Non Invasive Analysis of Natural Resin Extracts

1998 ◽  
Vol 6 (A) ◽  
pp. A211-A214 ◽  
Author(s):  
M. Ionita-Manzatu ◽  
I. Scarlat ◽  
M. Vasilescu ◽  
M. Puica ◽  
G. Blagoi ◽  
...  

The NIR reflection spectra of some purified conifer resin extracts used as a biologically active ingredient in pharmaceutical ointments were employed to reveal the possibility of applying NIR spectroscopy to quality control. The samples were analysed beforehand (by HPLC and compendial methods) in order to characterise them. The fingerprint of this raw material was achieved by using the standard methods recommended by the NSAS operating protocol (for the spectrometer delivered by NIRSystems Inc.). The poor quality samples were also tested by means of same protocol, the limits of method being pointed out.

AYUSHDHARA ◽  
2020 ◽  
pp. 2838-2846
Author(s):  
Vij Divya ◽  
Mishra Rajesh Kumar

Meda is one of the most important plants included in Astavarga. This plant is used in variety of Ayurvedic formulations such as Cyavanprasa. Dried underground parts (rhizomes) of this plant are used for medicinal purpose. This plant is claimed to possess rejuvenating, health promoting, immune system strengthening, anti-oxidant and cell regenerating properties. Also claimed to promote body fat, healing fractures, control fever, abdominal thirst, diabetic condition, seminal weakness, and as a cure for Vata, Pitta and Rakta dosa. The demand of this herb is increasing day by day but due to scarcity of this plant in wild, unaware about authentic botanical source, non-existing cultivation practices there is widespread problem of adulteration or substitution with other plants. The poor quality of raw material affect the quality of end product formed. So by taking into account the above situation this systematic review/ metadata analysis has conducted to find out adulteration in Meda.


2000 ◽  
Vol 66 ◽  
pp. 209-255 ◽  
Author(s):  
Francis Wenban-Smith ◽  
Clive Gamble ◽  
Arthur Apsimon

The site at Red Barns was excavated in 1975, but the large lithic collection remained unstudied following preliminary examination. This paper reports on further analysis of the lithic material from the site, together with a reappraisal of the faunal remains and original mineralogical analyses, and the results of processing sediment samples from the 1975 excavation. An abundant molluscan assemblage was recovered from the deposits covering the main archaeological horizon, allowing climatic/environmental reconstruction and amino acid dating. The synthesis of these data indicates the site to be older than previously thought, dating to between 425,000 and 200,000 BP.Analysis of the lithic material has suggested that the site is an undisturbed palimpsest of flint tools and debitage. The poor, severely frost-fractured nature of the raw material used for knapping, together with the location of the site on a Chalk outcrop, have enabled investigation of some assumptions about the influences upon knapping technology of i) poor quality raw material and ii) local availability of flint fresh from Chalk bedrock. The persistent manufacture of finely worked plano-convex handaxes suggests that, even in an area where fresh Chalk flint must have been abundant, the immediately available poor quality flint source was not a bar to formation of an assemblage dominated by handaxe production. Secondly, the emphasis on carefully shaped pointed plano-convex handaxes suggests that this shape was both deliberately imposed and not dictated by a lack of local availability of flint fresh from the Chalk. Behaviour at the site was investigated by analysis of the organisation of the lithic production and it was demonstrated that, while some handaxes and flake-tools were abandoned at the site and some flake core reduction also took place there, the dominant pattern was for handaxes to be made at the site and then removed and abandoned elsewhere.


2020 ◽  
pp. 34-36
Author(s):  
M. A. Pokhaznikova ◽  
E. A. Andreeva ◽  
O. Yu. Kuznetsova

The article discusses the experience of teaching and conducting spirometry of general practitioners as part of the RESPECT study (RESearch on the PrEvalence and the diagnosis of COPD and its Tobacco-related aetiology). A total of 33 trained in spirometry general practitioners performed a study of 3119 patients. Quality criteria met 84.1% of spirometric studies. The analysis of the most common mistakes made by doctors during the forced expiratory maneuver is included. The most frequent errors were expiration exhalation of less than 6s (54%), non-maximal effort throughout the test and lack of reproducibility (11.3%). Independent predictors of poor spirogram quality were male gender, obstruction (FEV1 /FVC<0.7), and the center where the study was performed. The number of good-quality spirograms ranged from 96.1% (95% CI 83.2–110.4) to 59.8% (95% CI 49.6–71.4) depending on the center. Subsequently, an analysis of the reasons behind the poor quality of research in individual centers was conducted and the identified shortcomings were eliminated. The poor quality of the spirograms was associated either with the errors of the doctors who undertook the study or with the technical malfunctions of the spirometer.


2016 ◽  
Vol 1 (3) ◽  
Author(s):  
Ani Saifuza Abd Shukor ◽  
Muhammad Fadhil Muhammad ◽  
Shamsida Saidan Khaderi ◽  
Faridah Muhammad Halil

The shift to an integrated IBS construction approach requires enhanced supply chain integration to improve the productivity as well as the poor quality of human behavioual aspect in IBS project. This paper is to identify the challenges at each tier between players to facilitate supply chain integration among the IBS players. Findings adopted from semi-structured interview revealed the critical attitude issues of human factors, lack of interaction and sharing knowledge between interdisciplinary people. The findings of this study is useful to improve integration of supply chain and enhance innovation and sharing interaction between players in the IBS Malaysian construction project environment.© 2016. The Authors. Published for AMER ABRA by e-International Publishing House, Ltd., UK. Peer–review under responsibility of AMER (Association of Malaysian Environment-Behaviour Researchers), ABRA (Association of Behavioural Researchers on Asians) and cE-Bs (Centre for Environment-Behaviour Studies), Faculty of Architecture, Planning & Surveying, Universiti Teknologi MARA, Malaysia.Keywords: Construction Environment; Industrialised Building System; Integration and Supply Chain 


2020 ◽  
pp. 1-17
Author(s):  
Vikas Kumar

The quality of metadata is a crucial determinant of usability/interpretability of data. This paper draws attention to the poor quality of India’s government statistics and the paucity of metadata necessary to understand the problems. The paper suggests that there has been a decline in India both in terms of the availability and quality of metadata for key government sources of information including maps, decennial population censuses and National Sample Surveys amidst growing sophistication in the understanding of metadata. The poor quality of metadata impairs cross-sectional as well as inter-temporal comparisons and policymaking apart from concealing biases and lapses of government statisticians. The paper draws on the experience of three states – erstwhile Jammu and Kashmir, Manipur and Nagaland – where government statistics have been affected by serious errors that are not well-understood due to the lack of adequate metadata.


2011 ◽  
Vol 243-249 ◽  
pp. 1360-1365 ◽  
Author(s):  
Wei Rong Lü ◽  
Meng Wang ◽  
Xi Jun Liu

The micro-model, which the brick and the mortar model are separated, is used to analyze masonry. Meanwhile, the mortar is divided into three layers along the thickness direction to obtain the internal mechanical behavior of mortar, and the vertical mortar joint strength is taken as 50% strength of the horizontal mortar joint for considering the poor quality of vertical mortar joint. The compressive ultimate load and failure mode of masonry taken from the finite element analysis result, especially the vertical cracks throughout all bricks and mortar and change of brick and mortar strain, are in agreement with the experimental results. It shows that the micro-model and method adopted in paper are able to effectively apply in nonlinear structural analysis for masonry.


2014 ◽  
Vol 50 (3) ◽  
pp. 671-704 ◽  
Author(s):  
CHRISTINA BEHME

The Science of Language, published in the sixth decade of Noam Chomsky's linguistic career, defends views that are visibly out of touch with recent research in formal linguistics, developmental child psychology, computational modeling of language acquisition, and language evolution. I argue that the poor quality of this volume is representative of the serious shortcomings of Chomsky's recent scholarship, especially of his criticism of and contribution to debates about language evolution. Chomsky creates the impression that he is quoting titbits of a massive body of scientific work he has conducted or is intimately familiar with. Yet his speculations reveal a lack of even basic understanding of biology, and an unwillingness to engage seriously with the relevant literature. At the same time, he ridicules the work of virtually all other theorists, without spelling out the views he disagrees with. A critical analysis of the ‘Galilean method’ demonstrates that Chomsky uses appeal to authority to insulate his own proposals against falsification by empirical counter-evidence. This form of discourse bears no serious relation to the way science proceeds.


2021 ◽  
pp. 096703352098731
Author(s):  
Adenilton C da Silva ◽  
Lívia PD Ribeiro ◽  
Ruth MB Vidal ◽  
Wladiana O Matos ◽  
Gisele S Lopes

The use of alcohol-based hand sanitizers is recommended as one of several strategies to minimize contamination and spread of the COVID-19 disease. Current reports suggest that the virucidal potential of ethanol occurs at concentrations close to 70%. Traditional methods of verifying the ethanol concentration in such products invite potential errors due to the viscosity of chemical components or may be prohibitively expensive to undertake in large demand. Near infrared (NIR) spectroscopy and chemometrics have already been used for the determination of ethanol in other matrices and present an alternative fast and reliable approach to quality control of alcohol-based hand sanitizers. In this study, a portable NIR spectrometer combined with classification chemometric tools, i.e., partial least square discriminant analysis (PLS–DA) and linear discriminant analysis with successive algorithm projection (SPA–LDA) were used to construct models to identify conforming and non-conforming commercial and laboratory synthesized hand sanitizer samples. Principal component analysis (PCA) was applied in an exploratory data study. Three principal components accounted for 99% of data variance and demonstrate clustering of conforming and non-conforming samples. The PLS–DA and SPA–LDA classification models presented 77 and 100% of accuracy in cross/internal validation respectively and 100% of accuracy in the classification of test samples. A total of 43% commercial samples evaluated using the PLS–DA and SPA–LDA presented ethanol content non-conforming for hand sanitizer gel. These results indicate that use of NIR spectroscopy and chemometrics is a promising strategy, yielding a method that is fast, portable, and reliable for discrimination of alcohol-based hand sanitizers with respect to conforming and non-conforming ethanol concentrations.


Sign in / Sign up

Export Citation Format

Share Document