Effect of heat on microstructural, mechanical and electrochemical evaluation of tungsten inert gas welding of low-nickel ASS

2018 ◽  
Vol 65 (6) ◽  
pp. 605-615 ◽  
Author(s):  
Ankur V. Bansod ◽  
Awanikumar P. Patil ◽  
Sourabh Shukla

Purpose The purpose of the study is to evaluate Cr-Mn ASS weld using different heat inputs for its microstructure, mechanical properties and electrochemical behavior. The microstructural examination used optical and scanning electron microscopy. It was observed that ferrite content decreases with increasing heat input. The length of dendrites, inter-dendritic space and volume of lathy ferrite increase with increasing heat input. The increasing heat input caused grain coarsening near the fusion boundary and produced wider heat-affected zone (HAZ). It also decreases hardness and tensile strength. This is attributed to formation of more δ ferrite in the weld. The electrochemical evaluation suggested that the δ ferrite helps in improving the pitting potential in 3.5 per cent NaCl solution saturated with CO2. Whereas in 0.5-M H2SO4 + 0.003-M NaF solution, higher passivation current density was observed because of dissolution of dferrite. The interphase corrosion resistance decreased with increasing heat input. Design/methodology/approach The Cr-Mn austenitic stainless steel or low-nickel ASS was procured in form of 3-mm sheets in rolled condition. The tungsten inert gas welding was performed at three different heat inputs (100 A, 120 A and 140 A), argon as shielding gas with a flow rate of 15 L/min. Different welded regions were observed using optical microscope and scanning electron microscope. Electrochemicals test were performed in solutions containing 3.5 per cent NaCl with saturated CO2 solution and 0.5 M sulfuric acid + 0.003 M NaF at a scan rate of 0.1667 mV/s at room temperature (30 °C ± 1 °C) using a potentiostat. Findings The test steel Cr-Mn ASS is suitable with the selected electrode (308 L) and it produces no defects. Vermicular ferrite and lathy ferrite form in welds of various heat inputs. The increase in heat input reduces the formation of lathy ferrite. The width of HAZ and un-mixed zone increases with increase in heat input. The weld zone of low heat input (LHI) has the highest hardness and tensile strength because of higher δ ferrite content and small grain size in the weld zone. The hardness at high heat input (HHI) is found to be lowest because of grain coarsening in the weld. With increase in δ ferrite, the pitting resistance increases. In 0.5-M sulfuric acid + 0.003-M NaF, the increase in ferrite content reduces the passivation current density. Interphase corrosion resistance increases with increase in δ ferrite content as higher per cent degree of sensitization was observed in LHI welds as compared to medium heat input and HHI welds. Originality/value This work focuses on welding of ASS by tungsten inert gas welding at different heat inputs. Welding is a critical process for joining metals in most of the fabrication industries and proper heat input is required for getting desired microstructure in the weld metal. This would highly affect the strength and corrosion behavior of the alloy. This paper would give an understanding of how the change in heat input by tungsten inert gas welding affects the microstructural and corrosion behavior in the weld metal.

Author(s):  
Vijaya Kumar K. ◽  
N. Ramanaiah ◽  
N. Bhargava Rama Mohan Rao

The current study investigates the metallurgical, mechanical properties and weld morphology of AH36 marine grade steel (with a thickness of 8 mm) by activated-tungsten inert gas  (A-TIG) butt joints, with the application of different fluxes (MoO3, V2O5, and duplex of MoO3 and V2O5) at various process parameters. The welding speed was kept constant at 120 mm/min, and current varied from 160 A to 220 A uniformly to optimise process parameters to achieve desired mechanical properties, weld morphology, and lowest possible heat input. The study also focused on comparing tensile strength, impact strength, and microhardness, heat input during welding, weld bead depth and width between conventional TIG welding and activated flux TIG welding processes at various operation parameters. Tensile results reported that fracture occurs at the base region in ordinary TIG welding and the activated tungsten inert gas welding process. It was noticed that a higher depth to width ratio attained MoO3 and V2O5 duplex flux coated weldments. There is evidence that the depth of weld joints is enhanced because of stable arc, Marangoni effect, and arc constriction. Microhardness results reported that the fusion zone has a higher microhardness in the activated tungsten inert gas welding than the ordinary TIG welding. It was concluded that out of all fluxes, MoO3 and V2O5 duplex flux coating produce better butt welds of AH36 steel.


2014 ◽  
Vol 18 (sup2) ◽  
pp. S2-1074-S2-1080 ◽  
Author(s):  
R. Sihotang ◽  
P. Sung-Sang ◽  
B. Eung-Ryul

2021 ◽  
Vol 1035 ◽  
pp. 739-745
Author(s):  
Yan Fei Chen ◽  
Jin Xiang Zhang ◽  
Zheng Qiang Zhu

The 0.6 mm tantalum sheet was welded under argon atmosphere by Tungsten Inert Gas Welding (TIG) in order to obtain a welded joint with high-quality and high-reliability. Metalloscope, scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS) were applied to analyze the joint. The results showed that the grain size of the base metal which affected by the welding heat remained the original size or enlarged slightly to 40-70 μm. What’s more, the weld zone was found to be composed of two components with different oxidation degree. And the distribution of these two components was related to the protection atmosphere of the location. The fusion line of the two tantalum sheets was clear which means high welding quality.


2015 ◽  
Vol 32 (1) ◽  
pp. 25-31 ◽  
Author(s):  
N. Patil ◽  
N.B. Velhal ◽  
R. Pawar ◽  
Vijaya Puri

Purpose – The purpose of this article is to study the effect of ferrite content on electric, magnetic and microwave properties of screen-printed y(Ni0.4Co0.2Cd0.4Fe2O4) + (1 − y)Pb(Zr0.52Ti0.48)O3 (y = 0.0, 0.15, 0.30, 0.45, 1.0) thick films on alumina. Design/methodology/approach – Thick films of ferrite–ferroelectric composite on alumina substrate have been delineated using screen printing technique. The structural analysis was carried out using X-ray diffraction method and scanning electron microscopy. The DC electrical resistivity was measured using the two-probe method. The magnetic measurement was carried out using a vibrating sample magnetometer. Microwave absorption was studied in the 8-18 GHz frequency range by using the vector network analyzer (N5230A). The permittivity in the 8-18 GHz frequency range was measured by using voltage standing wave ratio slotted section method. Findings – The formation of two individual ferrite–ferroelectric phases in composite thick films was confirmed by the X-ray diffraction patterns. The scanning electron microscope morphologies show the growth of cobalt-substituted nickel cadmium ferrite grains which are well dispersed in lead zirconium titanate matrix. The DC electrical resistivity increases with increase in ferrite content and decreases with increase in temperature. The present ferrite shows ferromagnetic nature and it increases saturation magnetization and coercivity of the composite thick films. Tuning properties are observed in the Ku-band and broadband X-band microwave absorption is observed in the composite thick films. The imaginary part of permittivity increases with an increase in ferrite content, which increases microwave absorption. The real part of microwave permittivity varied from 17 to around 22 with an increase in ferrite content and it decreases with frequency. The microwave conductivity, which increases with an increase in ferrite content, reveals the loss of polaron conduction, which supports the dielectric loss in the microwave region. Originality/value – Electric, magnetic and microwave properties of screen-printed y(Ni0.4Co0.2Cd0.4Fe2O4) + (1 − y)Pb(Zr0.52Ti0.48)O3 (y = 0.0, 0.15, 0.30, 0.45, 1.0) composite thick films on alumina substrate is reported for the first time.


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