Structural and Optical Characterization of ZnO and Glucose Capped ZnO Nanoparticles

2018 ◽  
Vol 21 (1) ◽  
pp. 001-005 ◽  
Author(s):  
A. Dhanalakshmi ◽  
S. Thanikaikarasan ◽  
B. Natarajan ◽  
V. Ramadas ◽  
T. Mahalingam ◽  
...  
Keyword(s):  
Zinc Oxide ◽  
Spectroscopic Analysis ◽  
Optical Characterization ◽  
Hexagonal Structure ◽  
X Ray Diffraction ◽  
X Ray ◽  
Infrared Spectroscopic Analysis ◽  
Structure Surface ◽  
Chemical Reaction Method

Zinc Oxide and Glucose capped Zinc Oxide nanoparticles have been prepared using modified chemical reaction method. X-ray diffraction analysis showed that the prepared samples possess polycrystalline nature with hexagonal structure. Surface morphology has been analyzed using scanning electron microscopy. The estimated value of band gap was found to be 3.41 and 3.87 eV for Zinc Oxide and Glucose capped ZnO respectively. Fourier Transform Infrared spectroscopic analysis has been carried out to find the chemical bond and elemental composition present in Zinc Oxide and Glucose capped Zinc Oxide.

Growth and Characterization of Misostructural Zinc Oxide Tubes

2005 ◽  
Vol 23 ◽  
pp. 293-296
Author(s):  
X.W. Sun ◽  
C.X. Xu ◽  
B.J. Chen ◽  
Y. Yang
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Zinc Oxide ◽  
Growth Process ◽  
Hexagonal Structure ◽  
Metallic Zinc ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron

Zinc oxide (ZnO) microtube has been fabricated by heating the mixture of ZnO and graphite powders in the atmosphere. The ZnO microtubes showed perfect hexagonal profiles with bell-mouth or normal hexagonal tops. Both X-ray diffraction (XRD) and high-resolution transmission electron microscopy (TEM) demonstrated that the product was composed of ZnO with typical hexagonal structure grown predominantly along (002) direction. The growth process was interpreted by means of vaporliquid-solid mechanism combining with the evaporation of metallic zinc.

Microwave-Assisted Synthesis and Characterization of Zinc Oxide Micropowder

2010 ◽  
Vol 93-94 ◽  
pp. 643-646
Author(s):  
Pusit Pookmanee ◽  
Supasima Makarunkamol ◽  
Sakchai Satienperakul ◽  
Jiraporn Kittikul ◽  
Sukon Phanichphant
Keyword(s):  
Zinc Oxide ◽  
Radiation Power ◽  
Ammonium Hydroxide ◽  
Zinc Nitrate ◽  
Hexagonal Structure ◽  
Microwave Assisted Synthesis ◽  
X Ray Diffraction ◽  
X Ray ◽  
Microwave Assisted

Zinc oxide micropowder was synthesized by a microwave-assisted method. Zinc nitrate and ammonium hydroxide were used as the starting precursors with the mole ratio of 1:1. The white precipitated powder was formed after adding ammonium hydroxide until the pH of final solution was 9 and treated with the microwave radiation power at 1000 Watt for 2-6 min. The phase of zinc oxide micropowder was examined by X-ray diffraction (XRD). A single phase of hexagonal structure was obtained. The morphology and chemical composition of zinc oxide micropowder were investigated by scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS). The particle was plate-like in shape with the range of particle size of 0.1-0.5 µm. The elemental composition of zinc oxide showed the characteristic X-ray energy value as follows: zinc of Lα = 1.012 keV, Kα = 8.630 keV and Kβ = 9.570 keV and oxygen of Kα = 0.525 keV, respectively.

scholarly journals Production and characterization of iron-chromium-zinc pigment based ceramic stain colour of red-brown shade

2013 ◽  
Vol 48 (3) ◽  
pp. 213-216 ◽  
Author(s):  
S Parveen ◽  
SA Jahan ◽  
S Ahmed
Keyword(s):  
Zinc Oxide ◽  
Iron Oxide ◽  
Chemical Durability ◽  
X Ray Diffraction ◽  
X Ray ◽  
Exposure Limit ◽  
Substitute Material ◽  
Pure Chromium ◽  
Iron Chromium

Considering the demand of ceramic stain colours in Bangladesh, an attempt has been taken to develop iron-chromium-zinc pigment based ceramic stain colour of red-brown shade which could be used as an import substitute material in the local ceramic industries. The desired shade of red-brown stain was synthesized from an equimolar mixture of pure chromium oxide (Cr2O3), iron oxide (Fe2O3) and zinc oxide (ZnO). The developed stain was characterized by X-ray diffraction (XRD) technique. The characteristic of the stain complied with the chemical durability. Moreover, chromium leaching was below the permissible exposure limit which makes it as a promising ceramic stain to be used in our ceramic industries. DOI: http://dx.doi.org/10.3329/bjsir.v48i3.17334 Bangladesh J. Sci. Ind. Res. 48(3), 213-216, 2013

Structural and Optical Characterization of Zinc Telluride Thin Films

2013 ◽  
Vol 665 ◽  
pp. 254-262 ◽  
Author(s):  
J.R. Rathod ◽  
Haresh S. Patel ◽  
K.D. Patel ◽  
V.M. Pathak
Keyword(s):  
Thin Films ◽  
Extinction Coefficient ◽  
Nir Spectroscopy ◽  
Optical Characterization ◽  
X Ray Diffraction ◽  
X Ray ◽  
Evaporation Technique ◽  
Film Form ◽  
Znte Thin Films

Group II-VI compounds have been investigated largely in last two decades due to their interesting optoelectronic properties. ZnTe, a member of this family, possesses a bandgap around 2.26eV. This material is now a day investigated in thin film form due to its potential towards various viable applications. In this paper, the authors report their investigations on the preparation of ZnTe thin films using vacuum evaporation technique and their structural and optical characterizations. The structural characterization, carried out using an X-ray diffraction (XRD) technique shows that ZnTe used in present case possesses a cubic structure. Using the same data, the micro strain and dislocation density were evaluated and found to be around 1.465×10-3lines-m2and 1.639×1015lines/m2respecctively. The optical characterization carried out in UV-VIS-NIR region reveals the fact that band gap of ZnTe is around 2.2eV in present case. In addition to this, it was observed that the value of bandgap decreases as the thickness of films increases. The direct transitions of the carries are involved in ZnTe. Using the data of UV-VIS-NIR spectroscopy, the transmission coefficient and extinction coefficient were also calculated for ZnTe thin films. Besides, the variation of extinction coefficient with wavelength has also been discussed here.

Preparation and Characterization of Tin Doped Tetra-Pod Shaped Zinc Oxide

2005 ◽  
Vol 475-479 ◽  
pp. 1161-1164 ◽  
Author(s):  
Jing Jing Liu ◽  
Zuo Wan Zhou ◽  
Kai Wang ◽  
Yanxia Li
Keyword(s):  
Zinc Oxide ◽  
Growth Process ◽  
X Ray Diffraction ◽  
Reaction Method ◽  
X Ray ◽  
Crystal Growth Process ◽  
Zno Crystal ◽  
Weight Proportion ◽  
Scanning Electron

Tin doped tetra-pod shaped ZnO (T-ZnO) were fabricated by equilibrant airflow reaction method. The microstructure of tin doped T-ZnO was characterized by X-ray Diffraction analysis and Scanning Electron Microscope. The results demonstrated that most of tin acted as a catalyst during the ZnO crystal growth process and the others reacted with ZnO to generate Zn2SnO4. Tin had catalytic influences on the morphology of T-ZnO, which promoted predominant growth on the c axis of ZnO crystal at the addition of 15% in weight and advanced the growth on the a axis at higher weight proportion.

Characterization of Zn0.96Al0.02Ga0.02O Thermoelectric Material

2013 ◽  
Vol 802 ◽  
pp. 227-231
Author(s):  
Panida Pilasuta ◽  
Pennapa Muthitamongkol ◽  
Chanchana Thanachayanont ◽  
Tosawat Seetawan
Keyword(s):  
Crystal Structure ◽  
Electron Microscopy ◽  
Single Phase ◽  
Hexagonal Structure ◽  
Hexagonal Crystal Structure ◽  
X Ray Diffraction ◽  
Hexagonal Crystal ◽  
X Ray ◽  
Transmission Electron

Crystal structure of Zn0.96Al0.02Ga0.02O was analyzed by X-Ray diffraction (XRD) technique and the microstructure was observed by scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The XRD results showed single phase and hexagonal structure a = b = 3.24982 Å, and c = 5.20661 Å. The SEM and TEM results showed the grain size of material arrangement changed after sintering and TEM diffraction pattern confirmed hexagonal crystal structure of Zn0.96Al0.02Ga0.02O after sintering.

Synthesis and Spectral Analysis of PVP Capped Zinc Oxide Nanostructures

2015 ◽  
Vol 1086 ◽  
pp. 75-78
Author(s):  
R. Kiruba ◽  
Solomon Jeevaraj A. Kingson
Keyword(s):  
Zinc Oxide ◽  
Chemical Precipitation ◽  
Hexagonal Structure ◽  
Spectroscopic Techniques ◽  
Photoluminescence Spectra ◽  
Zinc Oxide Nanostructures ◽  
X Ray Diffraction ◽  
X Ray ◽  
Oxide Nanostructures ◽  
Prepared Nanostructures

Monodispersed polyvinylpyrrolidone capped nanostructures of zinc oxide are prepared through chemical precipitation technique. The prepared nanostructures are characterized by XRD, SEM and Photoluminescence spectroscopic techniques. X-ray diffraction studies confirm the hexagonal structure of zinc oxide nanostructures. Nanostructures of the prepared zinc oxide are confirmed by SEM. The emission wavelength of PVP capped zinc oxide is found to be 551 nm using photoluminescence spectra.

Hydrothermal Synthesis of Zinc Oxide (ZnO) Microparticle

2008 ◽  
Vol 55-57 ◽  
pp. 845-848 ◽  
Author(s):  
Pusit Pookmanee ◽  
S. Khuanphet ◽  
Sukon Phanichphant
Keyword(s):  
Zinc Oxide ◽  
Single Phase ◽  
Ammonium Hydroxide ◽  
Hexagonal Structure ◽  
Deionized Water ◽  
X Ray Diffraction ◽  
Hydrothermal Route ◽  
X Ray ◽  
Calcination Step ◽  
Scanning Electron

Zinc oxide (ZnO) microparticle was synthesized by hydrothermal route using zinc acetate and ammonium hydroxide as the starting precursors in the mole ratio of 1:6. The final mixture solution was adjust with pH of 9 and treated in PTFE-line autoclave at 100 oC for 2, 4 and 6 h. The precipitate was washed with deionized water until the final pH solution of 7 and then dried at 100 oC for 4h. The phase structure was examined by X-ray diffraction (XRD). A single phase hexagonal structure was obtained without calcination step. Microstructure was investigated by scanning electron microscopy (SEM). The particle size of ZnO was in the range of 0.15-1.5 µm with irregular in shape. The chemical composition was identified by energy dispersive X-ray spectroscopy (EDXS). The elemental composition of ZnO showed the characteristic X-ray energy value as follows: zinc of Lα = 1.012 keV, Kα = 8.630 keV and Kβ = 9.570 keV and oxygen of Kα = 0.525 keV, respectively.

scholarly journals KARAKTERISASI ABU KAYU MERBAU (Intsia, spp.): PENGARUH TEMPERATUR DAN LAMA KALSINASI

2019 ◽  
Vol 15 (1) ◽  
pp. 30-38
Author(s):  
Darma Santi ◽  
Jacson Victor Morin
Keyword(s):  
Calcination Temperature ◽  
Wood Ash ◽  
Hexagonal Structure ◽  
Rhombohedral Structure ◽  
Water Molecules ◽  
X Ray Diffraction ◽  
X Ray ◽  
Ft Ir ◽  
Cubic Structure

Characterization of merbau wood ash (Intsia, spp.) due to the influence of temperature and time of calcination has been studied. The variations in calcination temperature were 500 ᴼC (as M500) and 600 ᴼC (as M600), while the variations in the duration of calcination were 1, 2, and 3 hours, noted as M1, M2, and M3, respectively. Characterization was carried out using X-ray diffraction (XRD) and spectroscopic analysis using FT-IR. XRD results identified the presence of CaCO3 species (rhombohedral structure) and K2Si4O9 species with a hexagonal structure on M500. The M600 species identified Si (cubic structure), SiO2 (cubic structure), K2Si4O9 (hexagonal structure), and CaCO3 (rhombohedral structure). In general, the calcination temperature increases the crystallinity of several compounds contained in merbau wood ash. The length of time calcination reduces the absorption peak due to the decomposition and adsorption reactions of the presence of water molecules bound to the ash material of merbau wood (Intsia, spp).

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