Fabrication and Mechanical Properties of PAN-based Carbon Composite Laminates for High Temperature Applications.

The main aim of this paper is an experimental investigation is to study the thermophysical and mechanical properties of polyacrylonitrile (PAN) based carbon fiber fabric and phenolic resin composites (Cf-PR) for thermal protection system (TPS) for high temperature applications. Composite laminates of Cf-PR were prepared by hand-layup method by considering the curing temperature of 1500 C at 100 kg/cm2 for 4hrs under hydraulic hot press machine. The mechanical properties of the materials such as the interlaminar shear stress (ILSS), flexural strength, compression strength, bar coal hardness, thermal property such as thermal conductivity and physical property such as density were studied. It was shown that the thermophysical and mechanical properties are responsibility for the higher strength and higher temperature applications for TPS.

Experimental studies on interlaminar shear strength and dynamic mechanical analysis of luffa fiber epoxy composites with nano PbO addition

In the present study, the significance of nanofiller lead oxide (PbO) on the dynamic mechanical analysis (DMA) and interlaminar shear strength (ILSS) performance of luffa fiber–reinforced epoxy composites was investigated. The epoxy matrix was altered with nanofiller PbO of different weight percent through a mechanical stirring process. The PbO-added luffa fiber epoxy composites were made through hand layup preceded by the compression molding method. The prepared composite samples were investigated for ILSS and DMA. The test results lead to the inference that the 1.25 wt% PbO nanofiller–added composite samples attained 25%, 17%, and 55% of higher loss modulus, storage modulus, and ILSS, respectively, as compared with the other prepared samples. The morphological investigation was conducted on the fractured surface of the interlaminar tested samples. The micrographic images show the bonding nature of the luffa fiber with the epoxy matrix, fiber breakage, and fiber pullouts. The characterization studies such as FTIR, XRD, and EDX were conducted on the fabricated composite samples. The XRD studies show that the rise in weight percent of the nanofiller PbO enhances the crystallinity of the composite samples. Moreover, the composite sample prepared with 1.25 wt% nanofiller PbO can be used to prepare low-cost roofing materials for sustainable housing projects.

EFFECT OF SALT-WATER AGING ON THE MECHANICAL PROPERTIES OF FLAX-WOVEN FABRIC-REINFORCED EPOXY COMPOSITES

In this investigation four varieties of plain derived-irregular basket-woven-flax fabric-reinforced epoxy (F-E) composites pre-treated with alkali and trimethoxymethylsilane (ATS) were prepared with a hand lay-up process by varying their weight fraction of fiber loadings (0; 25; 35; 45) w/%. A water-absorption test (salt water) as per ASTM D 570-98 was performed over the fabricated composites and studied its consequences on their static mechanical properties (such as tensile, flexural, impact and interlaminar shear strength) in accordance with the ASTM standards. The results revealed that salt-water-soaked ATS-treated F-E composites exhibited poorer mechanical properties than unsoaked ones. Moreover, this study elaborated the kinetics of water absorption and showed that the moisture-absorption rate depends on the weight fraction of fibre content. Furthermore, scanning electron microscopy (SEM) disclosed fiber splittings and severe damage at the fiber-matrix interface as experienced by soaked F-E composites.

Material Parameters Identification for Modelling of Carbon Rod Structures Delamination

The aim of the present work is to compare the interlaminar shear strength and fracture toughness of glued carbon fiber rods obtained using different experimental approaches and provide the effective way to characterise the interlaminar properties for reliable simulation of the delamination. Five different test methods (tension, single shear test, and double shear test, mode I and mode II delamination tests) were performed. Using the explicit LS-DYNA code the finite element model capable of simulating the damage process of bonded connection was developed. The interlaminar connection and delamination criteria were calibrated using the parameter identification methodology implemented in LS-OPT optimization tool.

Ramie fiber reinforced composites with flame retardant structure design: flammability, smoke suppression, and mechanical properties

In this work, the structure of composite was designed as Core Stack and Surface Stack, which was treated with the expandable graphite (EG) and metal oxides such as iron oxide (IO), hydroxyapatite (HA), and aluminum tri-hydroxide (ATH). The mechanical performance of composites was characterized via flexural performance and interlaminar shear strength analysis. The flame retardance and smoke suppression of composite was explored in detail by LOI, UL-94, and cone calorimeter test. The findings presented that flexural properties of composites were observed to decrease due to delamination of surface stack, whilst no significant effect on interlaminar shear strength. In comparison with control composite, the loading of metal oxide into composite Surface Stack led to the reduction of peak heat release rate, total heat release, and fire growth index effectively. Moreover, the remarkable decrease in total smoke production could be observed due to the addition of iron oxide and the flame retardant mechanism was discussed. This study was the preliminary exploration of composite with flame retardant design which could be potential solution to improve flame retardancy and smoke suppression of composite with better mechanical structure preservation.

Mechanical Properties, Surface Assessment, and Structural Analysis of Functionalized CFRPs after Accelerated Weathering

The present study focuses on the effect of two novel carbon fibre surface treatments, electropolymerisation of methacrylic acid and air pressure plasma, on the mechanical properties and structural integrity of carbon-fibre-reinforced composites under operational conditions. Extensive mechanical testing was applied, both in nano- and macro-scale, to assess the performance of the composites and the interphase properties after ultraviolet/humidity weathering. The results of the mechanical assessment are supported by structure, surface, and chemistry examination in order to reveal the failure mechanism of the composites. Composites with the electropolymerisation treatment exhibited an increase of 11.8% in interlaminar shear strength, while APP treatment improved the property of 23.9%, rendering both surface treatments effective in increasing the fibre-matrix adhesion. Finally, it was proven that the developed composites can withstand operational conditions in the long term, rendering them suitable for a wide variety of structural and engineering applications.

Influence of Twin-Screw Extrusion on The Dispersion of Nanoclay in Vinylester Composites

This paper reports the dispersion of nanoclay in vinylester using co-rotating twin screw extrusion and ultrasonication for preparing nanoclay/vinylester gel coat. Two sets MMT/vinylester specimens, namely Type 1 and Type 2 were prepared for comparative studies. While Type 1 specimens were prepared using ultrasonication only, Type 2 specimens were prepared using both ultrasonication and twin-screw extrusion. Type 2 specimens showed lower levels of nanoclay intercalation and higher levels of exfoliation. By using the MMT/vinylester gel coat so prepared by the two different routes, MMT/vinylester/glass specimens were fabricated and tested for mechanical properties. Type 2 based nanocomposite specimens showed greater values of ultimate tensile strength, flexural strength, interlaminar shear strength and impact strength. Scanning Electron Micrographs (SEM) of tensile fractured Type 2 based specimens showed less agglomeration of nanoclay than that of Type 1 based specimens.

In-situ damage sensing in intra-ply glass/carbon laminate composites under interlaminar shear loading

An experimental study is preformed to investigate the in-situ damage sensing capabilities of intra-ply hybrid carbon/glass laminate and epoxy composites under quasi-static interlaminar shear loading. A three-dimensional electrical sensory network is generated inside the composites through embedded carbon nanotubes (CNTs) in an epoxy matrix along with the carbon fibers in the intra-ply hybrid laminates. CNTs are dispersed in the epoxy matrix using a combination of ultrasonication and shear mixing techniques. Four circumferential ring probes are used to examine the electrical response under interlaminar shear load. The effect of four different intra-ply orientations (((0–90)C, where carbon fibers are oriented along the loading direction), ((0–90)G, where glass fibers are oriented along the loading direction), ((45/−45, where glass and carbon fibers are oriented at 45o/−45o and the laminates are repeated), and ((45/−45)A, where glass and carbon fibers are oriented at 45o/−45o and the laminates are alternated)) on the shear constitutive behavior and the damage detection are discussed. Intra-ply orientations of (45/−45) and (45/−45)A showed higher interlaminar shear strength and shear strain at break compared to (0/90)C and (0/90)G orientations. Out of all four orientations, (45/−45)A provided a better resolution of electrical response for damage sensing applications.