Breakage Characteristics of Quartz Sand Based on Ring Shear Tests: Implications for the Fragmentation Processes of Rock Avalanches

To investigate the effects of internal shear fragmentation on dry granular flow, in this study a series of ring shear tests were performed on quartz sand samples under different normal stresses (100 kPa, 200 kPa, and 300 kPa), shear displacements (3 m, 5 m, 10m, 15 m, and 20 m), and shear rates (30 deg min−1, 60 deg min−1, and 90 deg min−1). Next, the grain-size distributions, fractal dimensions, and microcharacteristics of the quartz sand before and after the experiments were compared and analyzed. The study results show that grain breakage under shearing preferentially occurs at the edges of the particles and forms a bimodal distribution in frequency grain-size distribution curves, which is consistent with observations of rock avalanches. The fine particles prevent the coarse particles from breaking, in turn leading to the ultimate grain-size distribution and stable fractal dimension (2.61) of quartz sand at relatively small shear displacements compared with the travel distance of rock avalanches. The results of this study suggest that the fragmentation of rock avalanches during the shear spread stage may be far less significant than previously believed. Therefore, the fragmentation effect is not considered to be a major factor of the hypermobility in the late stage of rock avalanches.

Utilization of Waste Glass in Autoclaved Silica–Lime Materials

This paper aims to investigate the possibility of using waste glass of different colours as a complete substitute for quartz sand in autoclaved silica–lime samples. On the one hand, this increases the possibility of recycling waste glass; on the other hand, it allows obtaining autoclaved materials with better properties. In this research, reference samples with quartz sand (R) and white (WG), brown (BG), and green (GG) waste container glass were made. Parameters such as compressive strength, bulk density, and water absorption were examined on all samples. The samples were examined using a scanning electron microscope with an energy dispersive spectroscopy detector (SEM/EDS) and subjected to X-ray diffraction (XRD) analysis. The WG samples showed 187% higher compressive strength, BG by 159%, and GG by 134% compared to sample R. In comparison to the reference sample, volumetric density was 16.8% lower for sample WG, 13.2% lower for BG, and 7.1% lower for GG. Water absorption increased as bulk density decreased. The WG sample achieved the highest water absorption value, 15.84%. An X-ray diffraction analysis confirmed the presence of calcite, portlandite, and tobermorite phases. Depending on the silica aggregate used, there were differences in phase composition linked to compressive strength. Hydrated calcium silicates with varying crystallisation degrees were visible in the microstructure image.

EXPERIMENTAL STUDY ON MECHANICAL PROPERTIES OF POLYURETHANE POWDER COMPOSITES

In this paper, the effects of emery, lime, quartz sand and cement on the mechanical properties of polyurethane powder composites were studied by three-point flexural test, and the stress-strain curve was drawn. In the flexural test, the polyurethane cement composite formed a control group by changing the content of polyester polyol. When polyester polyol: isocyanate: cement =1:1:2, the average flexural strength of polyurethane cement was 37.1 MPa, and the strain was 10854 με.When polyester polyol: isocyanate: cement =1.15:1:2, the average flexural strength is 38.9 MPa and the strain is 23520 με.When polyester polyol: isocyanate: cement =1.3:1:2, the average flexural strength is 42.5 MPa and the strain is 32942 με. The flexural strength and ductility are improved to a certain extent due to the addition of polyester polyol.The average flexural strength of other polyurethane powder composites such as polyurethane emery test block is 45.1 MPa and the strain is 6203 με, the average flexural strength of polyurethane lime test block is 33.4 MPa and the strain is 6470 με, the average flexural strength of polyurethane quartz sand test block is 49.23 MPa and the strain is 7521 με. The results show that the flexural strength of polyurethane emery material and polyurethane quartz sand material is higher than that of polyurethane cement, which can be used to replace cement to a certain extent to reduce the cost of polyurethane composite material.

Recycled PET Sand for Cementitious Mortar

Cementitious materials cause a great impact on the environment due to the calcination of clinker and the extraction of non-renewable mineral resources. In this work, the replacement of quartz sand from the river by PET sand was evaluated at levels of 10%, 20%, and 30%. Tests were performed in the fresh state through consistency, air retention, density, and incorporated air and in the hardened state for compressive strength, flexural strength, density, capillarity, and water absorption. The results show that PET sand is viable in contents of up to 10%, improving the mechanical properties of the mortar and without compromising its workability and incorporated air properties. Above that level, the loss of properties is very excessive, mainly of workability and incorporated air. The incorporated air of the 30% composition, for example, reaches 24%, an excessive value that impacts the properties of the hardened state, making it impossible to use the material at levels greater than 20%. It is concluded that the use of recycled PET sand is a possibility that contributes to sustainable development, as it reduces the extraction of quartz sand from the river, a non-renewable mineral resource.

Influence of Sand Casting Waste as Substitutor of Quartz Sand in Mortar

Sand casting waste has the potential to replace quartz sand in mortar manufacture because it contains high silica. This study uses sand casting waste from the steel industry in Gresik, Indonesia to observe how it affects the quality of the mortar. Initial characterization were carried out to determine the properties of the material, including; magnetic test which results are not attracted by magnets, moisture content test with a value of 0.328%, XRD test to determine the crystallinity content which results contain 99.52% Silica Quartz, and XRF test to determine the content of the compound in which results are 81.25% Silica dominant. Then observations were made by making mortar with the replacement of quartz sand by sand casting with variations of 0% wt, 25% wt, 50% wt, and 100% wt and then tested its compressive strength at 3 days, 7 days, and 28 days. Based on the research that has been done, the optimum result using sand casting is at 25% wt with a compressive strength of 251.15 kgf/cm2 at 28 days of age which is higher than the standard.

Understanding Mud Volcano System Using Hele-Shaw (H-S) Experiment: Seismic Confirmation at East Java Mud Volcano

Numerous researchers have carried out studies on the mud volcano system in East Java. However, there have been no experiments on the mud volcano system's mechanism, including overpressure confirmed by direct subsurface data. Therefore, this study aims to directly evaluate the mud volcano system's mechanism using the Hele-Shaw (H-S) experiment with the subsurface data confirmation. The H-S experiment utilized four primary materials: quartz sand diameter below 250 µm and 320 µm to analogize the porous layer. Gypsum flour clay is the ductile layer, while mud from the Kuwu and Kesongo Mud Volcanoes is the original material from nature. Wax represents impermeable material. The sealing layer is made of wax, and oxygen represents the natural fluids of the rock formation. The overpressured zone is created by pumping oxygen into a layer of quartz sand covered by a wax as an impermeable layer. Pressure is measured digitally, and the process is continuously recorded to produce traceable data. Each material was experimented on individually to determine the critical phase characteristics, valve fault structure geometry, and validation with seismic interpretation. The results indicate that the critical phase of the mud volcano system is characterized by the dome structure at the surface, with high intensify of gas and oil seepage. Piercement structure geometry is shown by plumbing of fluidization zone, which becomes shallower than before. Furthermore, each material's piercement structure geometry shows a consistent pattern, with differences in the density of the fault and pressure structures. Thus, the H-S experiment's validation with seismic interpretation shows a similar geometry in pressure structures and valve faults as the mud volcano system's migration paths.

New granular rock-analogue materials for simulation of multi-scale fault and fracture processes

In this study, we present a new granular rock-analogue material (GRAM) with a dynamic scaling suitable for the simulation of fault and fracture processes in analogue experiments. Dynamically scaled experiments allow the direct comparison of geometrical, kinematical and mechanical processes between model and nature. The geometrical scaling factor defines the model resolution, which depends on the density and cohesive strength ratios of model material and natural rocks. Granular materials such as quartz sands are ideal for the simulation of upper crustal deformation processes as a result of similar nonlinear deformation behaviour of granular flow and brittle rock deformation. We compared the geometrical scaling factor of common analogue materials applied in tectonic models, and identified a gap in model resolution corresponding to the outcrop and structural scale (1–100 m). The proposed GRAM is composed of quartz sand and hemihydrate powder and is suitable to form cohesive aggregates capable of deforming by tensile and shear failure under variable stress conditions. Based on dynamical shear tests, GRAM is characterized by a similar stress–strain curve as dry quartz sand, has a cohesive strength of 7.88 kPa and an average density of 1.36 g cm−3. The derived geometrical scaling factor is 1 cm in model = 10.65 m in nature. For a large-scale test, GRAM material was applied in strike-slip analogue experiments. Early results demonstrate the potential of GRAM to simulate fault and fracture processes, and their interaction in fault zones and damage zones during different stages of fault evolution in dynamically scaled analogue experiments.

Universal calibration of a scintillation spectrometer with a NaI(Tl) detector when measuring 137Cs activity in counting samples of arbitrary density and volume

The article proposes an empirical method for constructing a universal calibration for a scintillation gamma spectrometer, which allows determining the activity and specific activity of 137Cs with an accuracy of no more than 15% in counting samples of arbitrary density and volume in cylindrical containers with a volume of 250 ml and 500 ml. To construct calibration ratios, measurements of 137Cs sample media prepared on the basis of materials of different densities (quartz sand, plastic granules and sawdust) were performed. The calibration was carried out by preparing samples from the listed materials with a volume of 50 to 250 ml in increments of 50 ml for a 250 ml container and 100-500 ml in increments of 100 ml for a 500 ml container. Along with taking into account the volume of the counting sample, its weighing was also carried out. The result of the measurements performed for each material was the ratio of the activity of the counting sample to the counting intensity in the 137Cs window, depending on the volume. The universal calibration factor is obtained by taking into account the counting rate from the mass and volume of the sample for the corresponding measuring vessel.

Optimal Proportion of Similar Materials and Rockburst Tendency of White Sandstone

To explore the tendency of rockburst, a similar material ratio was optimised based on white sandstone. Quartz sand, iron powder, gypsum, cement, retarder, and a water-reducing agent were used as the main materials. The orthogonal test design principle was used to determine the four-factor and four-level orthogonal test design with the quartz sand content, iron powder content, gypsum-cement ratio, and sand particle size as the influencing factors. Uniaxial compression tests and tensile tests were conducted on similar material models. The tensile strength and elastic modulus were analysed, the significance of each influencing factor was investigated, and the test results of the similar materials were fitted. The optimal ratios of the similar materials of white sandstone were found to be quartz sand content of 36%, iron powder content of 1.9%, gypsum-cement ratio of 1.8 : 1, and sand particle size of 2–4 mm. The physical and mechanical properties of the similar materials were consistent with those of white sandstone. The mechanical properties of the similar materials were compared with those of the original rock. By judging the rockburst propensity and verifying the index, it is concluded that the similar materials can effectively simulate the characteristics of white sandstone, which is an ideal similar material of rockburst, and they all show strong rockburst propensity. The rock specimens with optimal proportions were produced, and the internal energy changes and rockburst mechanisms of the model at different temperatures were discussed. The results show that the rockburst process is closely related to energy, such as thermal energy and elastic strain energy, and the rock failure process can be divided into three main stages: energy accumulation, microcrack formation and propagation, and crack penetration and bursting. It provides an experimental basis for the preparation of rockburst similar materials that are more in line with the actual situation of the project and provides a basis for discussing the energy criterion of rockburst.