Residual Stress Measurements in Continuous Fiber Titanium Matrix Composites

1992 ◽  
Vol 36 ◽  
pp. 481-488 ◽  
Author(s):  
M. R. James ◽  
M. A. Bourke ◽  
J. A. Goldstone ◽  
A. C. Lawson
Keyword(s):  
Residual Stress ◽  
Neutron Diffraction ◽  
Thin Sheet ◽  
Matrix Composites ◽  
X Ray ◽  
Residual Stress State ◽  
Longitudinal Residual Stress ◽  
The Matrix ◽  
Reinforcement Fiber ◽  
Residual Strains

AbstractMetal matrix composites develop residual strains after consolidation due to the thermal expansion mismatch between the reinforcement fiber and the matrix. X-ray and neutron diffraction measured values for the longitudinal residual stress in the matrix of three titanium MMCs are reported. For thick composites (> 6 plies) the surface stress measured by x-ray diffraction matches that determined by neutron diffraction and therefore represents the stress in the bulk region consisting of the fibers and matrix. For thin sheet composites, the surface values are lower than in the interior and increase as the outer rows of fibers are approached. While a rationale for this behavior has yet to be developed, accounting for composite thickness is important when using x-ray measured values to validate analytic and finite element calculations of the residual stress state.

Combined Neutron and X-Ray Diffraction Analysis for the Characterization of a Case Hardened Disc

2010 ◽  
Vol 652 ◽  
pp. 37-43 ◽  
Author(s):  
Jeremy Epp ◽  
Thomas Hirsch ◽  
Martin Hunkel ◽  
Robert C. Wimpory
Keyword(s):  
Residual Stress ◽  
Neutron Diffraction ◽  
Diffraction Analysis ◽  
Force Balance ◽  
X Ray Diffraction ◽  
X Ray ◽  
Residual Stress State ◽  
Systematic Uncertainties ◽  
Combined Use ◽  
Stress States

The present work has been executed within the framework of the collaborative research center on Distortion Engineering (SFB 570) in order to evaluate the residual stress state of a disc after carburizing and quenching as well as to validate a simulation procedure. The combined use of X-ray and neutron diffraction analysis provided information about the residual stress states in the whole cross section. However, the stress free lattice spacing d0 for the neutron diffraction experiments is problematic and induces systematic uncertainties in the results and the application of a force balance condition to recalculate d0 might be a solution for improving the reliability of the results. Comparison of experimental results with simulation showed that an overall satisfying agreement is reached but discrepancies are still present.

scholarly journals Residual Stress Evaluation of Carburized Transmission Steel Gear Using Neutron and Synchrotron X-Ray Diffraction and Finite Element Methods

2010 ◽  
Vol 652 ◽  
pp. 31-36 ◽  
Author(s):  
Yoshihisa Sakaida ◽  
Takanori Serizawa ◽  
M. Kawauchi ◽  
M. Manzanka
Keyword(s):  
Finite Element Method ◽  
Residual Stress ◽  
Finite Element ◽  
Neutron Diffraction ◽  
Carbon Content ◽  
Residual Strain ◽  
Stress Fields ◽  
X Ray ◽  
Residual Strains ◽  
Transmission Gear

A motorcycle transmission gear of chromium-molybdenum steel with 0.2%C was carburized in carrier gas. Carburizing process including heating, carburizing, diffusing and quenching was simulated using elastoplastic finite element method. The carbon content, hardness, residual strain and residual stress fields of gear were analyzed. The unstressed lattice plane spacing and residual strains of the interior near the internal spline of gear were experimentally measured by synchrotron x-ray and neutron diffraction methods. As a result, the analyzed carbon content and hardness gradients of gear accorded with the experimental results. The radial, hoop and axial directions of cylindrical gear were found to be not always principal axes of residual stress field. On the other hand, the analyzed residual strains in the radial, hoop and axial directions of gear slightly discorded with the experimental results. Although correlation between the measured three strains was similar to that of the weighted average of analyzed strains, residual strain and stress fields of motorcycle transmission gear could not be accurately predicted at the present finite element analysis. It was concluded that carbon diffusion phenomenon and resultant hardening could be analyzed by the finite element method, and the actual interior residual strain and stress fields should be nondestructively measured by neutron diffraction method.

X-ray Elastic Constants for β-SiC and Residual Stress Anisotropy in a Hot-Pressed Al2O3/SiC(Whisker) Composite

1990 ◽  
Vol 34 ◽  
pp. 643-650
Author(s):  
Paul Predecki ◽  
Alias Abuhasan ◽  
Charles S. Barrett
Keyword(s):  
Residual Stress ◽  
Elastic Constants ◽  
Crystal Data ◽  
X Ray ◽  
Residual Macrostresses ◽  
The Matrix ◽  
Average Residual ◽  
Residual Strains ◽  
Residual Microstresses ◽  
Ray Methods

AbstractX-ray elastic constants for the 511+333 and the 422 reflections of β-SiC were calculated from the single crystal data of Tolpygo using the Voigt-Reuss, Eshelby-Kroner and x-ray methods. Agreement was satisfactory for the 511+333, but less so for the 422. A hot-pressed α-Al2O3/ 29 vol % β-SiC (whisker) composite was investigated on its 3 principal faces. The total residual strains were found to be consistently anisotropic on all 3 faces suggesting that texture was present in the whiskers as a result of hot-pressing. Assuming no texture in the matrix, it was found possible to determine the average residual microstresses in the whiskers using the theory of Noyan and Cohen, without needing to know the whisker elastic constants or texture. The average microstresses were determined in each phase as well as the average residual macrostresses on each face.

scholarly journals Stress-Dependent Elasticity of TiAlN Coatings

Coatings ◽  
2019 ◽  
Vol 9 (1) ◽  
pp. 24 ◽  
Author(s):  
Marcus Hans ◽  
Lena Patterer ◽  
Denis Music ◽  
Damian M. Holzapfel ◽  
Simon Evertz ◽  
...  
Keyword(s):  
Residual Stress ◽  
Elastic Modulus ◽  
Stress State ◽  
Effective Medium Theory ◽  
Plasma Exposure ◽  
X Ray ◽  
Residual Stress State ◽  
Scanning Transmission ◽  
The Matrix ◽  
Stress Dependent

We investigate the effect of continuous vs. periodically interrupted plasma exposure during cathodic arc evaporation on the elastic modulus as well as the residual stress state of metastable cubic TiAlN coatings. Nanoindentation reveals that the elastic modulus of TiAlN grown at floating potential with continuous plasma exposure is 7%–11% larger than for coatings grown with periodically interrupted plasma exposure due to substrate rotation. In combination with X-ray stress analysis, it is evident that the elastic modulus is governed by the residual stress state. The experimental dependence of the elastic modulus on the stress state is in excellent agreement with ab initio predictions. The macroparticle surface coverage exhibits a strong angular dependence as both density and size of incorporated macroparticles are significantly lower during continuous plasma exposure. Scanning transmission electron microscopy in combination with energy dispersive X-ray spectroscopy reveals the formation of underdense boundary regions between the matrix and TiN-rich macroparticles. The estimated porosity is on the order of 1% and a porosity-induced elastic modulus reduction of 5%–9% may be expected based on effective medium theory. It appears reasonable to assume that these underdense boundary regions enable stress relaxation causing the experimentally determined reduction in elastic modulus as the population of macroparticles is increased.

Residual Stress Determination in Al2O3/SiC (Whisker) Composites By X-Ray Diffraction

1987 ◽  
Vol 31 ◽  
pp. 231-243 ◽  
Author(s):  
Paul Predecki ◽  
Alias Abuhasan ◽  
Charles S. Barrett
Keyword(s):  
Residual Stress ◽  
Profile Analysis ◽  
Peak Shift ◽  
Stress Determination ◽  
X Ray Diffraction ◽  
X Ray ◽  
The Matrix ◽  
Sic Whiskers ◽  
Residual Strains ◽  
Two Phases

Residual strains and stresses were determined in both phases of a hot pressed α-Al2O3 composite containing 25 wt % β (cubic) SiC whiskers using conventional x-ray diffraction and profile analysis. Both phases in this composite were randomly oriented as confirmed by back reflection pinhole photographs. The reflections found most useful with Cu Kα radiation were: 511 + 333 for β-SiC at -134° 2θ and 146 for α-Al2O3 at -136° 2θ. The peak shift and broadening observed in these reflections, relative to the starting powders, were largely due to the two phases mutually constraining each other elastically. This was confirmed by the reversal of the peak shift and most of the broadening in the SiC reflections when the Al2O3 matrix was etched away. Using the method of Cohen and Noyan, it was found possible to separate the macrostresses from the microstress components in each phase. The microstresses were largely hydrostatic; of the order of 895 MPa (130 ksi) compressive in the whiskers and 370 MPa (54 ksi) tensile in the matrix. The macrostresses were ~79 MPa (11.5 ksi) tensile.

Investigation of Residual Strains of the Second Kind in Plastically Deformed Metallic Materials

1994 ◽  
Vol 376 ◽  
Author(s):  
M. Vrána ◽  
P. Klimanek ◽  
T. Kschidock ◽  
P. Lukáš ◽  
P. Mikula
Keyword(s):  
High Resolution ◽  
Neutron Diffraction ◽  
Stacking Faults ◽  
Metallic Materials ◽  
Line Broadening ◽  
X Ray Diffraction ◽  
X Ray ◽  
Neutron Diffractometer ◽  
Residual Strains ◽  
Good Agreement

ABSTRACTInvestigation of strongly distorted crystal structures caused by dislocations, stacking-faults etc. in both plastically deformed f.c.c. and b.c.c. metallic materials was performed by the analysis of the neutron diffraction line broadening. Measurements were realized by means of the high resolution triple-axis neutron diffractometer equipped by bent Si perfect crystals as monochromator and analyzer at the NPI Řež. The substructure parameters obtained in this manner are in good agreement with the results of X-ray diffraction analysis.

scholarly journals COMPUTATIONAL MICROSTRUCTURE-BASED ANALYSIS OF RESIDUAL STRESS EVOLUTION IN METAL-MATRIX COMPOSITE MATERIALS DURING THERMOMECHANICAL LOADING

2021 ◽  
Vol 19 (2) ◽  
pp. 241
Author(s):  
Ruslan Balokhonov ◽  
Varvara Romanova ◽  
Eugen Schwab ◽  
Aleksandr Zemlianov ◽  
Eugene Evtushenko
Keyword(s):  
Residual Stress ◽  
Metal Matrix ◽  
Spatial Scales ◽  
Three Dimensional ◽  
Matrix Composites ◽  
Two Phase ◽  
Irregular Shapes ◽  
The Matrix ◽  
Stress Formation ◽  
Mechanical Fragmentation

A technique for computer simulation of three-dimensional structures of materials with reinforcing particles of complex irregular shapes observed in the experiments is proposed, which assumes scale invariance of the natural mechanical fragmentation. Two-phase structures of metal-matrix composites and coatings of different spatial scales are created, with the particles randomly distributed over the matrix and coating computational domains. Using the titanium carbide reinforcing particle embedded into the aluminum as an example, plastic strain localization and residual stress formation along the matrix-particle interface are numerically investigated during cooling followed by compression or tension of the composite. A detailed analysis is performed to evaluate the residual stress concentration in local regions of bulk tension formed under all-round and uniaxial compression of the composite due to the concave and convex interfacial asperities.

Residual stresses in a SiC whisker-reinforced alumina composite by high-temperature X-ray diffraction

1994 ◽  
Vol 9 (1) ◽  
pp. 50-53 ◽  
Author(s):  
Benjamin L. Ballard ◽  
Paul K. Predecki ◽  
Camden R. Hubbard
Keyword(s):  
Residual Stress ◽  
Single Crystal Silicon ◽  
Linear Extrapolation ◽  
X Ray Diffraction ◽  
Crystal Silicon ◽  
X Ray ◽  
Fine Grained ◽  
Silicon Carbide Whiskers ◽  
Alumina Composite ◽  
Residual Strains

Residual strains and microstresses are evaluated for both phase of a hot-pressed, fine-grained α-alumina reinforced with 25 wt% (29 vol%) single-crystal silicon carbide whiskers at temperatures from 25 to 1000 °C. The sample was maintained in a nonoxidizing environment while measurements of the interplaner spacing of alumina (146) and SiC (511 + 333) were made using X-ray diffraction methods. The residual strains were profiled at temperature increments of 250 °C from which the corresponding microstresses were calculated. Linear extrapolation of the SiC ε33 profile indicates that the strains are completely relaxed at a temperature of approximately 1470 °C. These residual stress relaxation results suggest that elevated temperature toughness and fracture strength of this composite may result from cooperative mechanisms.

Direct X-Ray Measurement of Residual Strains in Textured Steel

1983 ◽  
Vol 27 ◽  
pp. 197-206
Author(s):  
C. P. Gazzara
Keyword(s):  
Residual Stress ◽  
Crystal Lattice ◽  
Elastic Constants ◽  
Random Distribution ◽  
Elastic Anisotropy ◽  
X Ray Diffraction ◽  
X Ray ◽  
Residual Strains ◽  
Residual Stress Analysis ◽  
Textured Materials

One of the most detrimental effects on the accuracy of an X-ray diffraction residual stress analysis, XRDRSA(l), is found in the examination of textured materials. The degree of elastic anisotropy and texture is in general agreement with the extent of the error in the residual stress. Several approaches have been made to correct for the effects of texture, particularly involving experimental techniques. Reviews of such efforts are given by H. D811e(2), v.M. Hauk﹛3) and G. Maeder, J.L. Lebrun and J.M. Sprauel (4), just to mention a few.A brief chronology of the texture corrections involved in XRDRSA follows. With isotropic materials the d spacing of a crystal lattice, d, is assumed to vary linearly with sin2ψ. With textured materials the d vs sin2ψ relationship is nonlinear. This is due to the anisotropy of the elastic constants and their departure from a random distribution, or taking on a preferred orientation.

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