scholarly journals Optimization of molding process parameters for CF/PEEK composites based on Taguchi method

2021 ◽  
Vol 30 ◽  
pp. 263498332110018
Author(s):  
Guangming Dai ◽  
Lihua Zhan ◽  
Chenglong Guan ◽  
Minghui Huang

In this article, nine groups of laminates were prepared according to the Taguchi L9(33) test array to study the influence of three process parameters, including molding pressure, molding temperature, and holding time on the performance of unidirectional carbon fiber/polyetheretherketone (CF/PEEK) laminates. A differential scanning calorimetry test was employed to select a reasonable process parameters range. The transverse tensile strength of the laminates was measured, and the fiber–matrix interfacial bonding behavior of the tested samples was analyzed by scanning electron microscopy. The results showed that the significance of factors to transverse tensile strength were molding temperature, holding time, and molding pressure in sequence. The optimal molding process parameters for CF/PEEK composite laminate were molding temperature of 400°C, molding pressure of 3 MPa, and holding time of 30 min. The optimization results were meaningful for the extension and application of thermoplastic composites.

Author(s):  
Satoshi Kobayashi ◽  
Toshiko Osada

Abstract Effect of molding condition on resin impregnation behavior and the associated mechanical properties were investigated for carbon fabric reinforced thermoplastic composites. Carbon fiber yarn (TORAYCA, Toray) was used as a reinforcement, and thermoplastic PI (AURUM PL 450 C, Mitsui Chemicals) was used as the matrix. CFRTP textile composites were compression-molded with a hot press system under the molding temperature, 390 °C, 410 °C and 430 °C, molding pressure 2 MPa and 4 MPa and molding time 0∼300 s. In order to evaluate the impregnated state, cross sectional observation was performed with an optical microscope. Specimen cross-section was polished and finished with alumina slurry for a clear observation. The images observed were processed through image processing software to obtained impregnation ratio which defined as the resin impregnation area to the cross-sectional area of a fiber yarn. Resin impregnation was accelerated with molding temperature and pressure. At molding temperature more than 410 °C, resin impregnation was similar irrespective of temperature. Tensile test results indicated that modulus and strength increased with resin impregnation. Resin impregnation during molding was predicted using the analytical model based on Darcy’s law and continuity condition. The analysis could successfully predict the impregnation behavior despite the difference in molding pressure and temperature.


2020 ◽  
Vol 54 (23) ◽  
pp. 3297-3312
Author(s):  
Caitlin M Arndt ◽  
Nelson V de Carvalho ◽  
Michael W Czabaj

Due to the observed dependence of transverse-tensile strength, Y T, on test geometry and specimen size, there is no consensus regarding a test method that can uniquely measure Y T. This study reexamines the characterization of Y T by comparing results from established flexure tests with results from a new tensile test that exhibits consistent failure in the gage region. Additionally, the effects of surface preparation and direction of transverse fracture are investigated. Results show that Y T is inversely proportional to specimen volume and surface roughness and is insensitive to direction of transverse fracture. The relationship between specimen volume and Y T is adequately captured by Weibull strength-scaling theory, except at the tails of the Y T distributions. However, specimens exhibited microcracking prior to failure, which violates the “weak-link” assumption of the Weibull theory. These findings highlight the challenges of using deterministic Y T values in progressive damage analysis.


1996 ◽  
Vol 5 (4) ◽  
pp. 096369359600500
Author(s):  
J Ziao ◽  
J Tao

In this paper, we directed our attention to the interlaminar defects and their influence on the interlaminar strengths. With the aid of a S-570 scanning electron microscope, the morphology and distribution of interlaminar defects were inspected and documented. According to their shape, size and cause of formation, the defects were classified into five types: flakiness void, irregular shaped debond, local imperfectly cured resin, debond in two multi-directional plies, and inhomogeneous fibers and the large scale debond by these fibers. The cause of defects formation was discussed by analyzing the manufacturing process of composites. The influence of defects on the interlaminar strength and its mechanism was analyzed experimentally and theoretically. The results indicate that these defects, with different effects, decrease the interlaminar strength because they form interlaminar cracks, and the interlaminar shear strength is less affected than interlaminar tensile strength, which is measured according to GB4944 test method. To comprehend defects distribution effect, a four-point-bending test method was introduced to measure the interlaminar peel strength, and a discussion was made on the correlation between the interlaminar tensile strength, interlaminar peel strength and in-plane transverse tensile strength. Finally the concept of interlaminar defect coefficient, which can be used to characterize the defects, was set up and the formula to calculate it was proposed.


2014 ◽  
Vol 695 ◽  
pp. 155-158 ◽  
Author(s):  
Dandi Bachtiar ◽  
Januar Parlaungan Siregar ◽  
Ahmad Syahrizan bin Sulaiman ◽  
Mohd Ruzaimi bin Mat Rejab

Study on hybridization of two types of natural fibres reinforced thermoplastic composites was an alternative option in research on natural composites. This paper presents the investigation on tensile properties of combining sugar palm and kenaf fibres reinforced polypropylene composites. The hybrid composites were prepared with different amounts of fibres (i.e. 10%, 20% and 30% by weight percent) while the ratios between sugar palm and kenaf fibre are 30:70, 50:50 and 70:30. The composites have been fabricated using melt mixer technique and followed by compression molding process. The specimens were cut according ASTM Standard D638 for conducting the tensile testing. The results shown that tensile strength of composites tend to decreased when the content of loading fibres increased. Among the composites with different ratios, the hybrid composites that contain more kenaf fibres exhibit the higher value in tensile strength than the composites that contain more sugar palm fibres.


2018 ◽  
Vol 25 (3) ◽  
pp. 489-499 ◽  
Author(s):  
V.R. Giri Dev ◽  
A.K.P. Dhanakodi

Abstract Natural fiber reinforced thermoplastic composites using flax and polypropylene were prepared using compression molding process. Needle punched nonwovens were used as preforms for preparing the composites. Three variables namely fiber weight proportion, areal weight of the mat, and needling density were chosen for the study. Modified Taguchi L18 experimental design with dummy variable was chosen for the study and the effect of the above variables on tensile, flexural, and impact properties of the composites were studied. By altering the fiber weight proportion and areal weight of the mat, tensile and flexural properties improved. An increase in 34% of tensile strength and 40% of flexural strength has been observed. Impact properties of the composites were significantly altered by modifying the process variables. Increasing the needling density led to a decrease in overall mechanical properties of the composites.


Metals ◽  
2018 ◽  
Vol 8 (12) ◽  
pp. 1086 ◽  
Author(s):  
Dilpreet Singh ◽  
Abhishek Rana ◽  
Pawan Sharma ◽  
Pulak Mohan Pandey ◽  
Dinesh Kalyanasundaram

Pressureless sintering is a powder metallurgical process wherein the powder particles are sintered without the aid of any compressive force. Though this additive manufacturing process is economical, the strength of the component is undermined due to the presence of pores; the elimination of which is a challenge. In this work, the optimal process parameters for the pressureless microwave sintering of a grade 5 titanium alloy that yields higher tensile strength and minimum sizes of pores were obtained. The three process parameters (sintering temperature, heating rate, and holding time) were experimented at five different levels using the design of experiments (DOE). Post sintering, the tensile strength was assessed as per ASTM standard B925-15, while the pore size was evaluated, non-destructively, using micro-computed tomography (μ-CT). The optimal process parameters that yielded minimum size pores were: sintering temperature—1293 °C, heating rate— 6.65 C/minute; and holding time—72 min.


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