Experimental investigation on the tribological property of functionalized graphene lubricant against steel

2020 ◽  
Vol 72 (3) ◽  
pp. 307-314
Author(s):  
Yong Qian ◽  
Hongying Gong ◽  
Xiaoyun Zhao ◽  
Lei Cao ◽  
Weizhong Shi ◽  
...  

Purpose The purpose of this study is to corroborate the advanced tribological properties of graphene as a lubricant additive. Design/methodology/approach Different concentrations of functionalized graphene were coated on the substrate surface. Tribological properties of the graphene lubricants were carried out by ball-on-disk tribology tests. Wear mechanism of functionalized graphene was studied by observing wear scars on the substrate surface. Finally, the wear resistance of modified graphene was calculated by calculating and analyzing the applied experimental conditions and the obtained experimental data. Findings The best concentration of graphene lubricant is 0.5 wt.% which shows the best tribological performance. And the coefficient of friction is 0.08. Compared with the dry friction condition, the coefficient of friction and wear rate of best graphene lubricant decreased by 80% and 82%. Originality/value The formula of graphene lubricant is independently developed and works very well. Graphene lubricant can prevent the substrate from oxidation. The thickness of the graphene lubricant is about 4-7µm. The concept of anti-wear strength was introduced in this paper. When 0.5 Vol.% graphene was added, the anti-wear strength was greatly improved from 115.3 kg·mm-2 to 657.6 kg·mm-2. Peer review The peer review history for this article is available at: https://publons.com/publon/10.1108/ILT-08-2019-0344

2016 ◽  
Vol 68 (5) ◽  
pp. 577-585 ◽  
Author(s):  
Zhengfeng Cao ◽  
Yanqiu Xia ◽  
Xiangyu Ge

Purpose The purpose of this paper is to synthesize a new kind of conductive grease which possesses a prominent conductive capacity and good tribological properties. Design/methodology/approach A two-step method was used to prepare complex lithium-based grease. Ketjen black (KB), acetylene black (AB) and carbon black (CB) were characterized by transmission electron microscope and used as lubricant additives to prepare conductive greases. Conductive capacity was evaluated by a conductivity meter, a surface volume resistivity meter and a circuit resistance meter. Tribological properties were investigated by a reciprocating friction and wear tester (MFT-R4000). The worn surfaces were analyzed by a scanning electron microscope, Raman spectroscopy, energy-dispersive X-ray spectroscopy and X-ray photoelectron spectroscope. Findings The conductive grease prepared with KB has a prominent conductive capacity at room temperature, 100°C and 150°C. Further, this conductive grease also possesses better tribological properties than AB and KB greases. When the concentration of KB is 1.8 Wt.%, the coefficient of friction and wear width reduced by 11 and 14 per cent, respectively. Originality/value This work is a new application of nanometer KB as a lubricant additive in grease, which provides a direction for preparing conductive grease. The conductivity and tribology experiments have been carried out though the variation of experiment conductions.


2020 ◽  
Vol 72 (7) ◽  
pp. 851-856
Author(s):  
Zhengfeng Cao ◽  
Yanqiu Xia ◽  
Chuan Chen ◽  
Kai Zheng ◽  
Yi Zhang

Purpose This paper aims to explore polyaniline (PANI) as a lubricant additive to improve the anti-corrosion and tribological properties of ionic liquids (ILs) for actual applications. Design/methodology/approach ILs were synthesized by dissolving lithium salts in synthetic oil and were used as a base oil to prepare ILs-based greases. PANI was used as an additive. The tribological properties were investigated in detail and the anti-corrosion ability was also assessed via salt spray test. After friction test, the worn surfaces were characterized by scanning electron microscopy, Raman spectroscopy and X-ray photoelectron spectroscopy to analyze the lubrication mechanisms. Findings PANI not only reduces the corrosion but also improves the friction reduction and anti-wear abilities of the ILs-based greases. The analysis indicates that the protective films generated on the worn surfaces were responsible for the preferable anti-corrosion and tribological properties. Originality/value This paper provides an effective approach to improve the anti-corrosion and tribological properties of ILs for actual applications. Peer review The peer review history for this article is available at: https://publons.com/publon/10.1108/ILT-11-2019-0469/


2019 ◽  
Vol 72 (9) ◽  
pp. 1103-1108 ◽  
Author(s):  
Joao Luiz do Vale ◽  
Carlos Henrique da Silva ◽  
Giuseppe Pintaude

Purpose This paper aims to present a proposal for evaluating the coefficient of friction (COF), under a reciprocating test that considers the energy dissipated by the friction force. In addition, this new parameter is compared to average COF, which is often used to evaluate COF in reciprocating tests. Design/methodology/approach Samples of compacted graphite iron were extracted directly from an internal combustion engine block. The piston ring used was a nitrided martensitic stainless steel with an asymmetrical profile, and the lubricant oil was the SAE 30 CF, controlled at 40°C. Different testing conditions were carried out in a CETR-UMT-Bruker tribometer, varying loads between 25-125 N, frequencies between 1-12.5 Hz and track length between 3-10 mm. Three maps comparing the average COF and the energetic definition were built, allowing to discuss their similarities. Findings In general, both parameters had similarities especially for low frequencies and small tracks. However, for test conditions that imposed higher accelerations (i.e. longer track lengths and higher frequencies), the energetic COF (COFe) was lower than the average COF (COFa) and presented better agreement in Stribeck-like curves – independent on the experienced lubrication regime along the stroke. As the COFe can be interpreted as a weighted average of instantaneous COF in relation to in-track displacements, an immediate consequence is that instantaneous COF closest to mid-stroke is considered more significant. Furthermore, perturbations associated with the intrinsic accelerations of the movement test are minimized in the COFe formulation. Originality/value The energetic COF parameter (COFe) is presented and compared to the average COF. The new parameter presented less data dispersion and is attractive to evaluate the COF behavior in reciprocating tests, as its formulation minimizes perturbations associated with the intrinsic accelerations of the movement (mainly in the initial and final part of the track where the acceleration has its greatest magnitude). Peer review The peer review history for this article is available at: https://publons.com/publon/10.1108/ILT-08-2019-0324


2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Ting Wang ◽  
Hanfei Guo ◽  
Jianjun Qiao ◽  
Xiaoxue Liu ◽  
Zhixin Fan

PurposeTo address the lack of data in this field and determine the relationship between the coefficient of friction and the interference between locomotive wheels and axles, this study evaluates the theoretical relationship between the coefficient of friction and the interference under elastic deformation.Design/methodology/approachWhen using numerical analyses to study the mechanical state of the contacting components of the wheels and axle, the interference between the axle parts and the coefficient of friction between the axle parts are two important influencing factors. Currently, as the range of the coefficient of friction between the wheel and axle in interference remains unknown, it is generally considered that the coefficient of friction is only related to the materials of the friction pair; the relationship between the interference and the coefficient of friction is often neglected.FindingsA total of 520 press-fitting experiments were conducted for 130 sets of wheels and axles of the HXD2 locomotive with 4 types of interferences, in order to obtain the relationship between the coefficient of friction between the locomotive wheel and axle and the amount of interference. These results are expected to serve as a reference for selecting the coefficient of friction when designing axle structures with the rolling stock, research on the press-fitting process and evaluations of the fatigue life.Originality/valueThe study provides a basis for the selection of friction coefficient and interference amount in the design of locomotive wheels and axles.


2020 ◽  
Author(s):  
Alexey Vereschaka ◽  
Sergey Grigoriev ◽  
Vladimir Tabakov ◽  
Mars Migranov ◽  
Nikolay Sitnikov ◽  
...  

The chapter discusses the tribological properties of samples with multilayer composite nanostructured Ti-TiN-(Ti,Cr,Al,Si)N, Zr-ZrN-(Nb,Zr,Cr,Al)N, and Zr-ZrN-(Zr,Al,Si)N coatings, as well as Ti-TiN-(Ti,Al,Cr)N, with different values of the nanolayer period λ. The relationship between tribological parameters, a temperature varying within a range of 20–1000°C, and λ was investigated. The studies have found that the adhesion component of the coefficient of friction (COF) varies nonlinearly with a pronounced extremum depending on temperature. The value of λ has a noticeable influence on the tribological properties of the coatings, and the nature of the mentioned influence depends on temperature. The tests found that for the coatings with all studied values of λ, an increase in temperature first caused an increase and then a decrease in COF.


2003 ◽  
Vol 125 (3) ◽  
pp. 661-669 ◽  
Author(s):  
Masaya Kurokawa ◽  
Yoshitaka Uchiyama ◽  
Tomoaki Iwai ◽  
Susumu Nagai

Tribological properties of several kinds of polyoxymethylene (POM) composites were evaluated for the purpose of developing a polymeric tribomaterial especially suited for mating with aluminum parts having low surface hardness. POM composites containing small amounts of silicon carbide (SiC), POM/SiC; those containing a small amount of calcium octacosanonoate besides SiC, POM/SiC/Ca-OCA; and the one blended with 24 wt % of polytetrafluoroethylene, POM/PTFE(24); were injection-molded into pin specimens and their tribological properties were tested by means of a pin-on-disk type wear apparatus using an aluminum (A5056) mating disk in comparison with a 303 stainless steel (SUS303) disk. Evaluation was focused on observation of the sliding surfaces of the pin specimens and the mating disks by a scanning electron microscope and an optical microscope together with the measurement of surface roughness. In the case of mating against a SUS303 disk having high surface hardness, all pin specimens did not roughen the disk surfaces even after long time of rubbing. Only POM/PTFE(24) composite obviously made a transfer film on the disk surface, while the other composites made an extremely thin one on it. POM/SiC(0.1)/Ca-OCA(1) composite, containing SiC 0.1 wt. % and Ca-OCA 1 wt. %, was found to show the lowest coefficient of friction and the lowest wear rate forming extremely thin transfer film on the mating disk. On the other hand, against an A5056 disk which has lower surface hardness than that of SUS303 disk, unfilled POM and POM composites except POM/SiC(0.1)/Ca-OCA(1) composite roughened the disk surfaces. However, the sliding surface of the A5056 disk rubbed with POM/SiC(0.1)/Ca-OCA(1) composite was significantly smoother and that of the pin specimen was also quite smooth in comparison with other pin specimens. Further, when each POM composite was rubbed against the A5056 disk, formation of transfer film was not obvious on the disk surfaces. For POM/SiC(0.1)/Ca-OCA(1) composite, the wear rate was the lowest of all POM composites, and the coefficient of friction was as low level as 60 percent of that of unfilled POM, but slightly higher than that of POM/PTFE(24) composite. For POM/SiC(0.1)/Ca-OCA(1) composite, the nucleating effect of SiC and Ca-OCA, which accelerated the crystallization of POM during its injection molding to form a matrix containing fine spherulites, must have resulted in increasing the toughness of the matrix and lowering the wear rate. Also, the lubricant effect of Ca-OCA should have lowered the coefficient of friction of the same matrix for rubbing against aluminum mating disk. POM/SiC(0.1)/Ca-OCA(1) composite was concluded as an excellent tribomaterial for mating with aluminum parts.


Author(s):  
Takashi Nogi

Some tribological properties of an ionic liquid were investigated by using a pin-on-disc friction and wear tester. Due to running-in, the coefficient of friction of the ionic liquid decreased with time to a very low value of 0.02 which suggests that the lubrication regime was hydrodynamic at the end of the tests. Anti-wear performance of the ionic liquid was substantially comparable to a paraffin-based oil.


2020 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Wei Feng ◽  
Lei Yin ◽  
Yanfeng Han ◽  
Jiaxu Wang ◽  
Ke Xiao ◽  
...  

Purpose This paper aims to explore the possibility of converting the nitrile butadiene rubber (NBR) water-lubricated bearing material into a self-lubricating bearing material by the action of polytetrafluoroethylene (PTFE) particles and water lubrication. Design/methodology/approach A group of experimental studies was carried out on a ring-on-block friction test. The physical properties, tribological properties and interface structure of PTFE-NBR self-lubricating composites filled with different percentages of PTFE particles were investigated. Findings The experimental results indicated that the reduction in friction and wear is a result of the formation of the lubricating film on the surface of the composites. The lubricating film was formed of a large amount of PTFE particles continuously supplied under water lubrication conditions and the PTFE particles here can greatly enhance the load capacity and lubrication performance. Originality/value In this study, the tribological properties of PTFE particles added to the NBR water-lubricated bearing materials under water lubrication were investigated experimentally, and the research was carried out by a ring-on-block friction test. It is believed that this study can provide some guidance for the application of PTFE-NBR self-lubricating. Peer review The peer review history for this article is available at: https://publons.com/publon/10.1108/ILT-05-2020-0187/


2020 ◽  
Vol 72 (9) ◽  
pp. 1109-1116
Author(s):  
Crislaine da Cruz ◽  
Ivan Mathias ◽  
Mariza Veiga Senk ◽  
Gelson Biscaia de Souza ◽  
Francisco Carlos Serbena

Purpose Lithium disilicate glass-ceramics (LS2 GC) are widely used as dental prosthetics and dental restorations. Based LS2 GC have hardness and translucency similar to that of natural teeth. This study aims to investigate the tribological features of LS2 GC with crystalline volume fraction of 64% and different crystal sizes from 8 µm to 34 µm for different counterparts. Design/methodology/approach The tribological behavior was investigated using a pin-on-disc tribometer with alumina and tungsten carbide (WC) spheres, applied load of 5 N and sliding speed of 5 cm/s at normal conditions. The coefficient of friction was measured continuously up to 10,000 sliding cycles. The specific wear rate was calculated from tribological and profile measurements. The wear mechanism was investigated by surface morphology analysis. Findings The coefficient of friction during running-in varied from 0.8 to 1.0 for the alumina counterpart, because of severe wear. Afterwards, it reduced and reached a stationary regime, characterized by a mild wear regime and the formation of a tribolayer formed by the debris. For the WC counterpart, the coefficient of friction curves increased initially with sliding cycles up to a stationary regime. The samples tested against WC presented the lowest specific wear rate (k), and no variation of wear rate with crystal size was observed. For samples tested against the alumina, crystallization and crystal size increased the wear resistance. Originality/value This study evaluated the effect of different counterfaces on the tribological properties of the LS2 GC, an important glass-ceramic base for many dental prosthetics and dental restorations, discussing results in light of the contact mechanics. Different specific wear rates, wear regimes and dependence on the glass-ceramic microstructure were observed depending on the counterpart. Peer review The peer review history for this article is available at: https://publons.com/publon/10.1108/ILT-08-2019-0352/


Tribologia ◽  
2019 ◽  
Vol 285 (3) ◽  
pp. 79-87 ◽  
Author(s):  
Jerzy MYALSKI ◽  
Andrzej Posmyk ◽  
Bartosz HEKNER ◽  
Marcin GODZIERZ

Carbon with an amorphous structure was used as a component to modify the tribological properties of engineering plastics. Its construction allows the formation of carbon-based wear products during friction, adhesively bonded to the surface of cooperating machine parts, acting as a solid lubricant. The work compares the tribological properties of two groups of composites with an aluminium alloy matrix in which glassy carbon appeared in the form of particles and an open cell foam fulfilling the role of strengthening the matrix. The use of spatial structures of reinforcement provides, in comparison with the strengthening of particles, homogeneity of carbon distribution in the entire volume of the composite. The tests carried out on a pin-disc tester showed that the use of spatial carbon structures in the composite ensures a greater coefficient of friction stability than when reinforcing with particles, and the coefficient of friction with a small proportion of carbon foams (about 1 wt%) is comparable with the coefficient of friction in the contact with composites containing 5-10% carbon particles in granular form.


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