Computation of hydrodynamic and capillary phenomena in binder jet 3D printing

2021 ◽  
pp. 1-51
Author(s):  
Joshua Wagner ◽  
C. Fred Higgs

Abstract The fundamental operation in binder jet 3D printing is the deposition of liquid binder into a powder layer to selectively bond particles together. Upon droplet impact, the binder spreads into the powder bed forming a bound network of wetted particles called a primitive. A computational fluid dynamics framework is proposed to directly simulate the capillary and hydrodynamic effects of the interfacial flow that is responsible for primitive formation. The computational model uses the volume-of-fluid method for capturing dynamic binder-air interfaces, and the immersed boundary method is adopted to include particle geometries on numerical Cartesian grids. Three-phase contact angles are prescribed through an interface extension algorithm. Binder droplet impact on powder beds of varying contact angle are simulated. Furthermore, the numerical model is used to simulate liquid bridges connecting binary and ternary particle systems, and the resulting capillary and hydrodynamic forces are validated by comparison with published experimental and theoretical model results.

2021 ◽  
Vol 12 (1) ◽  
pp. 266
Author(s):  
Seungyeop Chun ◽  
Geumyeon Lee ◽  
Sujin Kim ◽  
Bora Jeong ◽  
Jeehoon Shin ◽  
...  

With the development of the powder bed 3D printing process, sand casting can be performed with methods that are more advanced than the traditional ones, thus enabling new research on applied materials. When sand is 3D-printed with cement as a binder, its casting performance is improved and sufficient thermal stability of conventional organic and inorganic binders is ensured. In this study, to ensure high resolution and strength in a physical and simple mixture of cement and sand, the compatibility for casting was confirmed using submicron-level cement with ingredients and sizes similar to commercial sand, which is uniformly controlled at 4 µm, instead of conventional sand. To enable quick 3D printing, calcium aluminate cement, which has quick binding properties, was used for high-temperature casting. The strength up to 6 h after hydration was compared to determine the curing rate of silica, mullite, and alumina sand containing cement components. By investigating the change in strength due to heat treatment and comparing the adhesion drop test results after powder bed formation, the material containing silica sand was determined as the most suitable for powder layer 3D printing for application to the mold.


Carbon ◽  
2017 ◽  
Vol 119 ◽  
pp. 257-266 ◽  
Author(s):  
Amir Azhari ◽  
Ehsan Marzbanrad ◽  
Dilara Yilman ◽  
Ehsan Toyserkani ◽  
Michael A. Pope

Materials ◽  
2021 ◽  
Vol 14 (11) ◽  
pp. 2842
Author(s):  
Lucia Lizzul ◽  
Rachele Bertolini ◽  
Andrea Ghiotti ◽  
Stefania Bruschi

Additive manufacturing processes induce a high orientation in the microstructure of the printed part due to the strong thermal gradients developed during the process caused by the highly concentrated heat source that is used to melt the metal powder layer-by-layer. The resulting microstructural anisotropy may have an effect on the post-processing operations such as machining ones. This paper investigates the influence of the anisotropy in turning operations carried out on laser powder bed fused Ti6Al4V parts manufactured with different scanning strategies. The machinability under both transverse and cylindrical turning operations was assessed in terms of surface integrity, considering both surface and sub-surface aspects. The effect of the different cooling conditions, that is flood and cryogenic ones, was studied as well. The outcomes showed that the microstructural anisotropy had a remarkable effect on the machining operations and that the cryogenic cooling enhanced the effect of the anisotropy in determining the surface integrity.


Author(s):  
Neeharika Anantharaju ◽  
Mahesh Panchagnula ◽  
Wayne Kimsey ◽  
Sudhakar Neti ◽  
Svetlana Tatic-Lucic

The wettability of silicon surface hydrophobized using silanization reagents was studied. The advancing and receding contact angles were measured with the captive needle approach. In this approach, a drop under study was held on the hydrophobized surface with a fine needle immersed in it. The asymptotic advancing and receding angles were obtained by incrementally increasing the volume added and removed, respectively, until no change in angles was observed. The values were compared with the previously published results. Further, the wetting behavior of water droplets on periodically structured hydrophobic surfaces was investigated. The surfaces were prepared with the wet etching process and contain posts and holes of different sizes and void fractions. The surface geometry brought up a scope to study the Wenzel (filling of surface grooves) and Cassie (non filling of the surface grooves) theories and effects of surface geometry and roughness on the contact angle. Experimental data point to an anomalous behavior where the data does not obey either Wenzel or Cassie type phenomenology. This behavior is explained by an understanding of the contact line topography. The effect of contact line topography on the contact angle was thus parametrically studied. It was also inferred that, the contact angle increased with the increase in void fraction. The observations may serve as guidelines in designing surfaces with the desired wetting behavior.


2017 ◽  
Vol 21 (4) ◽  
pp. 207-218 ◽  
Author(s):  
Peeyush Nandwana ◽  
Amy M. Elliott ◽  
Derek Siddel ◽  
Abbey Merriman ◽  
William H. Peter ◽  
...  

Author(s):  
Rishi Thakkar ◽  
Yu Zhang ◽  
Jiaxiang Zhang ◽  
Mohammed Maniruzzaman

AbstractThis study demonstrated the first case of combining novel continuous granulation with powder-based pharmaceutical 3-dimensional (3D) printing processes to enhance the dissolution rate and physical properties of a poorly water-soluble drug. Powder bed fusion (PBF) and binder jetting 3D printing processes have gained much attention in pharmaceutical dosage form manufacturing in recent times. Although powder bed-based 3D printing platforms have been known to face printing and uniformity problems due to the inherent poor flow properties of the pharmaceutical physical mixtures (feedstock). Moreover, techniques such as binder jetting currently do not provide any solubility benefits to active pharmaceutical ingredients (APIs) with poor aqueous solubility (>40% of marketed drugs). For this study, a hot-melt extrusion-based versatile granulation process equipped with UV-Vis process analytical technology (PAT) tools for the in-line monitoring of critical quality attributes (i.e., solid-state) of indomethacin was developed. The collected granules with enhanced flow properties were mixed with vinylpyrrolidone-vinyl acetate copolymer and a conductive excipient for efficient sintering. These mixtures were further characterized for their bulk properties observing an excellent flow and later subjected to a PBF-3D printing process. The physical mixtures, processed granules, and printed tablets were characterized using conventional as well as advanced solid-state characterization. These characterizations revealed the amorphous nature of the drug in the processed granules and printed tablets. Further, the in vitro release testing of the tablets with produced granules as a reference standard depicted a notable solubility advantage (100% drug released in 5 minutes at >pH 6.8) over the pure drug and the physical mixture. Our developed system known as DosePlus combines innovative continuous granulation and PBF-3D printing process which can potentially improve the physical properties of the bulk drug and formulations in comparison to when used in isolation. This process can further find application in continuous manufacturing of granules and additive manufacturing of pharmaceuticals to produce dosage forms with excellent uniformity and solubility advantage.Abstract Figure


Author(s):  
Gulraiz Ahmed ◽  
Nektaria Koursari ◽  
Anna Trybala ◽  
Victor M. Starov

Wetting of deformable substrates has gained significant interest over the past decade due to its extensive applications and uses. This interest has developed due to technological advances which are able to capture interfacial behavior taking place when a liquid droplet is placed on a deformable substrate. Researchers have developed different theories to explain processes taking place in the process of wetting of deformable/soft substrates. For the scope of this review, we will consider the fluid to be Newtonian, partially wetting, and surface forces are incorporated with the help of disjoining/conjoining pressure acting in the vicinity of the apparent, three-phase contact line. The following subjects are briefly reviewed: (i) Equilibrium of droplets on soft substrates. It is shown that properties of the disjoining/conjoining pressure isotherm and properties of the deformable substrate determine both the shape of the liquid droplet and deformation of the substrate; (ii) Equilibrium conditions of droplets on deformable substrates. It is shown that for a droplet to be at equilibrium on a deformable substrate under consideration, Jacobi’s sufficient condition is satisfied; (iii) Hysteresis of contact angle of sessile droplets on deformable substrates. It is shown that as the elasticity of the deformable substrate is increased, both advancing and receding contact angles are reduced.


2020 ◽  
Vol 26 (1) ◽  
pp. 100-106 ◽  
Author(s):  
Tobias Kolb ◽  
Reza Elahi ◽  
Jan Seeger ◽  
Mathews Soris ◽  
Christian Scheitler ◽  
...  

Purpose The purpose of this paper is to analyse the signal dependency of the camera-based coaxial monitoring system QMMeltpool 3D (Concept Laser GmbH, Lichtenfels, Germany) for laser powder bed fusion (LPBF) under the variation of process parameters, position, direction and layer thickness to determine the capability of the system. Because such and similar monitoring systems are designed and presented for quality assurance in series production, it is important to present the dominant signal influences and limitations. Design/methodology/approach Hardware of the commercially available coaxial monitoring QMMeltpool 3D is used to investigate the thermal emission of the interaction zone during LPBF. The raw images of the camera are analysed by means of image processing to bypass the software of QMMeltpool 3D and to gain a high level of signal understanding. Laser power, scan speed, laser spot diameter and powder layer thickness were varied for single-melt tracks to determine the influence of a parameter variation on the measured sensory signals. The effects of the scan direction and position were also analysed in detail. The influence of surface roughness on the detected sensory signals was simulated by a machined substrate plate. Findings Parameter variations are confirmed to be detectable. Because of strong directional and positional dependencies of the melt-pool monitoring signal a calibration algorithm is necessary. A decreasing signal is detected for increasing layer thickness. Surface roughness is identified as a dominating factor with major influence on the melt-pool monitoring signal exceeding other process flaws. Research limitations/implications This work was performed with the hardware of a commercially available QMMeltpool 3D system of an LPBF machine M2 of the company Concept Laser GmbH. The results are relevant for all melt-pool monitoring research activities connected to LPBF, as well as for end users and serial production. Originality/value Surface roughness has not yet been revealed as being one of the most important origins for signal deviations in coaxial melt-pool monitoring. To the best of the authors’ knowledge, the direct comparison of influences because of parameters and environment has not been published to this extent. The detection, evaluation and remelting of surface roughness constitute a plausible workflow for closed-loop control in LPBF.


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