Fatigue response of a solid state self-healing resin

2020 ◽  
pp. 096739112095509
Author(s):  
Mohd Suzeren Md Jamil ◽  
Noor Nabilah Muhamad ◽  
Wan Naqiuddin Wan Zulrushdi
Keyword(s):  
Fatigue Life ◽  
Solid State ◽  
Fatigue Behavior ◽  
Fatigue Cracks ◽  
Healing Process ◽  
Fatigue Tests ◽  
Self Healing ◽  
Healing System ◽  
Healing Agent ◽  
Modified Epoxy

The present work verified the capability of a solid state self-healing system for retarding or arresting fatigue cracks in epoxy materials subjected to cyclic loading at room temperature. A solid state self-healing material is demonstrated using a thermosetting epoxy polymer which was modified by incorporating a linear thermoplastic polydiglycidyl ether bisphenol-A (PDGEBA) as a healing agent. The stress-controlled constant amplitude (CA) tensile fatigue behavior at stress ratio, R = 0.1 and frequency 10 Hz for both the neat and the modified epoxy was investigated. Fatigue life and residual strength degradation were continuously monitored during the fatigue tests. The modified epoxy fatigue life was shown to be increased by ∼50% after healing periods. The fatigue-healing process was proven through the surface and cross-section resin morphology analyses using microscopy optic and scanning electron microscope (SEM). On the whole, the solid state self-healing system has proven to be very effective in obstructing fatigue crack propagation, effectively improved the self-healing polymeric material to achieve higher endurance limits.

scholarly journals Dual Monitoring of Cracking and Healing in Self-healing Coatings using Microcapsules Loaded with Two Fluorescent Dyes

2019 ◽  
Author(s):  
Young Kyu Song ◽  
Tae Hee Lee ◽  
Jin Chul Kim ◽  
Kyu Cheol Lee ◽  
Sang Ho Lee ◽  
...  
Keyword(s):  
Solid State ◽  
Fluorescent Dyes ◽  
Urea Formaldehyde ◽  
Uv Curing ◽  
Coating System ◽  
Self Healing ◽  
Matrix Resin ◽  
Healing System ◽  
Fluorescence Color ◽  
Healing Agent

We report the development of an extrinsic self-healing coating system that shows no fluorescence from the intact coating, yellowish fluorescence in cracked regions, and greenish fluorescence in healed regions, thus allowing the separate monitoring of cracking and healing of coatings. This fluorescence monitoring self-healing system consisted of a top coating, an epoxy matrix resin containing mixed dye-loaded in single microcapsule. The dye-loaded microcapsules consisted of a poly(urea-formaldehyde) shell encapsulating a healing agent containing MAT-PDMS and styrene, a photo-initiator and a mixture of two dyes, one that fluoresces only in the solid state (DCM) and a second that fluoresces dramatically increased in the solid than solution state (4-TPAE). A mixture of the healing agent, photo-initiator and the two dyes was yellow due to fluorescence from DCM. On UV curing of this mixture, however, the color changed from yellow to green and the fluorescence intensity increased due to fluorescence from 4-TPAE in the solid state. When a self-healing coating embedded with microcapsules containing the DCM/4-TPAE dye mixture was scratched, the damaged region exhibited a yellowish color that changed to green after healing. Thus, the self-healing system reported here allows the separate monitoring of cracking and healing based on changes in fluorescence color.

scholarly journals Dual Monitoring of Cracking and Healing in Self-healing Coatings Using Microcapsules Loaded with Two Fluorescent Dyes

Molecules ◽  
2019 ◽  
Vol 24 (9) ◽  
pp. 1679 ◽  
Author(s):  
Young Kyu Song ◽  
Tae Hee Lee ◽  
Jin Chul Kim ◽  
Kyu Cheol Lee ◽  
Sang-Ho Lee ◽  
...  
Keyword(s):  
Solid State ◽  
Fluorescent Dyes ◽  
Urea Formaldehyde ◽  
Uv Curing ◽  
Coating System ◽  
Self Healing ◽  
Matrix Resin ◽  
Healing System ◽  
Fluorescence Color ◽  
Healing Agent

We report the development of an extrinsic, self-healing coating system that shows no fluorescence from intact coating, yellowish fluorescence in cracked regions, and greenish fluorescence in healed regions, thus allowing separate monitoring of cracking and healing of coatings. This fluorescence-monitoring self-healing system consisted of a top coating and an epoxy matrix resin containing mixed dye loaded in a single microcapsule. The dye-loaded microcapsules consisted of a poly(urea-formaldehyde) shell encapsulating a healing agent containing methacryloxypropyl-terminated polydimethylsiloxane (MAT-PDMS), styrene, a photo-initiator, and a mixture of two dyes: one that fluoresced only in the solid state (DCM) and a second that fluoresced dramatically in the solid than in the solution state (4-TPAE). A mixture of the healing agent, photo-initiator, and the two dyes was yellow due to fluorescence from DCM. On UV curing of this mixture, however, the color changed from yellow to green, and the fluorescence intensity increased due to fluorescence from 4-TPAE in the solid state. When a self-healing coating embedded with microcapsules containing the DCM/4-TPAE dye mixture was scratched, the damaged region exhibited a yellowish color that changed to green after healing. Thus, the self-healing system reported here allows separate monitoring of cracking and healing based on changes in fluorescence color.

scholarly journals Quantitative Analysis of Inclusion Engineering on the Fatigue Property Improvement of Bearing Steel

Metals ◽  
2019 ◽  
Vol 9 (4) ◽  
pp. 476 ◽  
Author(s):  
Chao Gu ◽  
Min Wang ◽  
Yanping Bao ◽  
Fuming Wang ◽  
Junhe Lian
Keyword(s):  
Fatigue Life ◽  
Quantitative Analysis ◽  
Critical Size ◽  
Fatigue Behavior ◽  
Fatigue Cracks ◽  
Fatigue Property ◽  
Bearing Steel ◽  
Fatigue Properties ◽  
Bearing Steels ◽  
Inclusion Distribution

The fatigue property is significantly affected by the inner inclusions in steel. Due to the inhomogeneity of inclusion distribution in the micro-scale, it is not straightforward to quantify the effect of inclusions on fatigue behavior. Various investigations have been performed to correlate the inclusion characteristics, such as inclusion fraction, size, and composition, with fatigue life. However, these studies are generally based on vast types of steels and even for a similar steel grade, the alloy concept and microstructure information can still be of non-negligible difference. For a quantitative analysis of the fatigue life improvement with respect to the inclusion engineering, a systematic and carefully designed study is still needed to explore the engineering dimensions of inclusions. Therefore, in this study, three types of bearing steels with inclusions of the same types, but different sizes and amounts, were produced with 50 kg hot state experiments. The following forging and heat treatment procedures were kept consistent to ensure that the only controlled variable is inclusion. The fatigue properties were compared and the inclusions that triggered the fatigue cracks were analyzed to deduce the critical sizes of inclusions in terms of fatigue failure. The results show that the critical sizes of different inclusion types vary in bearing steels. The critical size of the spinel is 8.5 μm and the critical size of the calcium aluminate is 13.5 μm under the fatigue stress of 1200 MPa. In addition, with the increase of the cleanliness of bearing steels, the improvement of fatigue properties will reach saturation. Under this condition, further increasing of the cleanliness of the bearing steel will not contribute to the improvement of fatigue property for the investigated alloy and process design.

High-cycle fatigue tests of pretensioned concrete beams

PCI Journal ◽  
2022 ◽  
Vol 67 (1) ◽  
Author(s):  
Jörn Remitz ◽  
Martin Empelmann
Keyword(s):  
Fatigue Life ◽  
High Cycle Fatigue ◽  
Concrete Beams ◽  
Fatigue Behavior ◽  
Fatigue Tests ◽  
Design Methods ◽  
Test Results ◽  
Cycle Fatigue ◽  
Pretensioned Concrete ◽  
Current Design

Pretensioned concrete beams are widely used as bridge girders for simply supported bridges. Understanding the fatigue behavior of such beams is very important for design and construction to prevent fatigue failure. The fatigue behavior of pretensioned concrete beams is mainly influenced by the fatigue of the prestressing strands. The evaluation of previous test results from the literature indicated a reduced fatigue life in the long-life region compared with current design methods and specifications. Therefore, nine additional high-cycle fatigue tests were conducted on pretensioned concrete beams with strand stress ranges of about 100 MPa (14.5 ksi). The test results confirmed that current design methods and specifications overestimate the fatigue life of embedded strands in pretensioned concrete beams.

scholarly journals Changing in Fatigue Life of 300 M Bainitic Steel After Laser Carburizing and Plasma Nitriding

2018 ◽  
Vol 165 ◽  
pp. 21002 ◽  
Author(s):  
Antonio J. Abdalla ◽  
Douglas Santos ◽  
Getúlio Vasconcelos ◽  
Vladimir H. Baggio-Scheid ◽  
Deivid F. Silva
Keyword(s):  
Mechanical Properties ◽  
Fatigue Life ◽  
Plasma Nitriding ◽  
Fatigue Behavior ◽  
High Strength ◽  
Tensile Tests ◽  
Steel Sample ◽  
Fatigue Tests ◽  
300M Steel ◽  
Structural Applications

In this work 300M steel samples is used. This high-strength steel is used in aeronautic and aerospace industry and other structural applications. Initially the 300 M steel sample was submitted to a heat treatment to obtain a bainític structure. It was heated at 850 °C for 30 minutes and after that, cooled at 300 °C for 60 minutes. Afterwards two types of surface treatments have been employed: (a) using low-power laser CO2 (125 W) for introducing carbon into the surface and (b) plasma nitriding at a temperature of 500° C for 3 hours. After surface treatment, the metallographic preparation was carried out and the observations with optical and electronic microscopy have been made. The analysis of the coating showed an increase in the hardness of layer formed on the surface, mainly, among the nitriding layers. The mechanical properties were analyzed using tensile and fatigue tests. The results showed that the mechanical properties in tensile tests were strongly affected by the bainitic microstructure. The steel that received the nitriding surface by plasma treatment showed better fatigue behavior. The results are very promising because the layer formed on steel surface, in addition to improving the fatigue life, still improves protection against corrosion and wear.

On the Effect of Electrodischarge Drilling on the Fatigue Life of Inconel 718

2014 ◽  
Vol 891-892 ◽  
pp. 1451-1456
Author(s):  
Elena Bassoli ◽  
Andrea Baldini ◽  
Andrea Gatto ◽  
Antonio Strozzi ◽  
Lucia Denti
Keyword(s):  
Fatigue Life ◽  
Inconel 718 ◽  
Metal Cutting ◽  
Fatigue Behavior ◽  
Fatigue Tests ◽  
Aerospace Applications ◽  
Rotating Bending Fatigue ◽  
Cutting Operation ◽  
Rotating Bending ◽  
Superposition Effect

Difficult-to cut-materials are associated with premature tool failure, most likely in the case of complex geometries and this shapes. However, Nickel-based alloys are commonly used in high-temperature and aerospace applications, where thin deep holes are often required. Then, the only viable manufacturing solution relies on non-contact processes, like electrodischarge (ED) drilling. Morphology of ED machined surfaces is significantly different than obtained by metal-cutting operation and is known to jeopardize fatigue strength, but the extent needs to be gauged and related to the process parameters. Aim of the paper is to study the effect of holes (0.8 mm diameter, aspect ratio 10) produced by ED drilling on the fatigue life of Inconel 718. Rotating bending fatigue tests are carried out on specimens drilled under two ED setups, as well as with a traditional cutting tool. Specimens free from holes are fatigued under the same conditions for comparison. Based on previous studies, extremal ED parameters are selected, giving best surface finish versus highest productivity. S-N curves show that the ED process causes a decrease of the fatigue resistance with respect to traditional drilling, whereas the effect of different ED setups is negligible. Maximum productivity can thus be pursued with no threat to fatigue performance. The fatigue limit variation is quantified by using the superposition effect principle: ED drilling causes an increase of the stress concentration factor around 25% if compared to traditional drilling. The macroscopic fatigue behavior is integrated with a study of the effects of the different drilling processes in the micro-scale, by means of a microstructural and fractographic analysis.

High Cycle Fatigue Behavior of Recycled Additive Manufactured Electron Beam Melted Titanium Ti6Al4V

2020 ◽  
Author(s):  
Melody Mojib ◽  
Rishi Pahuja ◽  
M. Ramulu ◽  
Dwayne Arola
Keyword(s):  
Electron Beam ◽  
Fatigue Life ◽  
Rough Surface ◽  
High Cycle Fatigue ◽  
Fatigue Behavior ◽  
High Strength ◽  
Fatigue Tests ◽  
Cycle Fatigue ◽  
Initiation And Propagation ◽  
Powder Recycling

Abstract Metal Additive Manufacturing (AM) has become a popular method for producing complex and unique geometries, especially gaining traction in the aerospace and medical industries. With the increase in adoption of AM and the high cost of powder, it is critical to understand the effects of powder recycling on part performance to move towards material qualification and certification of affordable printed components. Due to the limitations of the Electron Beam Melting (EBM) process, current as-printed components are susceptible to failure at limits far below wrought metals and further understanding of the material properties and fatigue life is required. In this study, a high strength Titanium alloy, Ti-6Al-4V, is recycled over time and used to print fatigue specimens using the EBM process. Uniaxial High Cycle Fatigue tests have been performed on as-printed and polished cylindrical specimens and the locations of crack initiation and propagation have been determined through the use of a scanning electron microscope. This investigation has shown that the rough surface exterior is far more detrimental to performance life than the powder degradation occurring due to powder reuse. In addition, the effects of the rough surface exterior as a stress concentration is evaluated using the Arola-Ramulu. The following is a preliminary study of the effects powder recycling and surface treatments on EBM Ti-6Al4V fatigue life.

scholarly journals The Influence of Laser Shock Peening on Fatigue Properties of AA2024-T3 Alloy with a Fastener Hole

Metals ◽  
2020 ◽  
Vol 10 (4) ◽  
pp. 495
Author(s):  
Ruslan Sikhamov ◽  
Fedor Fomin ◽  
Benjamin Klusemann ◽  
Nikolai Kashaev
Keyword(s):  
Fatigue Life ◽  
Fatigue Cracks ◽  
Initial Crack ◽  
Fatigue Tests ◽  
Laser Shock Peening ◽  
Fatigue Properties ◽  
Hole Drilling ◽  
Laser Shock ◽  
Fastener Hole ◽  
Shock Peening

The objective of the present study was to estimate the influence of laser shock peening on the fatigue properties of AA2024-T3 specimens with a fastener hole and to investigate the possibility to heal the initial cracks in such specimens. Fatigue cracks of different lengths were introduced in the specimens with a fastener hole before applying laser shock peening. Deep compressive residual stresses, characterized by the hole drilling method, were generated into the specimens by applying laser shock peening on both sides. Subsequently, the specimens were subjected to fatigue tests. The results show that laser shock peening has a positive effect regarding the fatigue life improvement in the specimens with a fastener hole. In addition, laser shock peening leads to a healing effect on fatigue cracks. The efficiency of this effect depends on the initial crack length. The effect of laser shock peening on the fatigue life periods was determined by using resonant frequency graphs.

The Effects of Mechanical Properties on Fatigue Behavior of ECAPed AA7075

2016 ◽  
Vol 35 (3) ◽  
pp. 225-234 ◽  
Author(s):  
Hasan Kaya ◽  
Mehmet Uçar
Keyword(s):  
Electron Microscope ◽  
Fatigue Life ◽  
Fatigue Behavior ◽  
Optical Microscope ◽  
Fatigue Tests ◽  
Angular Pressing ◽  
Four Point Bending ◽  
Selected Area Electron Diffraction ◽  
Transmission Electron ◽  
Hardness Values

AbstractIn this study, the effects of equal channel angular pressing (ECAP) on high-cycle fatigue and fatigue surface morphology of AA7075 have been investigated at a constant temperature (483 K) and the “C” route for four passes at ECAP process. ECAPed and as-received specimens were tested by four-point bending fatigue device. Fatigue tests were carried out by using 100, 120 and 140 MPa strength values. ECAPed specimens were characterized for each pass with optical microscope (OM), scanning electron microscope (SEM), energy-dispersive spectroscope (EDS), transmission electron microscope (TEM), selected area electron diffraction (SAED) and hardness measurements. Fracture surfaces of the specimens were also characterized with SEM. The results show that the highest hardness values (137 HV) and the best fatigue life (5.4 × 107for 100 MPa) were measured in ECAPed four-pass sample. For this reason hardness values and fatigue life were increased with increasing number of severe plastic deformation (SPD) process.

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