Density Measurement of Powder Metallurgy Compacts by Means of Small Indentation

2008 ◽  
Vol 130 (3) ◽  
Author(s):  
Fabrizio Quadrini ◽  
Erica Anna Squeo
Keyword(s):  
Powder Metallurgy ◽  
Density Measurement ◽  
Calibration Procedure ◽  
Indentation Load ◽  
Instrumented Indentation ◽  
Packing Pressure ◽  
Indentation Tests ◽  
Density Evaluation ◽  
Compaction Of Powders ◽  
Small Indentation

In this study, the density of powder metallurgy compacts was measured by means of small indentation. Zinc (Zn) and aluminum (Al) tablets were fabricated by cold compaction of powders: different tablet densities were obtained by changing the packing pressure. Instrumented indentation tests were carried out by means of flat cylindrical indenters having diameters of 1mm and 2mm. After a calibration procedure, the slope of the indentation curve or the indentation load can be used for the density evaluation.

Feasible Evaluation of Flow Properties and Stress State of Structural Materials Using Instrumented Indentation Tests

2006 ◽  
Vol 326-328 ◽  
pp. 487-492 ◽  
Author(s):  
Ju Young Kim ◽  
Jung Suk Lee ◽  
Kyung Woo Lee ◽  
Kwang Ho Kim ◽  
Dong Il Kwon
Keyword(s):  
Stress State ◽  
Structural Materials ◽  
Tensile Tests ◽  
Indentation Load ◽  
Uniaxial Tensile ◽  
Instrumented Indentation ◽  
Flow Properties ◽  
Friction Stir ◽  
Indentation Tests ◽  
Quantitative Stress

Flow properties and stress state are indispensable factors for safety assessment of structural materials in operation, which were evaluated using instrumented indentation tests (IITs). Flow properties were obtained by defining representative stress and strain, and IIT results for 10 steel materials were discussed by comparing with those from uniaxial tensile tests. The indentation load-depth curve is significantly affected by the presence of residual stress, and the stress-induced load change was converted to a quantitative stress value. The stress state of a friction stir-welded joint of API X80 steel was evaluated and compared with that measured by energy-dispersive X-ray diffraction.

Quantitative evaluation of adhesion of diamond coatings

1999 ◽  
Vol 14 (3) ◽  
pp. 1142-1147 ◽  
Author(s):  
Qi Hua Fan ◽  
A. Fernandes ◽  
E. Pereira ◽  
J. Grácio
Keyword(s):  
Quantitative Evaluation ◽  
Indentation Load ◽  
Diamond Coating ◽  
Diamond Coatings ◽  
Coating Adhesion ◽  
Indentation Tests ◽  
Deformation Stress ◽  
Small Indentation

This paper presents a model to evaluate quantitatively the adhesion of diamond coating according to indentation tests. It is found that small indentation load causes round spallation of the coating, no matter what the shape of the indenter. An exponential sink-in deformation of the coating under the indentation is proposed [y = −a × exp(−bx)]. The deformation stress at the spallation edge is considered the coating adhesion. Using an experimentally observed relation of the indentation load versus the film spallation radius, we evaluate the adhesion of a diamond coating on copper to be about 1.921–1.956 GPa, which is in agreement with thermal quench results. The validity of this model is also verified by its self-consistence.

Regularities and properties of instrumented indentation diagrams obtained by ball-shaped indenter

2020 ◽  
Vol 86 (5) ◽  
pp. 43-51
Author(s):  
V. M. Matyunin ◽  
A. Yu. Marchenkov ◽  
N. Abusaif ◽  
P. V. Volkov ◽  
D. A. Zhgut
Keyword(s):  
Yield Strength ◽  
Ultimate Strength ◽  
Elastoplastic Deformation ◽  
Elastic Limit ◽  
Tensile Tests ◽  
Indentation Load ◽  
International Standards ◽  
Instrumented Indentation ◽  
Indentation Methods ◽  
Special Points

The history of appearance and the current state of instrumented indentation are briefly described. It is noted that the materials instrumented indentation methods using a pyramid and ball indenters are actively developing and are currently regulated by several Russian and international standards. These standards provide formulas for calculating the Young’s modulus and hardness at maximum indentation load. Instrumented indentation diagrams «load F – displacement α» of a ball indenter for metallic materials were investigated. The special points on the instrumented indentation diagrams «F – α» loading curves in the area of elastic into elastoplastic deformation transition, and in the area of stable elastoplastic deformation are revealed. A loading curve area with the load above which the dF/dα begins to decrease is analyzed. A technique is proposed for converting «F – α» diagrams to «unrestored Brinell hardness HBt – relative unrestored indent depth t/R» diagrams. The elastic and elastoplastic areas of «HBt – t/R» diagrams are described by equations obtained analytically and experimentally. The materials strain hardening parameters during ball indentation in the area of elastoplastic and plastic deformation are proposed. The similarity of «HBt – t/R» indentation diagram with the «stress σ – strain δ» tensile diagrams containing common zones and points is shown. Methods have been developed for determining hardness at the elastic limit, hardness at the yield strength, and hardness at the ultimate strength by instrumented indentation with the equations for their calculation. Experiments on structural materials with different mechanical properties were carried out by instrumented indentation. The values of hardness at the elastic limit, hardness at the yield strength and hardness at the ultimate strength are determined. It is concluded that the correlations between the elastic limit and hardness at the elastic limit, yield strength and hardness at the yield strength, ultimate tensile strength and hardness at the ultimate strength is more justified, since the listed mechanical characteristics are determined by the common special points of indentation diagrams and tensile tests diagrams.

Comparison of mechanical properties of thermally modified wood at growth ring and cell wall level by means of instrumented indentation tests

Holzforschung ◽  
2009 ◽  
Vol 63 (4) ◽  
Author(s):  
Stefanie Stanzl-Tschegg ◽  
Wilfried Beikircher ◽  
Dieter Loidl
Keyword(s):  
Mechanical Properties ◽  
Cell Wall ◽  
Thermal Treatment ◽  
Mechanical Performance ◽  
Growth Ring ◽  
Beech Wood ◽  
Thermal Modification ◽  
Wood Structure ◽  
Instrumented Indentation ◽  
Indentation Tests

Abstract Thermal modification is a well established method to improve the dimensional stability and the durability for outdoor use of wood. Unfortunately, these improvements are usually accompanied with a deterioration of mechanical performance (e.g., reduced strength or higher brittleness). In contrast, our investigations of the hardness properties in the longitudinal direction of beech wood revealed a significant improvement with thermal modification. Furthermore, we applied instrumented indentation tests on different hierarchical levels of wood structure (growth ring and cell wall level) to gain closer insights on the mechanisms of thermal treatment of wood on mechanical properties. This approach provides a variety of mechanical data (e.g., elastic parameters, hardness parameters, and viscoelastic properties) from one single experiment. Investigations on the influence of thermal treatment on the mechanical properties of beech revealed similar trends on the growth ring as well as the on the cell wall level of the wood structure.

Evaluation of Young’s modulus of construction materials by instrumented indentation using a ball indenter

2021 ◽  
Vol 87 (8) ◽  
pp. 64-68
Author(s):  
V. M. Matyunin ◽  
A. Yu. Marchenkov ◽  
N. Abusaif ◽  
M. V. Goryachkina ◽  
R. V. Rodyakina ◽  
...  
Keyword(s):  
Young’S Modulus ◽  
Young's Modulus ◽  
High Surface ◽  
Construction Materials ◽  
Contact Problems ◽  
Indentation Load ◽  
Test Material ◽  
Elastic Displacement ◽  
Large Radius ◽  
Instrumented Indentation

Methods for evaluation of Young’s modulus (Em) of structural materials by instrumented indentation using ball indenter have been considered. All these techniques are based on the solution of elastic contact problems performed by H. Hertz. It has been shown that registration of the initial elastic region in the «load – displacement» indentation diagram provides the Em determination for metals and alloys. However, it is necessary to evaluate accurately the elastic compliance of a device, to use an indenter with a large radius R, and ensure a high surface quality of the test material in advance. Methods for Em determation, when indentation diagrams are recorded in the elastoplastic indentation region, should include the effect of plastic deformation on the elastic displacement calculated by H. Hertz expression. However, it appeared essential to determine the relation between the elastic αel and plastic h components of the total elastoplastic displacement α and the elastic displacement α0 estimated by H. Hertz expression for a definite indentation load. A close correlation between α0 and αel is revealed for steels, aluminum, magnesium, and titanium alloys when using indenters with a radius of R = 0.2 – 5 mm (diameter D = 0.4 – 10 mm) and maximum indentation load Fmax = 47 – 29430 N (4.8 – 3000 kgf). It is also shown that a gradual decrease in Em is observed with an increase in R(D) at the same degree of loading F/D2 for the same material. This fact was explained by the scale factor effect.

Instrumented indentation microscope applied to the elastoplastic indentation contact mechanics of coating/substrate composites

2009 ◽  
Vol 24 (6) ◽  
pp. 1950-1959 ◽  
Author(s):  
N. Hakiri ◽  
A. Matsuda ◽  
M. Sakai
Keyword(s):  
Contact Area ◽  
Film Coating ◽  
Instrumented Indentation ◽  
Thin Film Coating ◽  
Composite Systems ◽  
Indentation Tests ◽  
Film Substrate ◽  
Contact Parameters

In instrumented indentation tests for a thin film coating on a substrate (film/substrate composite), it is well known that the substrate-affected contact area estimated through conventional approximations includes significant uncertainties, leading to a crucial difficulty in determining the elastic modulus and the contact hardness. To overcome this difficulty, an instrumented indentation microscope that enables researchers to make an in situ determination of the contact area is applied to an elastoplastic film on substrates having various values of their elastic moduli. Using the indentation microscope, the substrate-affected indentation contact parameters including contact hardness of the film/substrate composites are determined directly as well as quantitatively without any undesirable assumptions and approximations associated with the contact area estimate. The effect of a stiffer substrate on the contact profile of impression is significant, switching the profile from sinking in to piling up during penetration, and resulting in the substrate-affected contact hardness being highly enhanced at deeper penetrations. Through the present experimental study, it is demonstrated how efficient that instrumented indentation microscopy is in determining the substrate-affected elastoplastic contact parameters of film/substrate composite systems.

Effects of strain hardening and residual stress in impression on the instrumented indentation technique

2006 ◽  
Vol 21 (7) ◽  
pp. 1680-1686
Author(s):  
L.Z. Liu ◽  
Y.W. Bao ◽  
Y.C. Zhou
Keyword(s):  
Residual Stress ◽  
Strain Hardening ◽  
Energy Analysis ◽  
Maximum Load ◽  
Contact Theory ◽  
Elastic Contact ◽  
Instrumented Indentation ◽  
Indentation Technique ◽  
Indentation Tests ◽  
Elastic Loading

Finite element analyses were carried out to simulate the loading, unloading, and reloading processes of indentation tests. It was found that the validity of applying the elastic contact theory to the indentation unloading process is strongly related to the strain hardening and residual stress in impression. It is the combination of strain hardening and residual stress that causes the unloading or reloading curves to show elastic loading in the range from zero to the maximum load whereas the reloading curve on the impression without strain hardening and residual stress shows elastic–plastic loading in the same range. These computations indicate that applying the elastic contact theory to the unloading or reloading processes, the fundamental prerequisite of the instrumented indentation technique, is valid because of the existence of strain hardening and residual stress. The mechanism of this hardening effect is discussed through energy analysis.

Analysis on Mechanical Properties of Instrumented Indentation Tester Frame

2012 ◽  
Vol 215-216 ◽  
pp. 895-898
Author(s):  
Jun Hong Guo ◽  
De Jun Ma ◽  
Wei Chen ◽  
Zhong Kang Song
Keyword(s):  
High Precision ◽  
Inclination Angle ◽  
Indentation Load ◽  
Measurement Precision ◽  
Instrumented Indentation ◽  
Element Analysis ◽  
Maximum Value ◽  
Load Analysis ◽  
The Relationship ◽  
Maximum Inclination

Finite element analysis is undertaken to identify the extent of loading deformation of instrumented indentation equipment frame which is a main part in High-precision instrumented indentation tester developed and realized by our group. The working load enacted in the model is varied from 10N to 100N, and the increment load is 10N. By plotting and fitting data of inclination angle and working load, the relationship between frame inclination angle and working load is established. The function of this relationship is θ=0.000024*F. When the working load is up to the upper bound 100N, the inclination angle of frame reaches the maximum value 0.00241°.Load analysis of push rod shows that the percent error between measured load values and real indentation load values caused by maximum inclination angle is in 10-8order. The conclusion is thus derived that frame inclination has nearly no effects on load measurement precision. The research in this paper confirms that the design of frame belonging to High-precision instrumented indentation tester is appropriate.

Instrumented-Indentation-Technique-Based Residual Stress Characterization for Weldment of Structural Components

2006 ◽  
Author(s):  
Dongil Kwon ◽  
Jung-Suk Lee ◽  
Kwang-Ho Kim ◽  
Afshin Motarjemi ◽  
Julian Speck
Keyword(s):  
Residual Stress ◽  
Welding Process ◽  
Indentation Load ◽  
Welding Residual Stress ◽  
Hole Drilling ◽  
Structural Components ◽  
Instrumented Indentation ◽  
Indentation Technique ◽  
Safety And Reliability ◽  
Depth Curve

The weld joints in structural components have long been considered important sites for safety and reliability assessment. In particular, the residual stress in piping weldments induced by the welding process must be evaluated accurately before and during service. This study reports an indentation technique for evaluating welding residual stress nondestructively. Indentation load-depth curves were found to shift with the magnitude and direction of the residual stress. Nevertheless, contact depths in the stress-free and stressed states were constant at a specific indentation load. This means that residual stress induces additional load to keep contact depth constant at the same load. By taking these phenomena into account, welding residual stress was obtained directly from the indentation load-depth curve. In addition, the results were compared with values from the conventional hole-drilling and saw-cutting method.

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