scholarly journals Measurement of Two Phase Flow

10.14311/716 ◽  
2005 ◽  
Vol 45 (3) ◽  
Author(s):  
J. Novotný ◽  
J. Nožička ◽  
J. Adamec ◽  
L. Nováková

This paper presents the results of experiments with moist wet steam. The aim of the experiment was to measure the velocity of the growth of a condensing nucleus in wet steam dependent on the velocity of condensation. For the experiments in wet steam an experimental setup was designed and constructed, which generated superheated steam at lowered pressure and a temperature of 50 °C. Low pressure and temperature of the hot vapour was chosen in order to minimize the risk of accidental disruption of the wall. The size of the condensing nucleus was measured by the method of Interferometric Particle Imaging (IPI). The IPI method is a technique for determining the particle size of transparent and spherical particles based on calculating the fringes captured on a CCD array. The number of fringes depends on the particle size and on the optical configuration. The experimental setup used is identical with the setup for measuring flow by the stereo PIV method. The only difference is the use of a special camera mount comprising a transparent mirror and enabling both cameras to be focused to one point. We present the results of the development of the growth of a condensing nucleus and histograms of the sizes of all measured particles depending on position and condensation velocity. 

2009 ◽  
Vol 283-286 ◽  
pp. 599-603
Author(s):  
Hikmet Ş. Aybar ◽  
Mohsen Sharifpur ◽  
Roozbeh Vaziri

Many researches have performed some studies about pressure gradient in the one phase flow, particle-liquid two-phase flow and porous media. However, there is no any report about interaction among them. In this study, this interaction idea is developed by using the same particle size for particle-liquid two-phase flow and porous media. For the experimental study, an apparatus is designed, and at the first step one phase water pressure gradient is investigated, next in the further steps, little by little spherical particles are added to the cycle till accumulation of the particles did not allow any movement to the particles (i.e. porous media occur), and after that well pack porous media is investigated. The results confirm the relation between pressure gradient over mass flow rate in the one phase flow, particle-liquid two-phase flow and porous media obeys as a parabolic curve.


2001 ◽  
Vol 32 (4-6) ◽  
pp. 5
Author(s):  
A. P. Sevast'yanov ◽  
I. V. An ◽  
S. I. Vainshtein ◽  
Yu. A. Sevast'yanov ◽  
A. V. Sidnev ◽  
...  

2020 ◽  
Vol 14 (3) ◽  
pp. 210-224
Author(s):  
Gayatri Patel ◽  
Bindu K.N. Yadav

Background: The purpose of this study was to formulate, characterize and in-vitro cytotoxicity of 5-Fluorouracil loaded controlled release nanoparticles for the treatment of skin cancer. The patents on nanoparticles (US8414926B1), (US61654404A), (WO2007150075A3) etc. helped in the selection polymers and method for the preparation of nanoparticles. Methods: In the present study nanoparticles were prepared by simple ionic gelation method using various concentrations of chitosan and sodium tripolyphosphate (TPP). Several process and formulation parameters were screened and optimized using 25-2 fractional factorial design. The prepared nanoparticles were evaluated for particle size, shape, charge, entrapment efficiency, crosslinking mechanism and drug release study. Results: The optimized 5-Fluorouracil loaded nanoparticle were found with particle size of of 320±2.1 nm, entrapment efficiency of 85.12%± 1.1% and Zeta potential of 29mv±1mv. Scanning electron microscopy and dynamic light scattering technique revealed spherical particles with uniform size. The invitro release profile showed controlled release up to 24 hr. Further study was carried using A375 basal cell carcinoma cell-line to elucidate the mechanism of its cytotoxicity by MTT assay. Conclusion: These results demonstrate that the possibility of delivering 5-Fluorouracil to skin with enhanced encapsulation efficiency indicating effectiveness of the formulation for treatment of basal cell carcinoma type of skin cancer.


Author(s):  
Spyridon Damilos ◽  
Ioannis Alissandratos ◽  
Luca Panariello ◽  
Anand N. P. Radhakrishnan ◽  
Enhong Cao ◽  
...  

AbstractA continuous manufacturing platform was developed for the synthesis of aqueous colloidal 10–20 nm gold nanoparticles (Au NPs) in a flow reactor using chloroauric acid, sodium citrate and citric acid at 95 oC and 2.3 bar(a) pressure. The use of a two-phase flow system – using heptane as the continuous phase – prevented fouling on the reactor walls, while improving the residence time distribution. Continuous syntheses for up to 2 h demonstrated its potential application for continuous manufacturing, while live quality control was established using online UV-Vis photospectrometry that monitored the particle size and process yield. The synthesis was stable and reproducible over time for gold precursor concentration above 0.23 mM (after mixing), resulting in average particle size between 12 and 15 nm. A hydrophobic membrane separator provided successful separation of the aqueous and organic phases and collection of colloidal Au NPs in flow. Process yield increased at higher inlet flow rates (from 70 % to almost 100 %), due to lower residence time of the colloidal solution in the separator resulting in less fouling in the PTFE membrane. This study addresses the challenges for the translation of the synthesis from batch to flow and provides tools for the development of a continuous manufacturing platform for gold nanoparticles.Graphical abstract


2021 ◽  
Vol 40 (1) ◽  
pp. 178-192
Author(s):  
Wen-Qiang Ren ◽  
Lu Wang ◽  
Zheng-Liang Xue ◽  
Cheng-Zhi Li ◽  
Hang-Yu Zhu ◽  
...  

Abstract Thermodynamic analysis of the precipitation behavior, growth kinetic, and control mechanism of MnS inclusion in U75V heavy rail steel was conducted in this study. The results showed that solute element S had a much higher segregation ratio than that of Mn, and MnS would only precipitate in the solid–liquid (two-phase) regions at the late stage during the solidification process at the solid fraction of 0.9518. Increasing the cooling rate had no obvious influence on the precipitation time of MnS inclusion; however, its particle size would be decreased greatly. The results also suggested that increasing the concentration of Mn would lead to an earlier precipitation time of MnS, while it had little effect on the final particle size; as to S, it was found that increasing its concentration could not only make the precipitation time earlier but also make the particle size larger. Adding a certain amount of Ti additive could improve the mechanical properties of U75V heavy rail steel due to the formation of TiO x –MnS or MnS–TiS complex inclusions. The precipitation sequences of Ti3O5 → Ti2O3 → TiO2 → TiO → MnS → TiS for Ti treatment were determined based on the thermodynamic calculation.


Author(s):  
Yu Wang ◽  
Qi He ◽  
Ming Liu ◽  
Weixiong Chen ◽  
Junjie Yan

In pulverized coal-fired plant, the U-type bend is commonly used in flue gas and pulverized coal pipe system to due to the constraints of outer space. And gas-solid two-phase flow exists in these pipelines. The erosion of the pipe has significant effect on the safety and reliability of pipelines. In present paper, the erosion characteristics of U-type bend were investigated through CFD (Computational Fluid Dynamics) method. The wear distribution on the pipe wall was obtained. And the particle flow characteristics in U-type bend were analyzed. The influence of inlet velocity, mass loading rate and particle size on the erosion rate was studied as well. Result suggested that the maximum erosion rate increases exponentially with the increase of inlet velocity. And maximum erosion rate increases linearly with the increasing mass loading rate. Increasing particle size can aggravate the wear on the pipe wall.


Author(s):  
Adam C. Gladen ◽  
Susan C. Mantell ◽  
Jane H. Davidson

A thermotropic material is modeled as an absorbing, thin slab containing anisotropic scattering, monodisperse, spherical particles. Monte Carlo ray tracing is used to solve the governing equation of radiative transfer. Predicted results are validated by comparison to the measured normal-hemispherical reflectance and transmittance of samples with various volume fraction and relative index of refraction. A parametric study elucidates the effects of particle size parameter, scattering albedo, and optical thickness on the normal-hemispherical transmittance, reflectance, and absorptance. The results are interpreted for a thermotropic material used for overheat protection of a polymer solar absorber. For the preferred particle size parameter of 2, the optical thickness should be less than 0.3 to ensure high transmittance in the clear state. To significantly reduce the transmittance and increase the reflectance in the translucent state, the optical thickness should be greater than 2.5 and the scattering albedo should be greater than 0.995. For optical thickness greater than 5, the reflectance is asymptotic and any further reduction in transmittance is through increased absorptance. A case study is used to illustrate how the parametric study can be used to guide the design of thermotropic materials. Low molecular weighted polyethylene in poly(methyl methacrylate) is identified as a potential thermotropic material. For this material and a particle radius of 200 nm, it is determined that the volume fraction and thickness should equal 10% and 1 mm, respectively.


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