scholarly journals Optimizing the energy bandwidth for transmission full-field X-ray microscopy experiments

2022 ◽  
Vol 29 (1) ◽  
Author(s):  
Malte Storm ◽  
Florian Döring ◽  
Shashidhara Marathe ◽  
Silvia Cipiccia ◽  
Christian David ◽  
...  

Full-field transmission X-ray microscopy (TXM) is a very potent high-resolution X-ray imaging technique. However, it is challenging to achieve fast acquisitions because of the limited efficiency of the optics. Using a broader energy bandwidth, for example using a multilayer monochromator, directly increases the flux in the experiment. The advantage of more counts needs to be weighed against a deterioration in achievable resolution because focusing optics show chromatic aberrations. This study presents theoretical considerations of how much the resolution is affected by an increase in bandwidth as well as measurements at different energy bandwidths (ΔE/E = 0.013%, 0.27%, 0.63%) and the impact on achievable resolution. It is shown that using a multilayer monochromator instead of a classical silicon double-crystal monochromator can increase the flux by an order of magnitude with only a limited effect on the resolution.

2001 ◽  
Vol 34 (4) ◽  
pp. 504-509 ◽  
Author(s):  
Z. Zhong ◽  
C. C. Kao ◽  
D. P. Siddons ◽  
J. B. Hastings

The ability of asymmetric Laue crystals to focus X-rays sagittally is demonstrated. The extent of such focusing is similar to that of sagittal focusing by a Bragg crystal, except for a factor related to the asymmetry angle. The anticlastic bending facilitates the use of inverse-Cauchois geometry in the meridional plane to provide better energy resolution and to increase the photon flux by an order of magnitude compared with traditional sagittal focusing with Bragg crystals. Furthermore, for sagittal focusing at X-ray energies above 30 keV, a Laue crystal is preferred to a Bragg crystal because the length of the beam's footprint on a Laue crystal, unlike on a Bragg crystal, is small and insensitive to energy. The conditions imposed on the asymmetry angle of the Laue crystal to achieve simultaneous sagittal focusing and inverse-Cauchois geometry in the meridional plane are derived for both single-crystal and double-crystal fixed-exit sagittally focusing monochromators.


1986 ◽  
Vol 47 (C8) ◽  
pp. C8-135-C8-137
Author(s):  
T. MURATA ◽  
T. MATSUKAWA ◽  
M. MORI ◽  
M. OBASHI ◽  
S.-I. NAO-E ◽  
...  

2012 ◽  
Vol 2012 ◽  
pp. 1-13 ◽  
Author(s):  
A. Teymurazyan ◽  
G. Pang

A Monte Carlo simulation was used to study imaging and dosimetric characteristics of a novel design of megavoltage (MV) X-ray detectors for radiotherapy applications. The new design uses Cerenkov effect to convert X-ray energy absorbed in optical fibres into light for MV X-ray imaging. The proposed detector consists of a matrix of optical fibres aligned with the incident X rays and coupled to an active matrix flat-panel imager (AMFPI) for image readout. Properties, such as modulation transfer function, detection quantum efficiency (DQE), and energy response of the detector, were investigated. It has been shown that the proposed detector can have a zero-frequency DQE more than an order of magnitude higher than that of current electronic portal imaging device (EPID) systems and yet a spatial resolution comparable to that of video-based EPIDs. The proposed detector is also less sensitive to scattered X rays from patients than current EPIDs.


2018 ◽  
Vol 74 (6) ◽  
pp. 673-680 ◽  
Author(s):  
V. G. Kohn

The article reports an accurate theory of X-ray coplanar multiple diffraction for an experimental setup that consists of a generic synchrotron radiation (SR) source, double-crystal monochromator (M) and slit (S). It is called for brevity the theory of X-ray coplanar multiple SRMS diffractometry. The theory takes into account the properties of synchrotron radiation as well as the features of diffraction of radiation in the monochromator crystals and the slit. It is shown that the angular and energy dependence (AED) of the sample reflectivity registered by a detector has the form of a convolution of the AED in the case of the monochromatic plane wave with the instrumental function which describes the angular and energy spectrum of radiation incident on the sample crystal. It is shown that such a scheme allows one to measure the rocking curves close to the case of the monochromatic incident plane wave, but only using the high-order reflections by monochromator crystals. The case of four-beam (220)(331)({\overline {11}}1) diffraction in Si is considered in detail.


Author(s):  
David Mascali ◽  
Eugenia Naselli ◽  
Richard Racz ◽  
Sándor Biri ◽  
Luigi Celona ◽  
...  

Abstract We hereby report the study of confinement and electron losses dynamics in the magnetic trap of an Electron Cyclotron Resonance Ion Source (ECRIS) using a special multi-diagnostic setup that has allowed the simultaneous collection of plasma radio-self-emission and X-ray images in the range 500 eV - 20 keV. Argon plasmas were generated in single and two close frequency heating (TCFH) modes. Evidences of turbulent regimes have been found: for stable and unstable configurations quantitative characterizations of the plasma radio self-emission have been carried out, then compared with local measurement of plasma energy content evaluated by X-ray imaging. This imaging method is the only one able to clearly separate X-ray radiation coming from the plasma from the one coming from the plasma chamber walls. X-ray imaging has been also supported and benchmarked by volumetric spectroscopy performed via SDD and HPGe detectors. The obtained results in terms of X-ray intensity signal coming from the plasma core and from the plasma chamber walls have permitted to estimate the average ratio: plasma vs. walls (i.e., plasma losses) as a function of input RF power and pumping wave frequency, showing an evident increase (above the experimental errors) of the intensity in the 2-20 keV energy range due to the plasma losses in case of unstable plasma. This ratio was well correlated with the strength of the instabilities, in single frequency heating (SFH) operation mode; in TCFH mode, under specific power balance conditions and frequency combinations, it was possible to damp the instabilities, thus the plasma losses were observed to decrease and a general reconfiguration of the spatial plasma structure occurred (the X-ray emission was more concentrated in the center of the plasma chamber). In the end, a simplified model has been used to simulate electron heating under different pumping frequencies, discussing the impact of velocity anisotropy vs. the onset of the instability, and the mechanism of particles diffusion in the velocity space in stable and unstable regimes.


1998 ◽  
Vol 69 (3) ◽  
pp. 1230-1235 ◽  
Author(s):  
C. S. Hwang ◽  
F. Y. Lin ◽  
Chih-Hao Lee ◽  
Kuan-Li Yu ◽  
C. H. Hsieh ◽  
...  

2010 ◽  
Vol 1 (MEDSI-6) ◽  
Author(s):  
A. Gambitta

A prototype of a new double crystal monochromator (DCM) has been designed and developed for the second crystallography beamline (XRD2) at ELETTRA. The new device has to cover the 8–35 keV X-ray range. Since the corresponding diffraction angles are quite small, the choice has been to design a DCM with a fixed distance between the two crystals. As a consequence, the output beam has a small vertical displacement during the scan. This movement is compensated by means of an upstream mask, vertically moving and cutting the input beam at different heights. The movement of the mask is driven by a mechanism linked to the primary rotation of crystals (self-compensation), without any additional motor and following the displacement law required for compensation. The principle, the mechanism and the general mechanical concept of the device will be described in this paper.


2018 ◽  
Vol 25 (5) ◽  
pp. 1541-1547 ◽  
Author(s):  
Jagannath ◽  
U. K. Goutam ◽  
R. K. Sharma ◽  
J. Singh ◽  
K. Dutta ◽  
...  

The Hard X-ray Photo-Electron Spectroscopy (HAXPES) beamline (PES-BL14), installed at the 1.5 T bending-magnet port at the Indian synchrotron (Indus-2), is now available to users. The beamline can be used for X-ray photo-emission electron spectroscopy measurements on solid samples. The PES beamline has an excitation energy range from 3 keV to 15 keV for increased bulk sensitivity. An in-house-developed double-crystal monochromator [Si (111)] and a platinum-coated X-ray mirror are used for the beam monochromatization and manipulation, respectively. This beamline is equipped with a high-energy (up to 15 keV) high-resolution (meV) hemispherical analyzer with a microchannel plate and CCD detector system with SpecsLab Prodigy and CasaXPS software. Additional user facilities include a thin-film laboratory for sample preparation and a workstation for on-site data processing. In this article, the design details of the beamline, other facilities and some recent scientific results are described.


2015 ◽  
Vol 22 (6) ◽  
pp. 1531-1539 ◽  
Author(s):  
A. K. Agrawal ◽  
B. Singh ◽  
Y. S. Kashyap ◽  
M. Shukla ◽  
P. S. Sarkar ◽  
...  

A full-field hard X-ray imaging beamline (BL-4) was designed, developed, installed and commissioned recently at the Indus-2 synchrotron radiation source at RRCAT, Indore, India. The bending-magnet beamline is operated in monochromatic and white beam mode. A variety of imaging techniques are implemented such as high-resolution radiography, propagation- and analyzer-based phase contrast imaging, real-time imaging, absorption and phase contrast tomographyetc. First experiments on propagation-based phase contrast imaging and micro-tomography are reported.


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