scholarly journals The synthesis of magnetic nanoparticles from naturaliron sand of Kata beach Pariaman West Sumatera using ball milling method as environmental material

2019 ◽  
Vol 276 ◽  
pp. 06014 ◽  
Author(s):  
Erwin Amiruddin ◽  
Adhy Prayitno

Synthesis, magnetic, and structural properties and adsorption study of magnetic particles of Fe3O4 have been carried out. Magnetic particles were synthesized from natural iron sand of Kata Beach Pariaman West Sumatera using ball milling method. The structural properties of the samples were determined using X-Ray Diffractometer (XRD) technique. Magnetic properties such as magnetization were measured based on hysteresis loop using vibrating sample magnetometer (VSM). Mass susceptibility of the sample was measured using Pasco magnetic probe. It was found that the mass susceptibility of magnetic particles increased significantly as ball milling time increased. Based on VSM results, the magnetic particle of Fe3O4 has magnetization value of 32.26 emu/g with small coercivity of 174 Oe. Moreover, the results showed that ball milling method has succeeded to obtain magnetic particles. The increase of ball milling time resulted in an increase of magnetic moment of the sample. In this research, the magnetic particle of Fe3O4 was added to a solution of methyline blue performed using shaker method. Atomic Adsorption Spectroscopy (AAS) method was used to study the methylene blue degradation.

2018 ◽  
Vol 15 (2) ◽  
pp. 120
Author(s):  
Tahayati Ichsan ◽  
Salomo Salomo ◽  
Erwin Erwin ◽  
Usman Malik

Preparation of micro magnetic particle and its magnetic propertis from iron sand beach of Batang Kapas west Sumatera using Ball Milling method has been done. Prior to the Ball Milling process, the samples were processed by iron sand separator (ISS) in order to separate between magnetic particles and non magnetic one. Next, the concentrates from ISS were crushed by Ball Milling method  as a function of time namely 20, 40, and 60 hours. For separation between magnetic particles and non magnetic one, then NdFeB magnet was utilized. The results showed that the magnetic degree of the sample is about 0,5%. Measurements of magnetic induction solenoids were carried out using a Magnetic Probe Pasco PS -2162 as a function of current (2, 4, 6, 8 and 10) A and a  functions of distance (1, 2, 3, 4, and 5) mm. Then the total magnetic induction of the solenoid (solenoid with sample core and concentrate) was measured as a function of an electric current for a fixed distance of 1 mm. The calculation results showed that magnetic susceptibility and mass susceptibility increase with Ball Milling time from (3376,400-7765,130). This value is within the interval of 46-80000 which is the interval of Ilmenite mineral (FeTiO3; Antiferromagnetik). The increase in magnetic susceptibility and mass susceptibility of samples processed by Ball Milling is thought to be due to the increasing number of magnetic particles in the sample.


2020 ◽  
Vol 861 ◽  
pp. 250-255
Author(s):  
Fang Wang ◽  
Ai Xia Chen ◽  
Chao Yang ◽  
Min Han Xu ◽  
Da Ming Du ◽  
...  

Cermet is an important new engineering material that not only maintains the excellent properties of ceramic materials, but also has the advantages of metal materials. In this paper, the encapsulated alumina-aluminum composite powder was prepared by ball milling and characterized, which laid a foundation for the development of high properties cermet materials. Through the analysis of experimental results, the conclusions are shown when the ball milling time is greater than 3 h, the alumina particles are more evenly distributed around the aluminum powder. the ball milling for 6 h may have reached a limit of the mixing uniformity of the two powder, so the ball milling is determined 6 h as the better ball milling time. Under the ball milling condition of 50 r/min, the distribution of alumina particles around the aluminum powder is more uniform around the aluminum powder than the ball mill under 75 r/min, the ball milling speed is preferably 50 r/min. As the content of aluminum powder increases, the distribution of alumina in aluminum powder is large and uniform, and there is a small amount of pinning. It provides a package-like composite for the preparation of cermet with a wrapped structure and the thermal conduction mechanism of the controlled cermet.


2013 ◽  
Vol 432 ◽  
pp. 47-50
Author(s):  
Zhi Wen Wang ◽  
Zhi Wen Qiu ◽  
Yan Ping Feng ◽  
Ting Ting Xie ◽  
Jin Yun Chen ◽  
...  

In order to lay raw materials foundation for increasing the performance of insulating brick with the low grade quartz sand along the Yangtze River, the effect of ball milling time on the properties of quartz sand powder was researched via the ball milling method in this paper. The results show the grain diameter of quartz sand powder is gradually decreased, the grain fineness distribution is tapered narrowing. The liquidity of quartz sand powders is became poor with an increaseding the ball milling rotate speed, howerver, the tendency of variation is gradually relaxative. The vibration compaction density is decreased with an increaseding the ball milling rotate speed, but the fall amplitude difference is gradually shrinked. The ball milling rotate speed for 250r/min is better through the whole cost performance analysis.


2018 ◽  
Vol 777 ◽  
pp. 80-84
Author(s):  
Jie Guang Song ◽  
Yue Liu ◽  
Long He ◽  
Jin Shi Li ◽  
Wang Chen ◽  
...  

The Al2O3/Al cermet composite powders were prepared via the ball milling method,which provide raw materials for preparing high performance cermet materials. The results show that the number of Al2O3 particles on the surface of Al particles increases first and then decreases with increasing the ball milling time and milling rotating speed. The number of Al2O3 particles on the surface of Al particles increases with increasing ball to powder mass ratio. The analysis of the ratio of performance to price shows that the better parameters for preparing the pinned Al2O3/Al cermet composite powders are as follows, the ball milling time 24h,the ball milling rotating speed 100 r/min and the ratio of ball to powder 1:2.


2015 ◽  
Vol 830-831 ◽  
pp. 429-432 ◽  
Author(s):  
Udaya ◽  
Peter Fernandes

The paper illustrates Carbon nanotubes reinforced pure Al (CNT/Al) composites and fly ash reinforced pure Al (FA/Al) composites produced by ball-milling and sintering. Microstructures of the fabricated composite were examined and the mechanical properties of the composites were tested and analysed. It was indicated that the CNTs and fly ash were uniformly dispersed into the Al matrix as ball-milling time increased with increase in hardness.


2018 ◽  
Vol 768 ◽  
pp. 261-266 ◽  
Author(s):  
Ju Yun Kang ◽  
Guang Yao Chen ◽  
Bao Tong Li ◽  
Zi Wei Qin ◽  
Xiong Gang Lu ◽  
...  

In this paper, the BaZrO3(BZ) and BaZr0.97Y0.03O3-δ(BZY3) powders were prepared by using the industrial grade BaCO3, ZrO2and Y2O3powders combining the conventional solid state reaction. The BaZrO3(BZ) and BaZr0.97Y0.03O3-δ(BZY3) ceramics were fabricated at 1750°C. The effect of ball milling time and sintering aid (TiO2) on the sinterability of BaZr0.97Y0.03O3-δ(BZY3) ceramics were investigated, and the improved stability of BaZrO3refractory with Y2O3additive were studied according to the refractory-metal interaction. The results revealed that the particle size of BZY3 powders decreased first and then increased with the increasing of ball milling time from 6h to 12h, and the minimum particle size was only 2.252μm at 8h. When 2wt.%TiO2was added, the sintered pellet of BZY3 was the most densest and the relative density was above 95%. After melting the Ti2Ni alloy on the BZY and BZ ceramics, the thickness erosion layer of BaZrO3and BZY3refractories and Ti2Ni alloy is approximately 50μm and 20μm respectively, showing that BZY3 was more stable than BaZrO3refractory.


2021 ◽  
Vol 136 (10) ◽  
Author(s):  
Naradala Jayarambabu ◽  
Linganaboina Srinivasa Rao ◽  
Allam Akshaykranth ◽  
Tumu Venkatappa Rao ◽  
Rajaboina Rakesh Kumar

Sign in / Sign up

Export Citation Format

Share Document