Effect of Ca content percentage and sintering temperature on corrosion rate in Mg-Ca composite fabricated using powder metallurgy technique

2016 ◽  
Author(s):  
M. S. Syaza Nabilla ◽  
C. D. Zuraidawani ◽  
D. M. Nazree
2013 ◽  
Vol 465-466 ◽  
pp. 886-890
Author(s):  
Adibah Amir ◽  
Othman Mamat

Tronohs raw sand was converted into fine silica particles via a series of milling process. Addition of these fine particles into iron composite was found to modify its mechanical properties. The composite was prepared using powder metallurgy technique with varying percentage of silica particles; 5, 10, 15, 20 and 25wt%. The composites were sintered at three different temperatures; 1000° C, 1100° C and 1200° C to find the most suitable sintering temperature. Changes in density and hardness were observed. The results showed that composite consist of 20wt% silica particles and sintered at 1100° C exhibits best improvement.


2015 ◽  
Vol 754-755 ◽  
pp. 907-911 ◽  
Author(s):  
M.S. Syaza Nabilla ◽  
C.D. Zuraidawani ◽  
M.N. Derman

Having the benefit of lightweight and low density makes magnesium (Mg) a good element with high potential to be used in various field of work. Yet, its application is limited for Mg is relatively low in term of strength. Hence, calcium (Ca) is chosen to be mixed with Mg as additional element for it is lightweight and non-toxic. In this research, Mg is prepared with different weight percentage (0, 1, 2 wt. %) of Ca via powder metallurgy (PM) method. The effect of sintering was investigated by focusing on the microstructure and properties of sintered sample. The samples were sintered at two sintering temperature (500 and 600 °C) in argon atmosphere. Morphological analysis carried out by optical microscope shows increase pores refinement with the increase of sintering temperature together with calcium content in Mg-Ca composites. Results show that the grain size and hardness of the samples increase as sintering temperature increase.


2016 ◽  
Vol 857 ◽  
pp. 242-245
Author(s):  
Mohd Tajuddin Mohd Tajuddin ◽  
Shamsul Baharin Jamaludin

PM Co-Cr-Mo (F75) alloys are widely used in implants due to their mechanical properties, good wear resistance and as well as biocompatibility. Currently, they are fabricated by casting technique. In this present research, F75 was fabricated by powder metallurgy technique. The powder was mixed with 2 wt. % of stearic acid in order to form green body and compacted at 500 MPa. The effect of sintering temperature was investigated to observe its effect to the microstructure of F75 (Co-Cr-Mo). Samples were sintered for 2 hours at 2 different temperatures (1250°C and 1300°C) with 10°C/min in argon atmosphere. Physical properties such as density and porosity were obtained by Archimedes principle. Microstructure was observed by using optical microscope Olympus BX41M. The results indicate that increasing the sintering temperature will influence the density and porosity, thus the microstructure itself.


2021 ◽  
Vol 18 (23) ◽  
pp. 683
Author(s):  
Bappi Sarker ◽  
Md. Arafat Rahman ◽  
Md. Mizanur Rahman ◽  
Md. Saiful Islam

Despite the importance of Nickel Oxide (NiO) in diverse functional applications, very little information is available on the mechanical properties of bulk or porous NiO or, mostly unnoticed. In this study, porous Ni-NiO foam was synthesized using space holding-powder metallurgy and sintering methods to produce opened-cell structure with macrogravel and Neolamarckia cadamba (Cadamba flower) like surface morphology. Four different types of porous Ni-NiO with different pore diameter of 35.65 ± 12.77, 36.10 ± 8.85, 68.20 ±7.36 and 62.45 ± 17.48 µm were fabricated for evaluating the effect of porosity on the mechanical properties of bulk porous Ni-NiO foam. The mechanical properties such as bulk crushing force of as synthesized Ni-NiO foam with various porosities such as 20.55, 27.35, 27.85 and 28.82 % exhibited the average crushing load of 115.40, 39.95, 138.10 and 151.20 N, respectively. This study suggests that crushing load of Ni-NiO foam is not only depending on the porosity but also on the sintering temperature and crystallite sizes of NiO. HIGHLIGHTS Ni-NiO foam is synthesized using space holding-powder metallurgy and sintering methods Different pore diameter is fabricated for evaluating the effect of porosity on the mechanical properties of bulk porous Ni-NiO foam Crushing strength of Ni-NiO foam is not only depending on the porosity but also on the sintering temperature and crystallite sizes of NiO GRAPHICAL ABSTRACT


2011 ◽  
Vol 410 ◽  
pp. 216-219 ◽  
Author(s):  
S. Mahathanabodee ◽  
Tippaban Palathai ◽  
S. Raadnui ◽  
Ruangdaj Tongsri ◽  
Narongrit Sombatsompop

In this work, the three compositions of hexagonal boron nitride (10, 15 and 20 vol. %)-embedded 316L stainless steel (SS316L/h-BN) composites were prepared by a conventional powder metallurgy technique and then sintered at varying temperatures of 1100 to 1250°C for 60 min in H2 atmosphere. The h-BN content and sintering temperature were found to affect the microstructure and hardness of the composites. The hardness decreased with increasing h-BN content and was improved by increasing the sintering temperature. Microstructure results revealed that the boride phase was formed at the grain boundary at the sintering temperature higher than 1150°C and the boride phase formation was observed to transform the h-BN in the composites.


2021 ◽  
Vol 30 (2) ◽  
pp. 1207-1220
Author(s):  
Amarjit Singh ◽  
Jarnail Singh ◽  
Manoj Kumar Sinha ◽  
Ravi Kumar ◽  
Vikram Verma

Crystals ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 540
Author(s):  
Mohamed Ali Hassan ◽  
Hossam M. Yehia ◽  
Ahmed S. A. Mohamed ◽  
Ahmed Essa El-Nikhaily ◽  
Omayma A. Elkady

To improve the AlCoCrFeNi high entropy alloys’ (HEAs’) toughness, it was coated with different amounts of Cu then fabricated by the powder metallurgy technique. Mechanical alloying of equiatomic AlCoCrFeNi HEAs for 25 h preceded the coating process. The established powder samples were sintered at different temperatures in a vacuum furnace. The HEAs samples sintered at 950˚C exhibit the highest relative density. The AlCoCrFeNi HEAs model sample was not successfully produced by the applied method due to the low melting point of aluminum. The Al element’s problem disappeared due to encapsulating it with a copper layer during the coating process. Because the atomic radius of the copper metal (0.1278 nm) is less than the atomic radius of the aluminum metal (0.1431 nm) and nearly equal to the rest of the other elements (Co, Cr, Fe, and Ni), the crystal size powder and fabricated samples decreased by increasing the content of the Cu wt%. On the other hand, the lattice strain increased. The microstructure revealed that the complete diffusion between the different elements to form high entropy alloy material was not achieved. A dramatic decrease in the produced samples’ hardness was observed where it decreased from 403 HV at 5 wt% Cu to 191 HV at 20 wt% Cu. On the contrary, the compressive strength increased from 400.034 MPa at 5 wt% Cu to 599.527 MPa at 15 wt% Cu with a 49.86% increment. This increment in the compressive strength may be due to precipitating the copper metal on the particles’ surface in the nano-size, reducing the dislocations’ motion, increasing the stiffness of produced materials. The formability and toughness of the fabricated materials improved by increasing the copper’s content. The thermal expansion has increased gradually by increasing the Cu wt%.


2020 ◽  
Vol 38 (3) ◽  
pp. 273-286 ◽  
Author(s):  
Cristina Garcia-Cabezon ◽  
Celia Garcia-Hernandez ◽  
Maria L. Rodriguez-Mendez ◽  
Gemma Herranz ◽  
Fernando Martin-Pedrosa

AbstractMicrostructural changes that result in relevant improvements in mechanical properties and electrochemical behavior can be induced using different sintering conditions of ASTM F75 cobalt alloys during their processing using powder metallurgy technique. It has been observed that the increase in carbon and nitrogen content improves corrosion resistance and mechanical properties as long as the precipitation of carbides and nitrides is avoided, thanks to the use of rapid cooling in water after the sintering stage. In addition, the reduction of the particle size of the powder improves hardness and resistance to corrosion in both acid medium with chlorides and phosphate-buffered medium that simulates the physiological conditions for its use as a biomaterial. These results lead to increased knowledge of the role of carbon and nitrogen content in the behavior displayed by the different alloys studied.


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