Densification behavior of 316L-NiB stainless steel powder and surface morphology during selective laser melting process using pulsed Nd:YAG laser

2019 ◽  
Vol 25 (1) ◽  
pp. 47-54 ◽  
Author(s):  
Jelena Stašić ◽  
Dušan Božić

Purpose This paper aims to report the production of 316L-1 Wt.% NiB cubes by using the selective laser melting (SLM) process. The laser used was pulsed, millisecond Nd:YAG system with maximum average power 100 W. Design/methodology/approach Densification under different processing conditions (pulse energy, average laser power, laser scan speed, powder layer thickness, pulse frequency) was investigated. Morphology, macro and microstructure of laser melted samples were characterized by digital camera images and by scanning electron microscope. Density of the cubes was determined by Archimedes method in water. Vickers microhardness of samples was determined under the load of 25 g. Corrosion behavior of 316L and 316L-NiB samples was conducted in 5 per cent HCl solution at the testing temperature of 20°C during 240 h. Findings Using laser power of ∼60-70 W, lower beam overlap and powder layer thickness of 200 µm, 3D cubical samples were obtained with significant balling in individual layers and an overall porosity being around 30 per cent. By increasing laser power to ∼80 W, with higher beam overlap and lower powder layer thickness of 100 µm, SLM parts with no balling and the presence of small pores of up to 4 per cent (20 Hz) and 9 per cent (40 Hz) were obtained. With further increase of laser power to 90 W, overall porosity rose to around 12 per cent. The addition of 1 Wt.% NiB to stainless steel negligibly lowered its corrosion resistance in 5 per cent HCl solution. Originality/value A part from 316L stainless steel with balling-free structure and good density was successfully obtained through pulsed-SLM process with the aid of 1 Wt.% of NiB addition. Aside from significant influence on the improved structure of cubes, NiB had a favorable effect on microhardness values while practically not affecting the corrosion resistivity of the base material in an aggressive surrounding.

2020 ◽  
Vol 26 (5) ◽  
pp. 871-879 ◽  
Author(s):  
Haihua Wu ◽  
Junfeng Li ◽  
Zhengying Wei ◽  
Pei Wei

Purpose To fabricate a selective laser melting (SLM)-processed AlSi10Mg part with almost full density and free of any apparent pores, this study aims to investigate the effect of ambient argon pressure and laser scanning speed on the particles splash during the AlSi10Mg powder bed laser melting. Design/methodology/approach Based on the discrete element method (DEM), a 3D model of random distribution of powder particles was established, and the 3D free surface of SLM forming process was dynamically tracked by the volume of fluid, where a Gaussian laser beam acts as the energy source melting the powder bed. Through the numerical simulation and process experimental research, the effect of the applied laser power and scanning speed on the operating laser melting temperature was studied. Findings The process stability has a fundamental role in the porosity formation, which is process-dependent. The effect of the processing conditions on the process stability and the resultant forming defects were clarified. Research limitations/implications The results shows that the pores were the main defects present in the SLM-processed AlSi10Mg sample, which decreases the densification level of the sample. Practical implications The optimal processing parameters (argon pressure of 1,000 Pa, laser power of 180 W, scan speed of 1,000 mm/s, powder layer thickness of 35 µm and hatch spacing of 50 µm ) applied during laser melting can improve the quality of selective laser melting of AlSi10Mg, Social implications It can provide a technological support for 3D printing. Originality/value Based on the analysis of the pore and balling formation mechanisms, the optimal processing parameters have been obtained, which were argon pressure of 1,000 Pa, laser power of 180 W, scan speed of 1,000 mm/s, powder layer thickness of 35 µm and hatch spacing of 50 µm. Then, a near-fully dense sample free of any apparent pores on the cross-sectional microstructure was produced by SLM, wherein the relative density of the as-built samples is larger than 97.5%.


2011 ◽  
Vol 189-193 ◽  
pp. 3668-3671 ◽  
Author(s):  
Qing Song Wei ◽  
Xiao Zhao ◽  
Li Wang ◽  
Rui Di Li ◽  
Jie Liu ◽  
...  

Selective Laser Melting (SLM) can produce high-performance metal parts with complex structures. However, it’s difficult to control the processing parameters, because many factors involves. From the perspective of the molten pool, the study focuses on the effects of processing parameters, including scanning speed, laser power, scanning space, layer thickness, and scanning strategies, on the surface quality, the balling effect, the density of SLM parts, by conducting experiments of single track, single layer and block forming. The results show that the quality of the molten pool is affected by laser power and scanning speed. Scanning drove in the strategy of “jumping and turning”,a smooth surface and a less balling effect will be obtained. The thicker the powder layer is, the lower density will be obtained. The optimal parameters from series of experiments are: laser power of 98W; scanning speed of 90mm/s; scanning space of 0.07mm; layer thickness of 0.1mm; and scanning strategy of “jumping and turning”.


2017 ◽  
Vol 23 (6) ◽  
pp. 1146-1163 ◽  
Author(s):  
Karl P. Davidson ◽  
Sarat B. Singamneni

Purpose This paper aims to establish the microstructures and the process-structure relationships in duplex stainless steel powders consolidated by selective laser melting (SLM). Design/methodology/approach A priori data on energy density levels most appropriate to consolidation of duplex stainless steel powders through SLM served as the basis to converge on the laser settings. Experimental designs with varying laser power and scan speeds and test pieces generated allowed metallographic evaluations based on optical and scanning electron microscopy and electro backscatter diffraction analyses. Findings Duplex stainless steel powders are established for processing by SLM. However, the dynamic point heat source and associated transient thermal fields affect the microstructures to be predominantly ferritic, with grains elongated in the build direction. Austenite precipitated either at the grain boundaries or as Widmanstätten laths, whereas the crystallographic orientations and the grain growth are affected around the cavities. Considerable CrN precipitation is also evidenced. Originality/value Duplex stainless steels are relatively new candidates to be brought into the additive manufacturing realm. Considering the poor machinability and other difficulties, the overarching result indicating suitability of duplex powders by SLM is of considerable value to the industry. More significantly, the metallographic evaluation and results of the current research allowed further understanding of the material consolidation aspects and pave ways for fine tuning and establishment of the process-structure-property relationships for this important process-material combination.


Author(s):  
Diego Augusto de Moraes ◽  
Aleksander Czekanski

Selective Laser Melting (SLM) process is a Powder Bed Fusion (PBF) technique, which has shown significantly growth in the recent years. The demand for this process is justified by the versatility and ease in manufacturing the parts from 3D models as well for the increased complexity of engineered parts generated from topology or shape optimization. Automotive, aerospace, medical and aviation industries are taking great advantage of this process due the unique geometry characteristics found in the components. To enhance the benefits of SLM, a vital task is to analyze the laser power input impact on the temperature distribution through the powder bed, important for posterior residual stresses analysis. The Finite Element Method proposed in this study is a transient thermal model, able to predict temperature distribution through different sections of the powder bed when performing a single track of the laser scanning. Furthermore, the impact of the laser power input is carried out utilizing SS 304L, a low cost Stainless Steel alloy that can be employed in the SLM process, in order to determine the influence on the temperature distribution along the different cross sections.


Metals ◽  
2020 ◽  
Vol 10 (7) ◽  
pp. 877
Author(s):  
Cong Ma ◽  
Xianshun Wei ◽  
Biao Yan ◽  
Pengfei Yan

A single-layer three-dimensional model was created to simulate multi-channel scanning of AlSi25 powder in selective laser melting (SLM) by the finite element method. Thermal behaviors of laser power and scanning speed in the procedure of SLM AlSi25 powder were studied. With the increase of laser power, the maximum temperature, size and cooling rate of the molten pool increase, while the scanning speed decreases. For an expected SLM process, a perfect molten pool can be generated using process parameters of laser power of 180 W and a scanning speed of 200 mm/s. The pool is greater than the width of the scanning interval, the depth of the molten pool is close to scan powder layer thickness, the temperature of the molten pool is higher than the melting point temperature of the powder and the parameters of the width and depth are the highest. To confirm the accuracy of the simulation results of forecasting excellent process parameters, the SLM experiment of forming AlSi25 powder was carried out. The surface morphology of the printed sample is intact without holes and defects, and a satisfactory metallurgical bond between adjacent scanning channels and adjacent scanning layers was achieved. Therefore, the development of numerical simulation in this paper provides an effective method to obtain the best process parameters, which can be used as a choice to further improve SLM process parameters. In the future, metallographic technology can also be implemented to obtain the width-to-depth ratio of the SLM sample molten pool, enhancing the connection between experiment and theory.


2014 ◽  
Vol 20 (4) ◽  
pp. 301-310 ◽  
Author(s):  
Teodora Marcu ◽  
Cinzia Menapace ◽  
Luca Girardini ◽  
Dan Leordean ◽  
Catalin Popa

Purpose – The purpose of this paper was to obtain by means of selective laser melting and then characterize biocomposites of medical-grade Ti6Al7Nb with hydroxyapatite (2 and 5 vol.%) and without hydroxyapatite, as reference. Design/methodology/approach – Rectangular samples were manufactured with the same scanning strategy; the laser power was between 50 W and 200 W. Processed samples were analysed by means of optical microscopy, scanning electron microscopy and microhardness. Findings – The results showed that despite the very short processing times, hydroxyapatite decomposed and interacted with the base Ti6Al7Nb material. The decomposition degree was found to depend on the applied laser power. From the porosity and bulk microstructure point of view, the most appropriate materials for the purposed medical applications were Ti6Al7Nb with hydroxyapatite processed with a laser power of 50 W. Originality/value – The originality of the present work consists in the study of the behaviour and interaction of hydroxyapatite additive with the Ti6Al7Nb base powder under selective laser melting conditions, as depending on the applied laser power.


Author(s):  
Yong Deng ◽  
Zhongfa Mao ◽  
Nan Yang ◽  
Xiaodong Niu ◽  
Xiangdong Lu

Although the concept of additive manufacturing has been proposed for several decades, momentum of selective laser melting (SLM) is finally starting to build. In SLM, density and surface roughness, as the important quality indexes of SLMed parts, are dependent on the processing parameters. However, there are few studies on their collaborative optimization in SLM to obtain high relative density and low surface roughness simultaneously in the previous literature. In this work, the response surface method was adopted to study the influences of different processing parameters (laser power, scanning speed and hatch space) on density and surface roughness of 316L stainless steel parts fabricated by SLM. The statistical relationship model between processing parameters and manufacturing quality is established. A multi-objective collaborative optimization strategy considering both density and surface roughness is proposed. The experimental results show that the main effects of processing parameters on the density and surface roughness are similar. It is noted that the effects of the laser power and scanning speed on the above objective quality show highly significant, while hatch space behaves an insignificant impact. Based on the above optimization, 316L stainless steel parts with excellent surface roughness and relative density can be obtained by SLM with optimized processing parameters.


Friction ◽  
2020 ◽  
Author(s):  
Hongqin Ding ◽  
Qing Tang ◽  
Yi Zhu ◽  
Chao Zhang ◽  
Huayong Yang

AbstractCavitation erosion degrades the performance and reliability of hydraulic machinery. Selective laser melting (SLM) is a type of metal additive manufacturing technology that can fabricate metal parts directly and provide lightweight design in various industrial applications. However, the cavitation erosion behaviors of SLM-fabricated parts have rarely been studied. In this study, SLM 316L stainless steel samples were fabricated via SLM technology considering the scanning strategy, scanning speed, laser power, and build orientation. The effect of the process parameters on the cavitation erosion resistance of the SLM-fabricated 316L stainless steel samples was illustrated using an ultrasonic vibratory cavitation system. The mass loss and surface topography were employed to evaluate the surface cavitation damage of the SLM-fabricated 316L stainless steel samples after the cavitation test. The cavitation damage mechanism of the SLM-fabricated samples was discussed. The results show that the degree of cavitation damage of the sample fabricated via SLM with a few defects, anisotropic build direction, and columnar microstructure is significantly decreased. Defects such as pores, which are attributed to low laser power and high scanning speed, may severely aggravate the cavitation damage of the SLM-fabricated samples. The sample fabricated via SLM with a low laser power and exposure time exhibited the highest porosity and poor cavitation erosion resistance. The cellular structures are more prone to cavitation damage compared with the columnar structures. A sample with a high density of grain boundaries will severely suffer cavitation damage.


2015 ◽  
Vol 21 (4) ◽  
pp. 423-432 ◽  
Author(s):  
Luke N. Carter ◽  
Khamis Essa ◽  
Moataz M Attallah

Purpose – The purpose of this paper is to optimise the selective laser melting (SLM) process parameters for CMSX486 to produce a “void free” (fully consolidated) material, whilst reducing the cracking density to a minimum providing the best possible fabricated material for further post-processing. SLM of high temperature nickel base superalloys has had limited success due to the susceptibly of the material to solidification and reheat cracking. Design/methodology/approach – Samples of CMSX486 were fabricated by SLM. Statistical design of experiments (DOE) using the response surface method was used to generate an experimental design and investigate the influence of the key process parameters (laser power, scan speed, scan spacing and island size). A stereological technique was used to quantify the internal defects within the material, providing two measured responses: cracking density and void per cent. Findings – The analysis of variance (ANOVA) was used to determine the most significant process parameters and showed that laser power, scan speed and the interaction between the two are significant parameters when considering the cracking density. Laser power, scan speed, scan spacing and the interaction between power and speed, and speed and spacing were the significant factors when considering void per cent. The optimum setting of the process parameters that lead to minimum cracking density and void per cent was obtained. It was shown that the nominal energy density can be used to identify a threshold for the elimination of large voids; however, it does not correlate well to the formation of cracks within the material. To validate the statistical approach, samples were produced using the predicted optimum parameters in an attempt to validate the response surface model. The model showed good prediction of the void per cent; however, the cracking results showed a greater deviation from the predicted value. Originality/value – This is the first ever study on SLM of CMSX486. The paper shows that provided that the process parameters are optimised, SLM has the potential to provide a low-cost route for the small batch production of high temperature aerospace components.


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