Low-temperature deformation of body-centred cubic metals I. Yield and How stress measurements

Measurements of the tensile yield stress and of the temperature and strain-rate sensitivity of the flow stress are reported for single crystals of niobium and for polycrystalline speci­mens of niobium, vanadium and tantalum over the temperature range 4.2 to 373°K. The temperature dependences of yield and flow stresses are nearly identical, and the results show that the high yield stresses at low temperatures are attributable mainly to a frictional force opposing the motion of free dislocations. The yield stress is very dependent on the purity of the metal, and the temperature and strain rate sensitivities vary slightly with purity, especially at higher temperatures. At very low temperatures, the stress needed to cause macroscopic deformation at a strain rate of 10 -4 s -1 is ca . 1% of the shear modulus in all specimens examined. The relation of the results to the interpretation of the para­meters in the Hall-Petch equation for the variation of yield stress with grain size is briefly discussed.

1990 ◽  
Vol 213 ◽  
Author(s):  
V. Vitek ◽  
Y. Sodani ◽  
J. Cserti

ABSTRACTIt is now generally accepted that in many L12 compounds the yielding behavior is controlled by the special features of the cores of screw dislocations. In this paper we first summarize results of the atomistic studies of the core structures of the <110> screw dislocations in these compounds. At this point we show that, depending on the atomic bonding, two distinct classes of L12 alloys exist. In the first, represented by alloys like Ni3Al, a glissile configuration of the core exists on {111} planes although a sessile configuration is energetically more favored. In the second class, represented by alloys like Pt3A1 and A13Ti modified by alloying into L12 structure, the cores of screw dislocations are always sessile. Using the results of the atomistic studies we present physical models explaining the temperature dependences of the yield stress in both classes of L12 alloys. At this point we also present a further development of the model for the anomalous temperature dependence of the yield stress in alloys like Ni3A1, originally put forward by Paidar et al. [15]. In this development strain rate effects are included and it is shown that the model explains not only the orientation dependences of the yield stress in the anomalous regime but also the very low strain rate sensitivity observed in this regime.


The mechanical characteristics (limit of forced elasticity σforc, fracture stress σfr, relative deformation to failure εfr) of polyimide films of kapton H type under uniaxial tension conditions along the direction of drawing in the temperature range (4.2-293 K), deformation rates (10-5 - 10-3 s-1) and film thicknesses (25, 75 and 125 μm) were investigated. It is discovered, that the forced-elastic state remains for all films up to 4.2 K of all strain rates - σfors<σfr. In this case, the reserve of elasticity significantly depends on the thickness of the film with a decrease in temperature. A sharp decrease in εfr occurs in films: 125 μm thick - at 77 K, 75 μm thick - at 4.2 K. Two variants of deformation curves are possible in a 25 μm thick film at 4.2 K: with a short nonlinear stage or with a long one proceeding jumpily. The working surface of the samples that have undergone jump deformation is covered with a deformation relief, partially representing a delayed highly elastic deformation. The σfors limit is most sensitive to the strain rate. The nature of the strain rate sensitivity σfors(έ) depends on the temperature and film thickness. The change to the opposite in the character of σfors(έ) and σfr(έ) with a decrease in temperature to 4.2 K in 75 and 125 thick films was found for a first time. Change in the character of σfors(έ) is not observed in 25 μm thick film which retains the maximum reserve of elasticity at 4.2 K


2012 ◽  
Vol 735 ◽  
pp. 93-100
Author(s):  
Alexander J. Carpenter ◽  
Anthony J. Barnes ◽  
Eric M. Taleff

Complex sheet metal components can be formed from lightweight aluminum and magnesium sheet alloys using superplastic forming technologies. Superplastic forming typically takes advantage of the high strain-rate sensitivity characteristic of grain-boundary-sliding (GBS) creep to obtain significant ductility at high temperatures. However, GBS creep requires fine-grained materials, which can be expensive and difficult to manufacture. An alternative is provided by materials that exhibit solute-drag (SD) creep, a mechanism that also produces elevated values of strain-rate sensitivity. SD creep typically operates at lower temperatures and faster strain rates than does GBS creep. Unlike GBS creep, solute-drag creep does not require a fine, stable grain size. Previous work by Boissière et al. suggested that the Mg-Y-Nd alloy, essentially WE43, deforms by SD creep at temperatures near 400°C. The present investigation examines both tensile and biaxial deformation behavior of ElektronTM 43 sheet, which has a composition similar to WE43, at temperatures ranging from 400 to 500°C. Data are presented that provide additional evidence for SD creep in Elektron 43 and demonstrate the remarkable degree of biaxial strain possible under this regime (>1000%). These results indicate an excellent potential for producing complex 3-D parts, via superplastic forming, using this particular heat-treatable Mg alloy.


1994 ◽  
Vol 364 ◽  
Author(s):  
M. L. Weaver ◽  
V. Levit ◽  
M. J. Kaufman ◽  
R. D. Noebe

AbstractThe strain aging behavior of three polycrystalline NiAl alloys has been investigated at temperatures between 300 and 1200 K. Yield stress plateaus, yield stress transients upon a tenfold increase in strain rate, work hardening peaks, and dips in the strain rate sensitivity (SRS) have been observed between 700 and 800 K. These observations are indicative of dynamic strain aging (DSA) and are discussed in terms of conventional strain aging theories.


The mechanical properties of pure iron single crystals and of polycrystalline specimens of a zone-refined iron have been measured in compression over the temperature and strain rate ranges 2.2 to 293 °K and 7 x 10 -7 to 7 x 10 -3 s -1 respectively. Various yield stress parameters were determined as functions of both temperature and strain rate, and the reversible changes in flow stress produced by isothermal changes of strain rate or by changes of temperature at constant strain rate were also measured as functions of temperature, strain and strain rate. Both the temperature variation of the flow stress and the strain rate sensitivity of the flow stress were generally identical for the single crystals ( ca. 0.005/M carbon) and the polycrystalline specimens ( ca. 9/M carbon). At low temperatures, the temperature dependence of the yield stress was smaller than that of the flow stress at high strains, probably because of the effects of mechanical twinning, but once again the behaviour of single and polycrystalline specimens was very similar. Below 10 °K, both the flow stress and the extrapolated yield stress were independent of temperature. The results show that macroscopic yielding and flow at low temperatures are both governed by the same deformation mechanism, which is not very impurity sensitive, even in the very low carbon range covered by the experiments. The flow stress near 0 °K is ca. 5.8 x 10 -3 u where [i is the shear modulus. On the basis of a model for thermally activated flow, the activation volume at low temperatures (high stresses) is found to be ca. 5 b 3 . The exponent in the empirical power law for the dislocation velocity against stress relation is ca. 3 near room temperature, but becomes quite large at low temperatures. The results indicate that macroscopic deformation at low temperatures is governed by some kind of lattice frictional stress (Peierls-Nabarro force) acting on dislocations.


1996 ◽  
Vol 11 (6) ◽  
pp. 1433-1439 ◽  
Author(s):  
Anne Vilette ◽  
S. L. Kampe

Cubic (δ) bismuth oxide (Bi2O3) has been subjected to high temperature deformation over a wide range of temperatures and strain rates. Results indicate that bismuth oxide is essentially incapable of plastic deformation at temperatures below the monoclithic to cubic phase transformation which occurs at approximately 730 °C. Above the transformation temperature, however, Bi2O3 is extensively deformable. The variability of flow stress to temperature and strain rate has been quantified through the determination of phenomenological-based constitutive equations to describe its behavior at these high temperatures. Analysis of the so-determined deformation constants indicate an extremely strong sensitivity to strain rate and temperature, with values of the strain-rate sensitivity approaching values commonly cited as indicative of superplastic behavior.


1994 ◽  
Vol 364 ◽  
Author(s):  
S. S. Ezz ◽  
Y. Q. Sun ◽  
P. B. Hirsch

AbstractThe strain rate sensitivity ß of the flow stress τ is associated with workhardening and β=(δτ/δln ε) is proportional to the workhardening increment τh = τ - τy, where τy is the strain rate independent yield stress. The temperature dependence of β/τh reflects changes in the rate controlling mechanism. At intermediate and high temperatures, the hardening correlates with the density of [101] dislocations on (010). The nature of the local obstacles at room temperature is not established.


2007 ◽  
Vol 351 ◽  
pp. 65-69 ◽  
Author(s):  
Cun Zhu Nie ◽  
Jia Jun Gu ◽  
Jun Liang Liu ◽  
Di Zhang

The elevated temperature deformation and fracture behavior of an 10vol%B4CP/7039 aluminum matrix composite plate was investigated by uniaxial tensile tests at temperatures ranging from573 to 773 K and at initial strain rates from 1x10-1 to 1x10-4s-1.The strain rate sensitivity exponent was found to be approximately 0.1-0.15 which was below that of a superplastic material. A maximum elongation of 116% was obtained at an initial strain rate of 10-1 s-1 and at a temperature of 773 K.


1996 ◽  
Vol 460 ◽  
Author(s):  
Y. Q. Sun

ABSTRACTBased on the superkink model, an explanation is given in this paper for the small strain-rate sensitivity of the anomalous yield stress of Ni3Al. The yield stress is proposed to be the stress needed to destabilise the average superkinks and it varies inversely with superkink height. The yield stress is insensitive to the strain-rate because the superkink height is controlled by the rate at which the superkink widens and is not directly related with the superkink propagation speed.


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