Possibility of non-destructive detection of electrochemical migration in epoxy resin by the pulsed electroacoustic method

2009 ◽  
Author(s):  
M. Natsui ◽  
H. Asakawa ◽  
T. Tanaka ◽  
Y. Ohki ◽  
T. Maeno ◽  
...  
Keyword(s):  
Epoxy Resin ◽  
Electrochemical Migration ◽  
Non Destructive

Non-destructive Inspection Method for Defects in Epoxy Resin by using THz Wave

2020 ◽  
Author(s):  
Rieko Mizuuchi ◽  
Yuji Hisazato ◽  
Hiroaki Cho ◽  
Yusuke Nakamura ◽  
Yuichi Sumimoto ◽  
...  
Keyword(s):  
Epoxy Resin ◽  
Inspection Method ◽  
Thz Wave ◽  
Non Destructive

Preparation and Properties of MWCNTs/CF Reinforced Epoxy Resin Composite Patch

2012 ◽  
Vol 193-194 ◽  
pp. 363-367
Author(s):  
Wei Song ◽  
Chang Qing Li ◽  
Lin Lin ◽  
Yang Chen
Keyword(s):  
Epoxy Resin ◽  
Resin Composite ◽  
High Heat ◽  
Composite Patch ◽  
Epoxy Resin Composite ◽  
Melt Impregnation ◽  
Carbon Nano Tubes ◽  
Interlaminar Shear ◽  
Non Destructive ◽  
Hot Melt

Multi-walled carbon nano-tubes and carbon fiber reinforced epoxy resin (MWCNTs/CF/EP) composite patch was prepared by the route of hot-melt impregnation. The results of the mechanical properties shown that adding MWCNTs had made the tensile strength and interlaminar shear strength increased by 9.79% and 3.1%, separatively. It was detected using the ultrasonic non-destructive technique that the composite patch had a good interlaminar combination with no defects as obvious resin enrichment or insufficient gel content except for some slight stratification phenomenon in few parts. The high heat-resistance obtained by TG.

Methods of Infrared Non-Destructive Techniques: Review and Experimental Studies

2013 ◽  
Vol 542 ◽  
pp. 131-141 ◽  
Author(s):  
Przemysław D. Pastuszak ◽  
Aleksander Muc ◽  
Marek Barski
Keyword(s):  
Epoxy Resin ◽  
Experimental Analysis ◽  
Experimental Studies ◽  
Non Destructive ◽  
Non Destructive Techniques

The first part of the paper is devoted to presentation and discussion of the capabilities, advantages and limitations of infrared non-destructive techniques (IR NDT). Then, the results of experimental analysis performed by testing several specimens made of woven glass epoxy resin and containing artificial delamination in the form of square PTFE foil are presented.

scholarly journals DESIGN, ANALYSIS AND MANUFACTURING OF AXLE SHAFT BY ALTERNATE MATERIAL

2020 ◽  
Vol 5 (12) ◽  
pp. 200-205
Author(s):  
Kulkarni Vipul V. ◽  
Ghodake Arvind P.
Keyword(s):  
Mechanical Properties ◽  
Composite Materials ◽  
Glass Fiber ◽  
Epoxy Resin ◽  
Strength Ratio ◽  
Conventional Steel ◽  
Low Weight ◽  
Running Cost ◽  
Two Wheeler ◽  
Non Destructive

This work focuses the running inconvenient weight and the weight to strength ratio of the components of the vehicle as the weight directly affects on the mileage and running cost so this is the to replace the current material by low weight material without harming the safety. In this work the axle shaft is designed and manufactured by alternate material i.e. glass fiber and epoxy resin, the objective is to replace the all components of vehicle but the representative basis is the axle of the two wheeler. The glass fiber and epoxy resin having additional properties as they are composite materials. The composite materials i.e. composition of the more materials having properties of the all materials. The composite axle of is compared with conventional steel axle under different mechanical testing destructive and non-destructive tests with evaluating of different mechanical properties such as tensile strength, crack free structure by using appropriate experimental techniques.

Ultrastructural investigation of spontaneous pituitary gonadotroph cell adenomas in aging Sprague-Dawley rats

1983 ◽  
Vol 41 ◽  
pp. 702-703
Author(s):  
D. J. McComb ◽  
J. Beri ◽  
F. Zak ◽  
K. Kovacs
Keyword(s):  
Electron Microscopy ◽  
Animal Model ◽  
Epoxy Resin ◽  
Immunoelectron Microscopy ◽  
Tumor Type ◽  
Gonadal Function ◽  
Sprague Dawley ◽  
Male And Female ◽  
Reticulin Fibers ◽  
Sprague Dawley Rats

Gonadotroph cell adenomas of the pituitary are infrequent in human patients and are not invariably associated with altered gonadal function. To date, no animal model of this tumor type exists. Herein, we describe spontaneous gonadotroph cell adenomas in old male and female Sprague-Dawley rats by histology, immunocytology and electron microscopy.The material consisted of the pituitaries of 27 male and 38 female Sprague Dawley rats, all 26 months of age or older, removed at routine autopsy. Sections of formal in-fixed, paraffin-embedded tissue were stained with hematoxylin-phloxine-saffron (HPS), the PAS method and the Gordon-Sweet technique for the demonstration of reticulin fibers. For immunostaining, sections were exposed to anti-rat β-LH, anti-ratβ-TSH, anti-rat PRL, anti-rat GH and anti-rat ACTH 1-39. For electron microscopy, tissue was fixed in 2.5% glutaraldehyde, postfixed in 1% OsO4 and embedded in epoxy-resin. Tissue fixed in 10% formalin, embedded in epoxy resin without osmification, was used for immunoelectron microscopy.

Surface Structure in Microtomed Sections Caused by Glass and Diamond Knives

1971 ◽  
Vol 29 ◽  
pp. 456-457
Author(s):  
J. Temple Black ◽  
William G. Boldosser
Keyword(s):  
Plastic Deformation ◽  
Epoxy Resin ◽  
Carbon Coating ◽  
Surface Damage ◽  
Body Angle ◽  
Normal Manner ◽  
Bottom Side ◽  
Cutting Direction ◽  
Made In ◽  
Diamond Knife

Ultramicrotomy produces plastic deformation in the surfaces of microtomed TEM specimens which can not generally be observed unless special preparations are made. In this study, a typical biological composite of tissue (infundibular thoracic attachment) infiltrated in the normal manner with an embedding epoxy resin (Epon 812 in a 60/40 mixture) was microtomed with glass and diamond knives, both with 45 degree body angle. Sectioning was done in Portor Blum Mt-2 and Mt-1 microtomes. Sections were collected on formvar coated grids so that both the top side and the bottom side of the sections could be examined. Sections were then placed in a vacuum evaporator and self-shadowed with carbon. Some were chromium shadowed at a 30 degree angle. The sections were then examined in a Phillips 300 TEM at 60kv.Carbon coating (C) or carbon coating with chrom shadowing (C-Ch) makes in effect, single stage replicas of the surfaces of the sections and thus allows the damage in the surfaces to be observable in the TEM. Figure 1 (see key to figures) shows the bottom side of a diamond knife section, carbon self-shadowed and chrom shadowed perpendicular to the cutting direction. Very fine knife marks and surface damage can be observed.

Epoxy Resin Embedment

1968 ◽  
Vol 26 ◽  
pp. 100-101
Author(s):  
J. G. Adams ◽  
M. M. Campbell ◽  
H. Thomas ◽  
J. J. Ghldonl
Keyword(s):  
Electron Microscopy ◽  
Electron Beam ◽  
Epoxy Resin ◽  
Light Microscope ◽  
Epoxy Resins ◽  
Image Contrast ◽  
Tissue Preservation ◽  
Resin System ◽  
Excellent Quality

Since the introduction of epoxy resins as embedding material for electron microscopy, the list of new formulations and variations of widely accepted mixtures has grown rapidly. Described here is a resin system utilizing Maraglas 655, Dow D.E.R. 732, DDSA, and BDMA, which is a variation of the mixtures of Lockwood and Erlandson. In the development of the mixture, the Maraglas and the Dow resins were tested in 3 different volumetric proportions, 6:4, 7:3, and 8:2. Cutting qualities and characteristics of stability in the electron beam and image contrast were evaluated for these epoxy mixtures with anhydride (DDSA) to epoxy ratios of 0.4, 0.55, and 0.7. Each mixture was polymerized overnight at 60°C with 2% and 3% BDMA.Although the differences among the test resins were slight in terms of cutting ease, general tissue preservation, and stability in the beam, the 7:3 Maraglas to D.E.R. 732 ratio at an anhydride to epoxy ratio of 0.55 polymerized with 3% BDMA proved to be most consistent. The resulting plastic is relatively hard and somewhat brittle which necessitates trimming and facing the block slowly and cautiously to avoid chipping. Sections up to about 2 microns in thickness can be cut and stained with any of several light microscope stains and excellent quality light photomicrographs can be taken of such sections (Fig. 1).

Luminescence from individual dislocations in II-VI and III-V semiconductors

1991 ◽  
Vol 49 ◽  
pp. 834-835
Author(s):  
J W Steeds
Keyword(s):  
Group Iv ◽  
Luminescence Properties ◽  
Carrier Recombination ◽  
Transmission Electron ◽  
Wide Range ◽  
Basic Physics ◽  
Semiconducting Compounds ◽  
Diamond Group ◽  
Non Destructive ◽  
Technological Significance

There is a wide range of experimental results related to dislocations in diamond, group IV, II-VI, III-V semiconducting compounds, but few of these come from isolated, well-characterized individual dislocations. We are here concerned with only those results obtained in a transmission electron microscope so that the dislocations responsible were individually imaged. The luminescence properties of the dislocations were studied by cathodoluminescence performed at low temperatures (~30K) achieved by liquid helium cooling. Both spectra and monochromatic cathodoluminescence images have been obtained, in some cases as a function of temperature.There are two aspects of this work. One is mainly of technological significance. By understanding the luminescence properties of dislocations in epitaxial structures, future non-destructive evaluation will be enhanced. The second aim is to arrive at a good detailed understanding of the basic physics associated with carrier recombination near dislocations as revealed by local luminescence properties.

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