An X-Ray Method for Studying Rapid Phase Changes in Steels at High Temperatures

When exposed to temperatures that are progressively and rapidly raised, large dimension fibre cement boards tend to crack. This occurrence is analysed and explained for a specific issue of asymmetric growth of a curvilinear crack in high temperatures. This phenomenon occurred while performing Single Burning Item (SBI) experiments at fire loads which are higher than those used in countries of the European Union, which better reflect fire events that may occur in high-rise buildings. In such conditions, fibre cement boards crack, allowing the fire to reach the thermal insulating material which then combusts, thereby helping to spread the conflagration to upper floors. This experiment investigated the temperatures at which fibre cement boards crack, and why. Thermal analysis methods and thermogravimetric experiments were conducted on the fibre boards, followed by X-ray phase analysis investigations. During this phase, X-ray structural analysis was performed while the fibre cement was exposed to temperatures of 1000 °C. The article also presents ongoing change results when heating only composite fibre-cement board materials; phase changes that take place in high temperatures are discussed.

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Phase Transformations in Ti-7w/oMo-3w/oMe Alloy

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100052584 ◽

1974 ◽

Vol 32 ◽

pp. 514-515

Author(s):

S. Fujishiro

Keyword(s):

Electron Microscopy ◽

Mechanical Properties ◽

Transmission Electron Microscopy ◽

Tensile Strength ◽

Mechanical Processing ◽

Ray Method ◽

X Ray ◽

Transmission Electron ◽

Water Quench ◽

Alpha Beta

The mechanical properties of three titanium alloys (Ti-7Mo-3Al, Ti-7Mo- 3Cu and Ti-7Mo-3Ta) were evaluated as function of: 1) Solutionizing in the beta field and aging, 2) Thermal Mechanical Processing in the beta field and aging, 3) Solutionizing in the alpha + beta field and aging. The samples were isothermally aged in the temperature range 300° to 700*C for 4 to 24 hours, followed by a water quench. Transmission electron microscopy and X-ray method were used to identify the phase formed. All three alloys solutionized at 1050°C (beta field) transformed to martensitic alpha (alpha prime) upon being water quenched. Despite this heavily strained alpha prime, which is characterized by microtwins the tensile strength of the as-quenched alloys is relatively low and the elongation is as high as 30%.

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The impact of point defects in n-type GaN layers on thermal decomposition of InGaN/GaN QWs

Scientific Reports ◽

10.1038/s41598-021-81017-w ◽

2021 ◽

Vol 11 (1) ◽

Author(s):

Mikolaj Grabowski ◽

Ewa Grzanka ◽

Szymon Grzanka ◽

Artur Lachowski ◽

Julita Smalc-Koziorowska ◽

...

Keyword(s):

Quantum Wells ◽

High Temperatures ◽

Point Defects ◽

X Ray Diffraction ◽

Helium Ions ◽

X Ray ◽

Sapphire Substrates ◽

Transmission Electron ◽

The Impact ◽

Ingan Quantum Wells

AbstractThe aim of this paper is to give an experimental evidence that point defects (most probably gallium vacancies) induce decomposition of InGaN quantum wells (QWs) at high temperatures. In the experiment performed, we implanted GaN:Si/sapphire substrates with helium ions in order to introduce a high density of point defects. Then, we grew InGaN QWs on such substrates at temperature of 730 °C, what caused elimination of most (but not all) of the implantation-induced point defects expanding the crystal lattice. The InGaN QWs were almost identical to those grown on unimplanted GaN substrates. In the next step of the experiment, we annealed samples grown on unimplanted and implanted GaN at temperatures of 900 °C, 920 °C and 940 °C for half an hour. The samples were examined using Photoluminescence, X-ray Diffraction and Transmission Electron Microscopy. We found out that the decomposition of InGaN QWs started at lower temperatures for the samples grown on the implanted GaN substrates what provides a strong experimental support that point defects play important role in InGaN decomposition at high temperatures.

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Specific Features of Material Recognition by the Multi-Energy X-Ray Method

Russian Journal of Nondestructive Testing ◽

10.1134/s1061830919040119 ◽

2019 ◽

Vol 55 (4) ◽

pp. 308-321 ◽

Cited By ~ 2

Author(s):

S. P. Osipov ◽

E. Yu. Usachev ◽

S. V. Chakhlov ◽

S. A. Shchetinkin ◽

O. S. Osipov

Keyword(s):

Ray Method ◽

X Ray ◽

Material Recognition

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Structural and Raman Vibrational Studies ofCeO2-Bi2O3Oxide System

Advances in Materials Science and Engineering ◽

10.1155/2009/502437 ◽

2009 ◽

Vol 2009 ◽

pp. 1-4 ◽

Cited By ~ 8

Author(s):

L. Bourja ◽

B. Bakiz ◽

A. Benlhachemi ◽

M. Ezahri ◽

J. C. Valmalette ◽

...

Keyword(s):

Solid Solution ◽

Raman Spectroscopy ◽

Phase Changes ◽

Phase System ◽

X Ray Diffraction ◽

X Ray ◽

Vibrational Studies ◽

Coprecipitation Route

A series of ceramics samples belonging to theCeO2-Bi2O3phase system have been prepared via a coprecipitation route. The crystallized phases were obtained by heating the solid precursors at600∘Cfor 6 hours, then quenching the samples. X-ray diffraction analyses show that forx<0.20a solid solutionCe1−xBixO2−x/2with fluorine structure is formed. For x ranging between 0.25 and 0.7, a tetragonalβ′phase coexisting with the FCC solid solution is observed. For x ranging between 0.8 and 0.9, a new tetragonalβphase appears. Theβ′phase is postulated to be a superstructure of theβphase. Finally, close tox=1, the classical monoclinicα Bi2O3structure is observed. Raman spectroscopy confirms the existence of the phase changes as x varies between 0 and 1.

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