scholarly journals The Preparation of Boron-doped Activated Alumina by impregnating boron in the period of boehmite

2021 ◽  
Vol 353 ◽  
pp. 01026
Author(s):  
Rong Fu
Keyword(s):  
Surface Acidity ◽  
Chemical Properties ◽  
Nitrogen Adsorption ◽  
Chemical Environment ◽  
Activated Alumina ◽  
Boron Doped ◽  
Pore Texture ◽  
Phase Surface ◽  
Physical And Chemical ◽  
And Chemical Properties

This paper systematically studied the pore structure, crystal phase, surface acidity and the chemical environment of aluminum of boron-doped γ-alumina, by impregnating boron in the period of boehmite. The nitrogen adsorption, XRD, FTIR etc. technique was used to determine the pore texture, crystallography, acid/base properties and aluminum coordination. the XRD spectrum of boria-alumina have no significant change due to the addition of boron. The specific surface area and pore volume diameter of B-Al2O3 increase significantly. The NMR spectra of B-Al2O3 shows that boron changed the chemical environment of aluminum, which caused differences in the physical and chemical properties of the surface.

Characterization of Shivirtui Zeolite Modified with Aluminum Oxyhydroxide Nanofibers

2019 ◽  
Vol 942 ◽  
pp. 40-49
Author(s):  
Yulia Murashkina ◽  
Olga B. Nazarenko
Keyword(s):  
Chemical Properties ◽  
Nitrogen Adsorption ◽  
X Ray Diffraction ◽  
Scanning Electronic Microscopy ◽  
Electronic Microscopy ◽  
X Ray ◽  
Physical And Chemical ◽  
And Chemical Properties ◽  
Aluminum Oxyhydroxide

Natural zeolite of Shivirtui deposit (Russia) was modified with nanofibers of aluminum oxyhydroxide AlOOH. Aluminum oxyhydroxide nanofibers were produced at the heating and oxidation of aluminum powder with water. The properties of modified zeolite were investigated by means of X-ray diffraction, transmission electronic microscopy, scanning electronic microscopy, low-temperature nitrogen adsorption, thermal analysis, and Fourier transform infrared spectroscopy. It was found that water content in the modified sample of zeolite was about 15 %. Based on the study of the physical and chemical properties, shivirtui zeolite modified with nanofibers of aluminum oxyhydroxide can be proposed for use as a flame-retardant additive to polymers.

Boron-doped coronenes with high redox potential for organic positive electrodes in lithium-ion batteries: a first-principles density functional theory modeling study

2018 ◽  
Vol 6 (21) ◽  
pp. 10111-10120 ◽  
Author(s):  
Yuntong Zhu ◽  
Ki Chul Kim ◽  
Seung Soon Jang
Keyword(s):  
Lithium Ion Batteries ◽  
Density Functional ◽  
Electrode Materials ◽  
Chemical Properties ◽  
Lithium Ion ◽  
Functional Theory ◽  
Positive Electrodes ◽  
Boron Doped ◽  
Physical And Chemical ◽  
And Chemical Properties

Boron-doped coronenes are attractive as promising positive electrode materials for lithium-ion batteries due to the unique physical and chemical properties of coronene.

Lignite Thermal Upgrading and its Effect on Surface Properties

2012 ◽  
Vol 524-527 ◽  
pp. 887-893 ◽  
Author(s):  
Jun Guan ◽  
De Min He ◽  
Bin Bin Song ◽  
Qiu Min Zhang
Keyword(s):  
Surface Properties ◽  
Functional Group ◽  
Group Analysis ◽  
Chemical Properties ◽  
Nitrogen Adsorption ◽  
Oxygen Absorption ◽  
Functional Group Analysis ◽  
Mild Pyrolysis ◽  
Physical And Chemical ◽  
And Chemical Properties

Lignite samples, Huolinhe(HLH) and Xiaolongtan(XLT) lignites were used for experiments. Mild pyrolysis experiments were carried out by final temperature 150～450°C. Physical and chemical properties have been investigated using thermogravimetric, FTIR analysis, nitrogen adsorption and oxygen-functional group analysis. Besides, the changes of the surface properties during upgrading were characterized in detail. The results show that specific surface area and moisture-holding capacity have the trend of first decreases and then increases in the upgrading temperature range. Furthermore, the decomposition of the oxygen-bearing functional groups on the coal surface which reduced the moisture-holding capacity. Oxygen absorption experiments indicate that thermal upgrading could decrease the tendency of lignite to spontaneous combustion.

Influence of tungsten sources on the synthesis and properties of ammonium dioxothiotungstate

2010 ◽  
Vol 64 (1) ◽  
Author(s):  
Yunfei Bi ◽  
Shuangqin Zeng ◽  
Dadong Li ◽  
Hong Nie
Keyword(s):  
Tungsten Oxide ◽  
Chemical Properties ◽  
Nitrogen Adsorption ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Detailed Characteristic ◽  
Temperature Programmed ◽  
Physical And Chemical ◽  
And Chemical Properties

AbstractAmmonium dioxothiotungstate was synthesized using different tungsten sources and characterized in detail by powder X-ray diffraction, energy dispersive X-ray spectrometry, transmission electron microscopy, nitrogen adsorption, and temperature-programmed sulfidation. It was found that tungsten oxide nanobelts are superior to ammonium metatungstate as tungsten source for the synthesis of ammonium dioxothiotungstate due to a time-consuming aging step being excluded from the synthesis route. Moreover, detailed characteristic data reveal that, when tungsten oxide nanobelts are used, the physical and chemical properties of the resulting ammonium dioxothiotungstate including particles size, specific surface area, and sulfidation pattern were improved. Also, the hydrodesulfurization measurements showed higher catalytic activity and balanced selectivity of the resulting ammonium dioxothiotungstate.

Research on Adsorption of H2S by Oil Shale Ash

2012 ◽  
Vol 463-464 ◽  
pp. 133-137 ◽  
Author(s):  
Hong Qin ◽  
Zhi Jia Tan ◽  
Qing Wang
Keyword(s):  
Adsorption Capacity ◽  
Oil Shale ◽  
Chemical Properties ◽  
Nitrogen Adsorption ◽  
Physical And Chemical Properties ◽  
Oil Shale Ash ◽  
Shale Ash ◽  
Physical And Chemical ◽  
And Chemical Properties

The ash of Huadian oil shale is made to remove H2S in this experiment. XRD and nitrogen adsorption experiments are used to analyze the physical and chemical properties of the ash, the results show that the ash of oil shale has many metal and nonmetal oxides, and also has much microporous and mesoporous, all above is helpful to remove H2S. The sample is modified by different ways to see the change of adsorption capacity. the sample which is modified by alkali and sprinkler is the best adsorbent, but the sample which is modified by microwave does not increase the removal ability obviously.

Statistical criteria of stellar population types

1966 ◽  
Vol 24 ◽  
pp. 101-110
Author(s):  
W. Iwanowska
Keyword(s):  
Stellar Population ◽  
Chemical Properties ◽  
Spectrophotometric Study ◽  
Physical And Chemical Properties ◽  
Population Type ◽  
The Galaxy ◽  
Distribution Parameters ◽  
Physical And Chemical ◽  
Statistical Criteria ◽  
And Chemical Properties

In connection with the spectrophotometric study of population-type characteristics of various kinds of stars, a statistical analysis of kinematical and distribution parameters of the same stars is performed at the Toruń Observatory. This has a twofold purpose: first, to provide a practical guide in selecting stars for observing programmes, second, to contribute to the understanding of relations existing between the physical and chemical properties of stars and their kinematics and distribution in the Galaxy.

Tailoring microstructures of materials through biomimetics

1993 ◽  
Vol 51 ◽  
pp. 500-501
Author(s):  
Mehmet Sarikaya ◽  
Ilhan A. Aksay
Keyword(s):  
Chemical Properties ◽  
Design And Synthesis ◽  
Structure Sensitive ◽  
Macro Scale ◽  
Methods Of Synthesis ◽  
Successive Level ◽  
Engineering Materials ◽  
Physical And Chemical ◽  
And Chemical Properties ◽  
Synthesis Of Materials

Biomimetics involves investigation of structure, function, and methods of synthesis of biological composite materials. The goal is to apply this information to the design and synthesis of materials for engineering applications.Properties of engineering materials are structure sensitive through the whole spectrum of dimensions from nanometer to macro scale. The goal in designing and processing of technological materials, therefore, is to control microstructural evolution at each of these dimensions so as to achieve predictable physical and chemical properties. Control at each successive level of dimension, however, is a major challenge as is the retention of integrity between successive levels. Engineering materials are rarely fabricated to achieve more than a few of the desired properties and the synthesis techniques usually involve high temperature or low pressure conditions that are energy inefficient and environmentally damaging.In contrast to human-made materials, organisms synthesize composites whose intricate structures are more controlled at each scale and hierarchical order.

Response of corn (Zea mays L.) to various organic-based fertilizers in marginal upland of Sta. Rita, Samar

2017 ◽  
pp. 31-43
Author(s):  
Berta Ratilla ◽  
Loreme Cagande ◽  
Othello Capuno
Keyword(s):  
Block Design ◽  
Management Strategies ◽  
Chemical Properties ◽  
Organic Fertilizers ◽  
Growth And Yield ◽  
Physical And Chemical Properties ◽  
Total N ◽  
Randomized Complete Block Design ◽  
Physical And Chemical ◽  
And Chemical Properties

Organic farming is one of the management strategies that improve productivity of marginal uplands. The study aimed to: (1) evaluate effects of various organic-based fertilizers on the growth and yield of corn; (2) determine the appropriate combination for optimum yield; and (3) assess changes on the soil physical and chemical properties. Experiment was laid out in Randomized Complete Block Design, with 3 replications and 7 treatments, namely; T0=(0-0-0); T1=1t ha-1 Evans + 45-30-30kg N, P2O5, K2O ha-1; T2=t ha-1 Wellgrow + 45-30-30kg N, P2O5, K2O ha-1; T3=15t ha-1 chicken dung; T4=10t ha-1 chicken dung + 45-30-30kg N, P2O5, K2O ha-1; T5=15t ha-1 Vermicast; and T6=10t ha-1 Vermicast + 45-30-30kg N, P2O5, K2O ha-1. Application of organic-based fertilizers with or without inorganic fertilizers promoted growth of corn than the control. But due to high infestation of corn silk beetle(Monolepta bifasciata Horns), its grain yield was greatly affected. In the second cropping, except for Evans, any of these fertilizers applied alone or combined with 45-30-30kg N, P2O5, K2O ha-1 appeared appropriate in increasing corn earyield. Soil physical and chemical properties changed with addition of organic fertilizers. While bulk density decreased irrespective of treatments, pH, total N, available P and exchangeable K generally increased more with chicken dung application.

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