scholarly journals Properties of polycapillary optics dedicated to low-energy parallel-beam wavelength-dispersive spectrometer for synchrotron-based X-ray fluorescence study

2021 ◽  
Author(s):  
Pawel Jagodzinski ◽  
Marek Pajek ◽  
Dariusz Banas ◽  
Aldona Kubala-Kukus ◽  
Jakub Szlachetko ◽  
...  
1997 ◽  
Vol 3 (S2) ◽  
pp. 889-890 ◽  
Author(s):  
R. Agnello ◽  
J. Howard ◽  
J. McCarthy ◽  
D. OHara

There has been much interest in the last few years in the technique for focusing x-rays into high intensity spots using tapered glass capillaries or other forms of grazing incident x-ray reflectors. The resulting microbeams have been used in applications that include microfluorescence, microdiffraction, tomography and lithography. Instead of focusing x-rays to a spot, a collimating optic can be used to capture x-rays from a point source and turn them into a collimated parallel beam at the exit aperture to the optic. Kirkland et. al. have pointed out that the use of such an optic could provide enhanced detection sensitivity in wavelength dispersive spectroscopy.We have developed a grazing incidence collimating x-ray optic that can be coupled to a simple wavelength dispersive spectrometer (WDS). This combined instrument was designed to enhance the intensity of x-rays from a sample by an order of magnitude or more in the energy range of 0 to 1 keV compared to a conventional WDS.


1975 ◽  
Vol 19 ◽  
pp. 587-596 ◽  
Author(s):  
Louis N. Koppel

Self-scanning photodiode arrays were tested for their ability to measure the spatial distribution of low-energy x rays in a wavelength dispersive spectrometer. X-ray spectral sensitivity was measured with a calibrated de source of nearly-monochromatic characteristic-x rays with photon energies in the range of 1.5 to 8 keV. Photodiode response was found to be linear with x-ray flux. Exposure to large doses of copper radiation did not effect sensitivity. A mathematical model that describes the experimental data is presented. We found that spatial resolving power was lowered by the dispersal of photogenerated charges. This effect was investigated with collimated beams and is described with a formula that predicts the loss of diode signals.


Author(s):  
Richard L. McConville

A second generation twin lens has been developed. This symmetrical lens with a wider bore, yet superior values of chromatic and spherical aberration for a given focal length, retains both eucentric ± 60° tilt movement and 20°x ray detector take-off angle at 90° to the tilt axis. Adjust able tilt axis height, as well as specimen height, now ensures almost invariant objective lens strengths for both TEM (parallel beam conditions) and STEM or nano probe (focused small probe) modes.These modes are selected through use of an auxiliary lens situ ated above the objective. When this lens is on the specimen is illuminated with a parallel beam of electrons, and when it is off the specimen is illuminated with a focused probe of dimensions governed by the excitation of the condenser 1 lens. Thus TEM/STEM operation is controlled by a lens which is independent of the objective lens field strength.


2021 ◽  
Vol 11 (10) ◽  
pp. 4349
Author(s):  
Tianzhong Xiong ◽  
Wenhua Ye ◽  
Xiang Xu

As an important part of pretreatment before recycling, sorting has a great impact on the quality, efficiency, cost and difficulty of recycling. In this paper, dual-energy X-ray transmission (DE-XRT) combined with variable gas-ejection is used to improve the quality and efficiency of in-line automatic sorting of waste non-ferrous metals. A method was proposed to judge the sorting ability, identify the types, and calculate the mass and center-of-gravity coordinates according to the shading of low-energy, the line scan direction coordinate and transparency natural logarithm ratio of low energy to high energy (R_value). The material identification was satisfied by the nearest neighbor algorithm of effective points in the material range to the R_value calibration surface. The flow-process of identification was also presented. Based on the thickness of the calibration surface, the material mass and center-of-gravity coordinates were calculated. The feasibility of controlling material falling points by variable gas-ejection was analyzed. The experimental verification of self-made materials showed that identification accuracy by count basis was 85%, mass and center-of-gravity coordinates calculation errors were both below 5%. The method proposed features high accuracy, high efficiency, and low operation cost and is of great application value even to other solid waste sorting, such as plastics, glass and ceramics.


Author(s):  
Asahina Shunsuke ◽  
Takahashi Hideyuki ◽  
Takakura Masaru ◽  
Ferdi Schüth ◽  
Terasaki Osamu

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