scholarly journals Selective laser melting of Ti6Al7Nb with hydroxyapatite addition

2014 ◽  
Vol 20 (4) ◽  
pp. 301-310 ◽  
Author(s):  
Teodora Marcu ◽  
Cinzia Menapace ◽  
Luca Girardini ◽  
Dan Leordean ◽  
Catalin Popa

Purpose – The purpose of this paper was to obtain by means of selective laser melting and then characterize biocomposites of medical-grade Ti6Al7Nb with hydroxyapatite (2 and 5 vol.%) and without hydroxyapatite, as reference. Design/methodology/approach – Rectangular samples were manufactured with the same scanning strategy; the laser power was between 50 W and 200 W. Processed samples were analysed by means of optical microscopy, scanning electron microscopy and microhardness. Findings – The results showed that despite the very short processing times, hydroxyapatite decomposed and interacted with the base Ti6Al7Nb material. The decomposition degree was found to depend on the applied laser power. From the porosity and bulk microstructure point of view, the most appropriate materials for the purposed medical applications were Ti6Al7Nb with hydroxyapatite processed with a laser power of 50 W. Originality/value – The originality of the present work consists in the study of the behaviour and interaction of hydroxyapatite additive with the Ti6Al7Nb base powder under selective laser melting conditions, as depending on the applied laser power.

2016 ◽  
Vol 22 (1) ◽  
pp. 20-30 ◽  
Author(s):  
David Joguet ◽  
Sophie Costil ◽  
Hanlin Liao ◽  
Yoann Danlos

Purpose – The purpose of this paper consists in the optimization and understanding of the Selective Laser Melting (SLM) manufacturing process of biomaterials, such as T40 and CoCrMo, as scaffolds. Moreover, process optimization is also challenging, with regards to the huge number of parameters and their influence on the finished product. Design/methodology/approach – The paper opted for an exploratory study using Taguchi analysis method to precisely identify the most relevant parameters and justify the energy estimation. Findings – The study showed that SLM fits perfectly with the T40 and CoCrMo part manufacturing. This method allowed to have a complete overview of all the potential applications of SLM for implant manufacturing. Originality/value – With this research approach, the results may be generalized to other material and showed a good theoretical approach.


2020 ◽  
Vol 26 (5) ◽  
pp. 871-879 ◽  
Author(s):  
Haihua Wu ◽  
Junfeng Li ◽  
Zhengying Wei ◽  
Pei Wei

Purpose To fabricate a selective laser melting (SLM)-processed AlSi10Mg part with almost full density and free of any apparent pores, this study aims to investigate the effect of ambient argon pressure and laser scanning speed on the particles splash during the AlSi10Mg powder bed laser melting. Design/methodology/approach Based on the discrete element method (DEM), a 3D model of random distribution of powder particles was established, and the 3D free surface of SLM forming process was dynamically tracked by the volume of fluid, where a Gaussian laser beam acts as the energy source melting the powder bed. Through the numerical simulation and process experimental research, the effect of the applied laser power and scanning speed on the operating laser melting temperature was studied. Findings The process stability has a fundamental role in the porosity formation, which is process-dependent. The effect of the processing conditions on the process stability and the resultant forming defects were clarified. Research limitations/implications The results shows that the pores were the main defects present in the SLM-processed AlSi10Mg sample, which decreases the densification level of the sample. Practical implications The optimal processing parameters (argon pressure of 1,000 Pa, laser power of 180 W, scan speed of 1,000 mm/s, powder layer thickness of 35 µm and hatch spacing of 50 µm ) applied during laser melting can improve the quality of selective laser melting of AlSi10Mg, Social implications It can provide a technological support for 3D printing. Originality/value Based on the analysis of the pore and balling formation mechanisms, the optimal processing parameters have been obtained, which were argon pressure of 1,000 Pa, laser power of 180 W, scan speed of 1,000 mm/s, powder layer thickness of 35 µm and hatch spacing of 50 µm. Then, a near-fully dense sample free of any apparent pores on the cross-sectional microstructure was produced by SLM, wherein the relative density of the as-built samples is larger than 97.5%.


2016 ◽  
Vol 843 ◽  
pp. 284-288 ◽  
Author(s):  
P.A. Lykov ◽  
E.V. Safonov ◽  
A.M. Akhmedianov

In this work the selective laser melting (SLM) of pure copper powder was studied. Because of low laser radiation absorption and high thermal conductivity it is very difficult to organize stable SLM process for copper. Five 10x10x5 mm specimens were fabricated by using different process parameters (scanning speed, point distance, exposure time, scanning strategy). The structure of fabricated specimens was studied by scanning electron microscopy of polished cross-sections. The tensile test was carried out for SLM regime with the lowest porosity.


2020 ◽  
Vol 26 (10) ◽  
pp. 1713-1722
Author(s):  
Eduardo Cuesta ◽  
Braulio J. Alvarez ◽  
Pablo Zapico ◽  
Sara Giganto

Purpose This study aims to analyze the effect of the different common post-processes on the geometrical and dimensional accuracy of selective laser melting (SLM) parts. Design/methodology/approach An artefact has been designed including cubic features formed by planar surfaces orientated according to the machine axes, covering all the X-Y area of the working space. The artefact has been analyzed both geometrically (flatness, parallelism) and dimensionally (sizes, distances) from coordinate measuring machine measurement results at three stages, namely, as-built, after sand-blasting and after stress-relieving heat treatment. Findings Results from the SLM machine used in this study lead to smaller parts than the nominal ones. This effect depends on the direction of the evaluated dimension of the parts, i.e. X, Y or Z direction and is differently affected by the sandblasting post-process (average erosion ratio of 68, 54 and 9 µm, respectively), being practically unaltered by the HT applied after. Originality/value This paper shows the influence, from a geometric and dimensional point of view, of two of the most common post-processes used after producing SLM parts, such as sand-blasting and stress-relieving heat treatment, that have not been considered in previous research.


2015 ◽  
Vol 21 (4) ◽  
pp. 423-432 ◽  
Author(s):  
Luke N. Carter ◽  
Khamis Essa ◽  
Moataz M Attallah

Purpose – The purpose of this paper is to optimise the selective laser melting (SLM) process parameters for CMSX486 to produce a “void free” (fully consolidated) material, whilst reducing the cracking density to a minimum providing the best possible fabricated material for further post-processing. SLM of high temperature nickel base superalloys has had limited success due to the susceptibly of the material to solidification and reheat cracking. Design/methodology/approach – Samples of CMSX486 were fabricated by SLM. Statistical design of experiments (DOE) using the response surface method was used to generate an experimental design and investigate the influence of the key process parameters (laser power, scan speed, scan spacing and island size). A stereological technique was used to quantify the internal defects within the material, providing two measured responses: cracking density and void per cent. Findings – The analysis of variance (ANOVA) was used to determine the most significant process parameters and showed that laser power, scan speed and the interaction between the two are significant parameters when considering the cracking density. Laser power, scan speed, scan spacing and the interaction between power and speed, and speed and spacing were the significant factors when considering void per cent. The optimum setting of the process parameters that lead to minimum cracking density and void per cent was obtained. It was shown that the nominal energy density can be used to identify a threshold for the elimination of large voids; however, it does not correlate well to the formation of cracks within the material. To validate the statistical approach, samples were produced using the predicted optimum parameters in an attempt to validate the response surface model. The model showed good prediction of the void per cent; however, the cracking results showed a greater deviation from the predicted value. Originality/value – This is the first ever study on SLM of CMSX486. The paper shows that provided that the process parameters are optimised, SLM has the potential to provide a low-cost route for the small batch production of high temperature aerospace components.


2016 ◽  
Vol 22 (1) ◽  
pp. 115-122 ◽  
Author(s):  
Monica Mahesh Savalani ◽  
Jorge Martinez Pizarro

Purpose – The purpose of this paper is to investigate the effect of preheat and layer thickness in selective laser melting (SLM) of magnesium using pulse mode. Magnesium has been considered as a new generation of implant materials which are bioactive and biodegradable for orthopaedic applications. Design/methodology/approach – To produce optimal single magnesium tracks to compare the effect of layer thickness and preheat, different laser parameters were investigated. The analysis was made based on digital and electronic microscope images and mechanical measurements. Findings – Improvements in the magnesium tracks due to preheating were successfully achieved. The analysis shows better bonding to the surface. The preheated tracks present an improvement in quality surface: smoother and flatter surfaces are discovered for the low layer thicknesses. When the thickness increases, the surface was disrupted and presented high surface roughness values. These were attributed to the Marangoni convection. Originality/value – This study continues valuing the fabrication of magnesium with SLM. It shows the improvements of preheat and effect of different layer thicknesses on the part properties.


2019 ◽  
Vol 25 (1) ◽  
pp. 47-54 ◽  
Author(s):  
Jelena Stašić ◽  
Dušan Božić

Purpose This paper aims to report the production of 316L-1 Wt.% NiB cubes by using the selective laser melting (SLM) process. The laser used was pulsed, millisecond Nd:YAG system with maximum average power 100 W. Design/methodology/approach Densification under different processing conditions (pulse energy, average laser power, laser scan speed, powder layer thickness, pulse frequency) was investigated. Morphology, macro and microstructure of laser melted samples were characterized by digital camera images and by scanning electron microscope. Density of the cubes was determined by Archimedes method in water. Vickers microhardness of samples was determined under the load of 25 g. Corrosion behavior of 316L and 316L-NiB samples was conducted in 5 per cent HCl solution at the testing temperature of 20°C during 240 h. Findings Using laser power of ∼60-70 W, lower beam overlap and powder layer thickness of 200 µm, 3D cubical samples were obtained with significant balling in individual layers and an overall porosity being around 30 per cent. By increasing laser power to ∼80 W, with higher beam overlap and lower powder layer thickness of 100 µm, SLM parts with no balling and the presence of small pores of up to 4 per cent (20 Hz) and 9 per cent (40 Hz) were obtained. With further increase of laser power to 90 W, overall porosity rose to around 12 per cent. The addition of 1 Wt.% NiB to stainless steel negligibly lowered its corrosion resistance in 5 per cent HCl solution. Originality/value A part from 316L stainless steel with balling-free structure and good density was successfully obtained through pulsed-SLM process with the aid of 1 Wt.% of NiB addition. Aside from significant influence on the improved structure of cubes, NiB had a favorable effect on microhardness values while practically not affecting the corrosion resistivity of the base material in an aggressive surrounding.


2017 ◽  
Vol 31 (16-19) ◽  
pp. 1744015 ◽  
Author(s):  
Zeng Zheng ◽  
Lianfeng Wang ◽  
Biao Yan

Selective laser melting (SLM) was used to prepare 316L stainless steel parts and the effects of laser power on the microstructure and mechanical properties of the final products were studied. With increasing applied laser power, the defects of as-built parts were reduced greatly and the as-built parts presented a highest relative density of 99.1%. The tensile strength of samples was significantly improved from 321 ± 10 MPa to 722 ± 10 MPa. The microhardness was homogeneous; the residual stresses in the samples were tensile, which were higher in the section perpendicular to the laser scanning strategy. The probable reasons for this phenomenon were proposed.


2018 ◽  
Vol 24 (2) ◽  
pp. 333-341 ◽  
Author(s):  
Kai Zhang ◽  
Tingting Liu ◽  
Wenhe Liao ◽  
Changdong Zhang ◽  
Yishuai Yan ◽  
...  

Purpose The purpose of this paper is to obtain high-performance ceramics and enrich additive manufacturing of ceramic parts. Also, a new manufacturing technique based on slurry by selective laser melting (SLM) was studied, which has some significant advantages compared to indirect selective laser sintering of ceramic powders. Design/methodology/approach To study the effect of laser parameters on the surface morphology and melting state of pure Al2O3 ceramics, laser power varied between 100 and 200 W and scan speed varied between 60 and 90 mm/s. Findings Experimental results show that Al2O3 slurry melts completely when the laser power is about 200 W and the scanning speed is 90 mm/s. Surface quality cannot be improved effectively by changing the scanning speed. However, surface quality improves when the laser power is 200∼205 W and energy density is 889∼911 J/mm3. Thermocapillary convection was observed during SLM. By changing the temperature gradient, streak convection and flowing Bénard cells were obtained during SLM of Al2O3 slurry. Originality/value It is feasible to produce slurry ceramic parts without binders through SLM. Increasing the laser power is the most effective way to fully melt the ceramics. Complex thermocapillary convection was observed during this new process; it may be used to produce crystals.


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