface of high-quality graphene sheets.


2017 ◽  
Vol 5 (32) ◽  
pp. 16712-16721 ◽  
Author(s):  
P. Santhoshkumar ◽  
K. Prasanna ◽  
Yong Nam Jo ◽  
I. Nirmal Sivagami ◽  
Suk Hyun Kang ◽  
...  

In the present work, we have synthesized zero-dimensional (0D) and three-dimensional (3D) iron oxide (α-Fe2O3) sub-micron particles using a one-pot hydrothermal approach.


2013 ◽  
Vol 834-836 ◽  
pp. 3-7
Author(s):  
Yan Yan Guo ◽  
Hai Bo Wu ◽  
Ming Yu Li ◽  
Shuai Sun

We prepared the novel coralloid hierarchical structure of α-FeOOH composed of rod-shaped nanosheets by wet method using ammonia and ferrous sulfate. Through observation by Field emission scanning electron microscope (FESEM), the morphology and structure of α-FeOOH in the process of growth was presented. And the formation mechanism of this coralloid crystal α-FeOOH was studied, in order to provide important theoretical support for the preparation of high quality iron oxide yellow products.


2017 ◽  
Vol 59 (3) ◽  
Author(s):  
Román A. Hernández Hernández

<p>This paper presents a study of kaolin ore bleaching from the municipality of Agua Blanca of Iturbide, Hidalgo, México. This process was carried out using solutions of phosphoric acid as the leaching reagent for the iron dissolution process. It is well known that iron oxide is the major contaminant of clay minerals and silicate used in industry. These contents should be decreased, usually by .1%, to achieve a required whiteness index of 90% (ISO) or higher. The whitening improves its economic value, making it possible to use it as a high-quality raw material in industries such as ceramics and paper. For this purpose, we examined the effect of parameters such as the concentration of the leaching reagent (0.10 M,0.50 M,1 M, and3 M), temperature (298–373 K), and pH level (1, 2 and 3). The experimental results showed that the studied variables have a great influence over the ability to obtain an iron dissolution percentage of more than 98% after 2 hours and  373 K.</p>


Radiocarbon ◽  
2010 ◽  
Vol 52 (3) ◽  
pp. 1380-1393 ◽  
Author(s):  
Mojmír Němec ◽  
Lukas Wacker ◽  
Heinz Gäggeler

The reaction conditions for the graphitization of CO2 with hydrogen were optimized for a fast production of high-quality carbon samples for accelerator mass spectrometry (AMS) measurement. The iron catalyst in use is first oxidized by heating with air to remove possible carbon and other impurities and then after evacuation reduced back to iron with hydrogen in several flushing steps to remove any iron oxide. The optimum conditions for a fast graphitization reaction were experimentally determined by changing the reaction temperatures and the H2/CO2 ratio. The resulting graphite samples were measured by AMS to find the smallest isotopic changes (δ13C) at a minimum of molecular fragment formation (13CH current). The improvements are based on thermodynamic data and are explained with Baur-Glaessner diagrams.


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