Effect of crystal size on the tribological properties of lithium disilicate glass-ceramics sliding against alumina and tungsten carbide spheres

2020 ◽  
Vol 72 (9) ◽  
pp. 1109-1116
Author(s):  
Crislaine da Cruz ◽  
Ivan Mathias ◽  
Mariza Veiga Senk ◽  
Gelson Biscaia de Souza ◽  
Francisco Carlos Serbena

Purpose Lithium disilicate glass-ceramics (LS2 GC) are widely used as dental prosthetics and dental restorations. Based LS2 GC have hardness and translucency similar to that of natural teeth. This study aims to investigate the tribological features of LS2 GC with crystalline volume fraction of 64% and different crystal sizes from 8 µm to 34 µm for different counterparts. Design/methodology/approach The tribological behavior was investigated using a pin-on-disc tribometer with alumina and tungsten carbide (WC) spheres, applied load of 5 N and sliding speed of 5 cm/s at normal conditions. The coefficient of friction was measured continuously up to 10,000 sliding cycles. The specific wear rate was calculated from tribological and profile measurements. The wear mechanism was investigated by surface morphology analysis. Findings The coefficient of friction during running-in varied from 0.8 to 1.0 for the alumina counterpart, because of severe wear. Afterwards, it reduced and reached a stationary regime, characterized by a mild wear regime and the formation of a tribolayer formed by the debris. For the WC counterpart, the coefficient of friction curves increased initially with sliding cycles up to a stationary regime. The samples tested against WC presented the lowest specific wear rate (k), and no variation of wear rate with crystal size was observed. For samples tested against the alumina, crystallization and crystal size increased the wear resistance. Originality/value This study evaluated the effect of different counterfaces on the tribological properties of the LS2 GC, an important glass-ceramic base for many dental prosthetics and dental restorations, discussing results in light of the contact mechanics. Different specific wear rates, wear regimes and dependence on the glass-ceramic microstructure were observed depending on the counterpart. Peer review The peer review history for this article is available at: https://publons.com/publon/10.1108/ILT-08-2019-0352/

2018 ◽  
Vol 70 (3) ◽  
pp. 506-511 ◽  
Author(s):  
S. Shankar ◽  
M. Manikandan ◽  
G. Raja

Purpose The decrease in availability of mineral oils and their environmental hazards created the need to search for alternate bio-based oils. The aim of this study is to investigate the friction and wear characteristics of kapok (Ceiba pentandra) oil as a bio-lubricant. Design/methodology/approach The wear and friction characteristics between steel-steel contact under lubrication were found using a pin-on-disk tribometer under different loads and sliding speeds, respectively. The corrosion and oxidation stability of the test lubricants were also analyzed. The worn surfaces of the specimen are analyzed with the help of an optical microscope. The obtained results were compared with palm oil and mineral oil (SAE20W 40). Findings From the investigation, it is found that the kapok oil possess a lower coefficient of friction and wear rate than palm and mineral oil. It is also found that the coefficient of friction varies proportionally and the wear rate varies inversely with the sliding speed as expected. Originality/value The present results confirm that the kapok oil can be used as an alternative lubricant to reduce the demand for mineral-based oil lubricants.


Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4217
Author(s):  
Üsame Ali Usca ◽  
Mahir Uzun ◽  
Mustafa Kuntoğlu ◽  
Serhat Şap ◽  
Khaled Giasin ◽  
...  

Tribological properties of engineering components are a key issue due to their effect on the operational performance factors such as wear, surface characteristics, service life and in situ behavior. Thus, for better component quality, process parameters have major importance, especially for metal matrix composites (MMCs), which are a special class of materials used in a wide range of engineering applications including but not limited to structural, automotive and aeronautics. This paper deals with the tribological behavior of Cu-B-CrC composites (Cu-main matrix, B-CrC-reinforcement by 0, 2.5, 5 and 7.5 wt.%). The tribological characteristics investigated in this study are the coefficient of friction, wear rate and weight loss. For this purpose, four levels of sliding distance (1000, 1500, 2000 and 2500 m) and four levels of applied load (10, 15, 20 and 25 N) were used. In addition, two levels of sliding velocity (1 and 1.5 m/s), two levels of sintering time (1 and 2 h) and two sintering temperatures (1000 and 1050 °C) were used. Taguchi’s L16 orthogonal array was used to statistically analyze the aforementioned input parameters and to determine their best levels which give the desired values for the analyzed tribological characteristics. The results were analyzed by statistical analysis, optimization and 3D surface plots. Accordingly, it was determined that the most effective factor for wear rate, weight loss and friction coefficients is the contribution rate. According to signal-to-noise ratios, optimum solutions can be sorted as: the highest levels of parameters except for applied load and reinforcement ratio (2500 m, 10 N, 1.5 m/s, 2 h, 1050 °C and 0 wt.%) for wear rate, certain levels of all parameters (1000 m, 10 N, 1.5 m/s, 2 h, 1050 °C and 2.5 wt.%) for weight loss and 1000 m, 15 N, 1 m/s, 1 h, 1000 °C and 0 wt.% for the coefficient of friction. The comprehensive analysis of findings has practical significance and provides valuable information for a composite material from the production phase to the actual working conditions.


2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Ting Wang ◽  
Hanfei Guo ◽  
Jianjun Qiao ◽  
Xiaoxue Liu ◽  
Zhixin Fan

PurposeTo address the lack of data in this field and determine the relationship between the coefficient of friction and the interference between locomotive wheels and axles, this study evaluates the theoretical relationship between the coefficient of friction and the interference under elastic deformation.Design/methodology/approachWhen using numerical analyses to study the mechanical state of the contacting components of the wheels and axle, the interference between the axle parts and the coefficient of friction between the axle parts are two important influencing factors. Currently, as the range of the coefficient of friction between the wheel and axle in interference remains unknown, it is generally considered that the coefficient of friction is only related to the materials of the friction pair; the relationship between the interference and the coefficient of friction is often neglected.FindingsA total of 520 press-fitting experiments were conducted for 130 sets of wheels and axles of the HXD2 locomotive with 4 types of interferences, in order to obtain the relationship between the coefficient of friction between the locomotive wheel and axle and the amount of interference. These results are expected to serve as a reference for selecting the coefficient of friction when designing axle structures with the rolling stock, research on the press-fitting process and evaluations of the fatigue life.Originality/valueThe study provides a basis for the selection of friction coefficient and interference amount in the design of locomotive wheels and axles.


2008 ◽  
Vol 396-398 ◽  
pp. 153-156 ◽  
Author(s):  
Xanthippi Chatzistavrou ◽  
E. Hatzistavrou ◽  
Nikolaos Kantiranis ◽  
Lambrini Papadopoulou ◽  
Eleana Kontonasaki ◽  
...  

The aim of this study was the fabrication using a sol-gel technique of a new glass-ceramic with potential use in dental applications. The characterization of the composition and microstructural properties of the produced material confirmed the similarity between the new sol-gel derived glass-ceramic and a commercial leucite based fluorapatite dental glass-ceramic. The produced material has potential application in dental restorations and it is expected to exhibit better control of composition, microstructure and properties due to the intrinsic advantages of the sol-gel preparation method.


2003 ◽  
Vol 125 (3) ◽  
pp. 661-669 ◽  
Author(s):  
Masaya Kurokawa ◽  
Yoshitaka Uchiyama ◽  
Tomoaki Iwai ◽  
Susumu Nagai

Tribological properties of several kinds of polyoxymethylene (POM) composites were evaluated for the purpose of developing a polymeric tribomaterial especially suited for mating with aluminum parts having low surface hardness. POM composites containing small amounts of silicon carbide (SiC), POM/SiC; those containing a small amount of calcium octacosanonoate besides SiC, POM/SiC/Ca-OCA; and the one blended with 24 wt % of polytetrafluoroethylene, POM/PTFE(24); were injection-molded into pin specimens and their tribological properties were tested by means of a pin-on-disk type wear apparatus using an aluminum (A5056) mating disk in comparison with a 303 stainless steel (SUS303) disk. Evaluation was focused on observation of the sliding surfaces of the pin specimens and the mating disks by a scanning electron microscope and an optical microscope together with the measurement of surface roughness. In the case of mating against a SUS303 disk having high surface hardness, all pin specimens did not roughen the disk surfaces even after long time of rubbing. Only POM/PTFE(24) composite obviously made a transfer film on the disk surface, while the other composites made an extremely thin one on it. POM/SiC(0.1)/Ca-OCA(1) composite, containing SiC 0.1 wt. % and Ca-OCA 1 wt. %, was found to show the lowest coefficient of friction and the lowest wear rate forming extremely thin transfer film on the mating disk. On the other hand, against an A5056 disk which has lower surface hardness than that of SUS303 disk, unfilled POM and POM composites except POM/SiC(0.1)/Ca-OCA(1) composite roughened the disk surfaces. However, the sliding surface of the A5056 disk rubbed with POM/SiC(0.1)/Ca-OCA(1) composite was significantly smoother and that of the pin specimen was also quite smooth in comparison with other pin specimens. Further, when each POM composite was rubbed against the A5056 disk, formation of transfer film was not obvious on the disk surfaces. For POM/SiC(0.1)/Ca-OCA(1) composite, the wear rate was the lowest of all POM composites, and the coefficient of friction was as low level as 60 percent of that of unfilled POM, but slightly higher than that of POM/PTFE(24) composite. For POM/SiC(0.1)/Ca-OCA(1) composite, the nucleating effect of SiC and Ca-OCA, which accelerated the crystallization of POM during its injection molding to form a matrix containing fine spherulites, must have resulted in increasing the toughness of the matrix and lowering the wear rate. Also, the lubricant effect of Ca-OCA should have lowered the coefficient of friction of the same matrix for rubbing against aluminum mating disk. POM/SiC(0.1)/Ca-OCA(1) composite was concluded as an excellent tribomaterial for mating with aluminum parts.


2013 ◽  
Vol 834-836 ◽  
pp. 309-314
Author(s):  
Zi Fan Xiao ◽  
Jin Shu Cheng ◽  
Jun Xie

A glass-ceramic belonging to the CaO-Al2O3-SiO2(CAS) system with different composition of spodumene and doping the Li2O with amount between 0~2.5 % (mass fraction) were prepared by onestage heat treatment, under sintering and crystallization temperature at 1120 °C for two hours. In this paper, differential thermal analysis, X-ray diffraction, scanning electron microscopy, energy dispersive spectrometry and bending strength test were employed to investigate the microstructure and properties of all samples. β-wollastonite crystals were identified as the major crystalline phases, and increasing Li2O was found to be benefit for the crystallization and tiny crystalline phases remelting, resulting in the content of major crystalline phases increased first and then decreased with increasing the expense of spodumene. Meanwhile, the crystal size can be positively related with the content of Li2O. The preferable admixed dosage of spodumene can be obtained, besides the strength of glass-ceramics can be more than 90 MPa.


2020 ◽  
Vol 26 (4) ◽  
pp. 765-776 ◽  
Author(s):  
Gurminder Singh ◽  
Pulak Mohan Pandey

Purpose The purpose of this study is to study the mechanical, tribological and electrical properties of the copper-graphene (Cu-Gn) composites fabricated by a novel rapid tooling technique consist of three-dimensional printing and ultrasonic-assisted pressureless sintering (UAPS). Design/methodology/approach Four different Cu-Gn compositions with 0.25, 0.5, 1 and 1.5 per cent of graphene were fabricated using an amalgamation of three-dimensional printing and UAPS. The polymer 3d printed parts were used to prepare mould cavity and later the UAPS process was used to sinter Cu-Gn powder to acquire free-form shape. The density, hardness, wear rate, coefficient of friction and electrical conductivity were evaluated for the different compositions of graphene and compared with the pure copper. Besides, the comparison was performed with the conventional method. Findings Cu-Gn composites revealed excellent wear properties due to higher hardness, and the lubrication provided by the graphene. The electrical conductivity of the fabricated Cu-Gn composites started increasing initially but decreased afterwards with increasing the content of graphene. The UAPS fabricated composites outperformed the conventional method manufactured samples with better properties such as density, hardness, wear rate, coefficient of friction and electrical conductivity due to homogeneous mixing of metal particles and graphene. Originality/value The fabrication of Cu-Gn composite freeform shapes was found to be difficult using conventional methods. The novel technique using a combination of polymer three-dimensional printing and UAPS as rapid tooling was introduced for the fabrication of freeform shapes of Cu-Gn composites and mechanical, tribological and electrical properties were studied. The method can be used to fabricate optimized complex Cu-Gn structures with improved wear and electrical applications.


2017 ◽  
Vol 25 (3) ◽  
pp. 193-198 ◽  
Author(s):  
A. Madhanagopal ◽  
S. Gopalakannan

This study determines the friction and the wear properties of the unidirectional glass epoxy composite with Gr, SiC TiO2 powder by using pin on disk apparatus. This tribological data is obtained in dry sliding condition for a constant sliding time of 30 minutes. Test specimens are prepared using hand lay-up process and by varying the different (2, 5, 7) percentage each of graphite and SiC, TiO2 particles addition for the combination of fiber and matrix. The tests are performed by varying the operating parameters of contact pressure (p) and velocity (v). The composites (2% 5%, and 7%) are worn by dry sliding at the steel counter face under ambient conditions. The coefficient of friction reaches maximum of 0.78 at 2 kg load, 2 m/s velocity with testing time duration of 24 min. whereas 5%, 7% sample shows the coefficient of friction 0.28, 0.25 respectively. The specific wear rate value drops to 0.79 (mm3/N-m×10−6) at 2 kg load at 2 m/s velocity for the 5% specimen. The maximum reduction in the specific wear rate at 3 kg load, 1m/s velocity is 32.7 percentages, 5.63 percentages for the 5,7 percentage specimen compared to 2% specimen for the graphite and SiC, TiO2 particle filled composite specimen respectively. The SEM images are also taken to support the results.


Author(s):  
S. W. E. Earles ◽  
D. G. Powell

Experiments have been conducted in a normal atmosphere using a 0·25-in diameter mild-steel pin specimen sliding on a 10-in diameter mild-steel disc. The ranges of normal force and speed are 0·5–10·4 lbf and 20–190 ft/s respectively. Initially the coefficient of friction is comparatively large, and the wear is of the severe metallic form. However, frictional heating causes rapid oxidation of the surfaces and, if the sliding distance is sufficient, the eventual retention of an oxide layer causes a rapid decrease in the coefficient of friction and the wear rate decreases by 3–4 orders of magnitude. At speeds above about 75 ft/s and loads below about 5 lbf the formation, after several hours' sliding, of a continuous oxide layer on the track causes a further reduction in the pin wear rate. At higher loads and/or lower speeds this track condition is not attained. At speeds of 75 ft/s and above there exists a critical load (the magnitude of which depends on speed) above which periodic removals of the surface film(s) occur producing metallic wear and high friction. However, the subsequent increase in oxidation allows conditions of mild wear to be re-established generally within a few seconds. The steady-state coefficient of friction has been observed to be a function of load1/2 × speed, and periodic surface breakdowns found to occur when load1/2 × speed exceeds 170 lbf1/2 ft/s, the frequency decreasing with increasing load or speed.


2001 ◽  
Vol 16 (12) ◽  
pp. 3567-3574 ◽  
Author(s):  
Xiaoling Zhang ◽  
W. Lauwerens ◽  
L. Stals ◽  
Jiawen He ◽  
J-P. Celis

The fretting wear of sulphur-deficient MoSx coatings with different crystallographic orientations has been investigated in ambient air of controlled relative humidity. The coefficient of friction and the wear rate of MoSx coatings sliding against corundum depend not only on fretting parameters like contact stress, fretting frequency, and relative humidity, but also strongly on the crystallographic orientation of the coatings. For randomly oriented MoSx coatings, the coefficient of friction and the wear rate increased significantly with increasing relative humidity. In contrast, basal-oriented MoSx coatings were less sensitive to relative humidity. The coefficient of friction of both types of MoSx coatings decreased on sliding against corundum with increasing contact stress and decreasing fretting frequency. A correlation between dissipated energy and wear volume is proposed. This approach allows detection in a simple way of differences in fretting wear resistance between random- and basal-oriented MoSx coatings tested in ambient air of different relative humidity.


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