scholarly journals Synthesis of magnetic g-C3N4 by one-step method and its adsorption performance for Cd(II)

Author(s):  
Shuangzhen Guo ◽  
Chenmu Zhang ◽  
Fan Zhang ◽  
Xianlong Li ◽  
Peilei Zhang ◽  
...  
Nanoscale ◽  
2019 ◽  
Vol 11 (40) ◽  
pp. 18653-18661 ◽  
Author(s):  
Yinli Liu ◽  
Miao Liu ◽  
Jie Jia ◽  
Dequn Wu ◽  
Tingting Gao ◽  
...  

β-CD-based hollow nanoparticles (β-CDHN) were first fabricated through a facile one-step method, which presented extraordinary adsorption performance towards pollutants.


2020 ◽  
Vol 2020 ◽  
pp. 1-11 ◽  
Author(s):  
Fujiao Song ◽  
Yan Cao ◽  
Yunxia Zhao ◽  
Ruiyu Jiang ◽  
Qi Xu ◽  
...  

Li+- and Na+-exchanged ZIF-67 was synthesized by a new one-step method of ion as-exchange technique and tested as CO2 adsorbents. As a comparison, the standard ion-exchange procedure was also carried out. The powder X-ray diffraction (XRD), scanning electronic microscope (SEM), particle size analyzer (PSD), and thermal gravimetry analysis (TGA) were used to investigate the effect of ion-exchange techniques on the structure of the materials. CO2 uptake of ZIF-67 ion exchanged by one-step method is much higher than that by the standard ion-exchange procedure. All of the adsorption isotherms show linear patterns with stable adsorption rate from 0 bar to 1 bar, which reveals the materials could get excellent adsorption performance at higher pressure range (>1 bar). Elemental analysis, N2 physical adsorption, and the point of zero charge (PZC) were carried out to confirm the adsorption mechanism. van der Waals interaction determined by the surface area and coordination interaction resulting from electrostatic interaction work in synergy to enhance CO2 adsorption performance of ZIF-67 ion exchanged by the one-step method.


2014 ◽  
Vol 1073-1076 ◽  
pp. 990-994
Author(s):  
Jin Ping Song ◽  
Qi Ma ◽  
Shao Min Shuang ◽  
Yong Guo ◽  
Chuan Dong

A simple, fast one-step method was used to prepare graphene/SnO2/citric acid (GN/SnO2/CA) nanocomposites. Fourier transform Infrared spectroscopy, UV-vis adsorption spectroscopy, transmission electron microscopy, X-Ray diffraction, Raman spectroscopy and X-ray photoelectron spectroscopy were employed to characterize as-prepared GN/SnO2/CA nanocomposites. Furthermore, in the adsorption performance research, GN/SnO2/CA nanocomposites indeed displayed excellent adsorption ability towards cationic dyes.


1993 ◽  
Vol 58 (11) ◽  
pp. 2642-2650 ◽  
Author(s):  
Zdeněk Kruliš ◽  
Ivan Fortelný ◽  
Josef Kovář

The effect of dynamic curing of PP/EPDM blends with sulfur and thiuram disulfide systems on their mechanical properties was studied. The results were interpreted using the knowledge of the formation of phase structure in the blends during their melt mixing. It was shown, that a sufficiently slow curing reaction is necessary if a high impact strength is to be obtained. Only in such case, a fine and homogeneous dispersion of elastomer can be formed, which is the necessary condition for high impact strength of the blend. Using an inhibitor of curing in the system and a one-step method of dynamic curing leads to an increase in impact strength of blends. From the comparison of shear modulus and impact strength values, it follows that, at the stiffness, the dynamically cured blends have higher impact strength than the uncured ones.


2019 ◽  
Vol 375 ◽  
pp. 122000 ◽  
Author(s):  
Yang Xuan ◽  
Xian-Lin Song ◽  
Xiao-Quan Yang ◽  
Ruo-Yun Zhang ◽  
Zi-Yu Song ◽  
...  

Materials ◽  
2021 ◽  
Vol 14 (11) ◽  
pp. 3138
Author(s):  
Kamila Gosz ◽  
Agnieszka Tercjak ◽  
Adam Olszewski ◽  
Józef Haponiuk ◽  
Łukasz Piszczyk

The utilization of forestry waste resources in the production of polyurethane resins is a promising green alternative to the use of unsustainable resources. Liquefaction of wood-based biomass gives polyols with properties depending on the reagents used. In this article, the liquefaction of forestry wastes, including sawdust, in solvents such as glycerol and polyethylene glycol was investigated. The liquefaction process was carried out at temperatures of 120, 150, and 170 °C. The resulting bio-polyols were analyzed for process efficiency, hydroxyl number, water content, viscosity, and structural features using the Fourier transform infrared spectroscopy (FTIR). The optimum liquefaction temperature was 150 °C and the time of 6 h. Comprehensive analysis of polyol properties shows high biomass conversion and hydroxyl number in the range of 238–815 mg KOH/g. This may indicate that bio-polyols may be used as a potential substitute for petrochemical polyols. During polyurethane synthesis, materials with more than 80 wt% of bio-polyol were obtained. The materials were obtained by a one-step method by hot-pressing for 15 min at 100 °C and a pressure of 5 MPa with an NCO:OH ratio of 1:1 and 1.2:1. Dynamical-mechanical analysis (DMA) showed a high modulus of elasticity in the range of 62–839 MPa which depends on the reaction conditions.


2013 ◽  
Vol 321-324 ◽  
pp. 209-212
Author(s):  
Chun Yan Xia

nfluences on properties of the concrete highway pavement were analyzed in this paper, and the optimal formulation materials were gotten to use in the repair of used-broken cement blocks in the experiment. Polyurethane concrete material was prepared, combing the ordinary concrete technology with one-step method of the synthesis of polyurethane hard bubble, and then its mechanical properties of the relevant parameters were measured to determine the optimal preparation program. The results show that the polyurethane concrete also has sufficiently good mechanical properties while it has the characteristic of fast patching.


2002 ◽  
Vol 43 (21) ◽  
pp. 3887-3890 ◽  
Author(s):  
Michael R. Wood ◽  
June Y. Kim ◽  
Kathy M. Books

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