The Second Expansion Cycle in Ultramicrocellular Foams
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Ultramicrocellular PMMA foams made from the low temperature rubbery phase, obtained by saturating the polymer with CO2 at 0°C and 34 atm, was subjected to a second expansion cycle by heating it rapidly to temperatures in the range 30 to 120°C. The blowing agent for the secondary expansion was either the residual CO2 in the foam at about 19 wt% level or fresh CO2 re-equilibrated at 0°C and 34 atm to a loading level of about 29 wt%. In the former case, the second expansion cycle led to lower foam densities whereas in the latter case it led to stretching and re-orientation of the cell walls with no significant gain in further foam density reduction or cell density increase.
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2011 ◽
Vol 77
(23)
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pp. 8295-8302
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1998 ◽
Vol 152
(4-5)
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pp. 473-479
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2011 ◽
Vol 2011
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pp. 1-14
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2010 ◽
Vol 57
(2)
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pp. 198-204
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2013 ◽
Vol 84
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pp. 195-204
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2003 ◽
Vol 74
(3)
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pp. 1909-1912
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