The characterization of the dynamic arc-anode interaction and using plasma deposition of nanocomposites to tailor materials properties

Author(s):  
Joachim Heberlein
Author(s):  
L.E. Murr ◽  
A.B. Draper

The industrial characterization of the machinability of metals and alloys has always been a very arbitrarily defined property, subject to the selection of various reference or test materials; and the adoption of rather naive and misleading interpretations and standards. However, it seems reasonable to assume that with the present state of knowledge of materials properties, and the current theories of solid state physics, more basic guidelines for machinability characterization might be established on the basis of the residual machined microstructures. This approach was originally pursued by Draper; and our presentation here will simply reflect an exposition and extension of this research.The technique consists initially in the production of machined chips of a desired test material on a horizontal milling machine with the workpiece (specimen) mounted on a rotary table vice. A single cut of a specified depth is taken from the workpiece (0.25 in. wide) each at a new tool location.


Materials ◽  
2020 ◽  
Vol 13 (13) ◽  
pp. 2981 ◽  
Author(s):  
Dorian Minkov ◽  
George Angelov ◽  
Radi Nestorov ◽  
Aleksey Nezhdanov ◽  
Dmitry Usanov ◽  
...  

Three AsxTe100−x films with different x and dissimilar average thickness d ¯ are characterized mainly from one interference transmittance spectrum T(λ = 300 to 3000 nm) of such film on a substrate based on the advanced optimizing envelope method (AOEM). A simple dual transformation of T(λ) is proposed and used for increasing the accuracy of computation of its envelopes T+(λ) and T−(λ) accounting for the significant glass substrate absorption especially for λ > 2500 nm. The refractive index n(λ) of As40Te60 and As98Te2 films is determined with a relative error <0.30%. As far as we know, the As80Te20 film is the only one with anomalous dispersion and the thickest, with estimated d ¯ = 1.1446 nm, ever characterized by an envelope method. It is also shown and explained why the extinction coefficient k(λ) of any of the three AsxTe100−x films is computed more accurately from the quantity Ti(λ) = [T+(λ)T−(λ)]0.5 compared to its commonly employed computation from T+(λ). The obtained results strengthen our conviction that the AOEM has a capacity for providing most accurate optical characterization of almost every dielectric or semiconductor film with d ¯ > 300 nm on a substrate, compared to all the other methods for characterization of such films only from T(λ).


2004 ◽  
Vol 338-340 ◽  
pp. 91-96 ◽  
Author(s):  
R. Ambrosio ◽  
A. Torres ◽  
A. Kosarev ◽  
A. Ilinski ◽  
C. Zúñiga ◽  
...  

2017 ◽  
Vol 79 (5-3) ◽  
Author(s):  
Shajaratuldur Ismail ◽  
Nurlidia Mansor ◽  
Zakaria Man ◽  
Khairun Azizi Azizli

Starch is one of natural materials that been used for producing biodegradable materials. The starch-based materials are produced through a process known as gelatinization with the presence of plasticizer and elevated temperature. Properties of starch-based materials are lacking in terms of viscosity, water absorption, thermal and mechanical properties compare with synthetic materials. Researchers are involved in finding ways for improvement of starch-based materials properties and one of that is introducing new plasticizer. 1-ethyl-3-methylimidazolium acetate, [Emim][OAc] is an ionic liquid that used as plasticizer to produce thermoplastic starch. Starch plasticized by [Emim][OAc] were prepared with different total plasticizer contents (50%,70%) and [Emim][OAc]/water ratio (1:6,1:4,2:3 wt%). The thermoplastic starches were characterized in terms of morphology, crystalline structure and thermal degradation. The results showed that 70% of total plasticizer contents were mixed well during gelatinization process. [Emim][OAc] contributed to granule disruption as shown by SEM. Based on the XRD analysis, it was shown that thermoplastic starch at 70% total plasticizer contents and 1:4 wt% ratio of [Emim][OAc]/water, caused disruption of the A-type crystalline structure, generated VH-type crystalline structure and thus increased the mobility of the amorphous starch. The presence of [Emim][OAc] promotes the thermal degradation of starch molecules as described by TGA. Therefore, plasticizer contents and [Emim][OAc]/water ratio are vital parameters that influences the properties of thermoplastic starch.


2008 ◽  
Vol 139 (1-2) ◽  
pp. 3-28 ◽  
Author(s):  
N.P. Berezina ◽  
N.A. Kononenko ◽  
O.A. Dyomina ◽  
N.P. Gnusin

2011 ◽  
Vol 50 (8S1) ◽  
pp. 08JD03 ◽  
Author(s):  
Dmitry Yarmolich ◽  
Petr Nozar ◽  
Svetlana Gleizer ◽  
Yakov E. Krasik ◽  
Giuseppe Mittica ◽  
...  

1995 ◽  
Vol 32 (5) ◽  
pp. 689-693 ◽  
Author(s):  
D.E. Lawrynowicz ◽  
J. Wolfenstine ◽  
E.J. Lavernia ◽  
S.R. Nutt ◽  
D.E. Bailey ◽  
...  

2020 ◽  
Author(s):  
Jimmy Thörnberg ◽  
Justinas Palisaitis ◽  
Niklas Hellgren ◽  
Fedor Klimashin ◽  
Naureen Ghafoor ◽  
...  

<p>In the present research article we report synthesis of TiB<sub>x</sub>, 1.43<i>n-situ</i> mass- and energy-spectroscopy is used to explain the obtained compositional range. Excess B in overstoichiometric TiB<i><sub>x</sub></i><sub> </sub>thin films from DCMS results in a hardness up to 37.7±0.8 GPa, attributed to the formation of an amorphous B-rich tissue phase separating stoichiometric TiB<sub>2</sub> columnar structures. With a particular focus on characterization of the understoichiometric samples, we show that understoichiometric TiB<sub>1.43</sub> thin films synthesized by HiPIMS exhibit a superior hardness of 43.9±0.9 GPa, where the deficiency of B is found to be accommodated by Ti planar defects. The apparent fracture toughness, electrical resistivity and thermal conductivity of the same sample is 4.2±0.1 MPa√m, 367±7 μΩ·cm and 5.1 W/(m.K), respectively, as compared to corresponding values for overstoichiometric TiB<sub>2.20</sub> DCMS thin film samples of 3.2±0.1 MPa√m, 309±4 μΩ·cm and 3.0 W/(m.K). </p>


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