scholarly journals Effects of vacuum heat treatment and wax impregnation on the color of Pterocarpus macrocarpus Kurz.

BioResources ◽  
2020 ◽  
Vol 16 (1) ◽  
pp. 954-963
Author(s):  
Lin Yang ◽  
Tianqi Han ◽  
Yunxia Liu ◽  
Qin Yin

Pterocarpus macrocarpus Kurz. wood was vacuum heat treated (VHT) at 120, 150, and 180 °C, under a pressure of 13.3 kPa. Half of the VHT specimens at 120 and 150 °C were subjected to wax impregnation (WI) for 48 h at 90 °C under an atmospheric pressure. The effect of VHT and WI on wood color were investigated. The results showed that the VHT at 120 and 150 °C resulted in minor changes in lightness (L*), green-red chromatic coordinate (a*), blue-yellow chromatic coordinate (b*), total color change (ΔE*), and chroma (C*). However, the effect of VHT on L*, a*, b*, and C* at 180 °C became more obvious over the duration. After WI, the L*, a*, b*, and C* of the VHT wood at moderate temperatures varied noticeably, showing similar behavior with the VHT wood at 180 °C as L*, b*, and C* decreased and ΔE increased. However, a* increased after WI compared to that of VHT at 180 °C. The wood color of P. macrocarpus Kurz. after WI became reddish and blue, and the color deviation decreased. The wood color was closer to the dark mahogany, which facilitates its further application in rosewood furniture and woodwork art.

BioResources ◽  
2021 ◽  
Vol 16 (3) ◽  
pp. 5574-5585
Author(s):  
Intan Fajar Suri ◽  
Jong Ho Kim ◽  
Byantara Darsan Purusatama ◽  
Go Un Yang ◽  
Denni Prasetia ◽  
...  

Color changes were tested and compared for heat-treated Paulownia tomentosa and Pinus koraiensis wood treated with hot oil or hot air for further utilization of these species. Hot oil and hot air treatments were conducted at 180, 200, and 220 °C for 1, 2, and 3 h. Heat-treated wood color changes were determined using the CIE-Lab color system. Weight changes of the wood before and after heat treatment were also determined. The weight of the oil heat-treated wood increased considerably but it decreased in air heat-treated wood. The oil heat-treated samples showed a greater decrease in lightness (L*) than air heat-treated samples. A significant change in L* was observed in Paulownia tomentosa. The red/green chromaticity (a*) of both wood samples increased at 180 and 200 °C and slightly decreased at 220 °C. The yellow/blue chromaticity (b*) in both wood samples increased at 180 °C, but it rapidly decreased with increasing treatment durations at 200 and 220 °C. The overall color change (ΔE*) in both heat treatments increased with increasing temperature, being higher in Paulownia tomentosa than in Pinus koraiensis. In conclusion, oil heat treatment reduced treatment duration and was a more effective method than air heat treatment in improving wood color.


Holzforschung ◽  
2011 ◽  
Vol 65 (3) ◽  
Author(s):  
Miyuki Matsuo ◽  
Misao Yokoyama ◽  
Kenji Umemura ◽  
Junji Sugiyama ◽  
Shuichi Kawai ◽  
...  

Abstract The color properties of aging wood samples from historical buildings have been compared with those of recent wood samples that were heat treated at temperatures ranging from 90°C to 180°C. The results of kinetic analysis obtained by the time-temperature superposition method showed that the color change during natural aging was mainly due to a slow and mild oxidation process. In other words, heat treatment could accelerate the changes in wood color that occur during aging. In one sample, the color change (ΔE* ab ) after 921 years at ambient temperature was almost equivalent to that of heating (artificial aging) approximately for 6.7 h at 180°C. The results have been interpreted that the aging and the subsequent change in wood color begin at the time of tree harvesting.


2020 ◽  
Vol 66 (1) ◽  
Author(s):  
Memiş Akkuş ◽  
Mehmet Budakçı

Abstract The aim of this study was to use bleaching chemicals to remove the discoloration occurring on the surface of wood after heat treatment in order to restore the natural color of the wood. For this purpose, samples prepared from Scots pine (Pinus sylvestris L.), sessile oak (Quercus petraea L.), Eastern beech (Fagus orientalis L.), and Uludağ fir (Abies bornmuelleriana Mattf.) were exposed to heat treatment at temperatures of 140 and 160 °C for time periods of 3, 5, and 7 h. Bleaching solutions S1 (NaOH + H2O2), S2 (NaSiO3 + H2O2), and S3 (H2C2O4) at a concentration of 18% were then applied to the surface of the materials and the color change was determined according to ASTM D 2244 standard. Depending on the heat treatment temperature and duration, an increase in total color change values was detected on the surfaces of the materials and the color of the samples became darker. The total color change values decreased after bleaching with the S2 solution in the heat-treated Scots pine and fir samples, with the S3 solution in the beech samples, and with the S1, S2, and S3 solutions in the oak samples. The findings showed that by using bleaching chemicals to lighten wood materials darkened after heat treatment, it is possible to obtain results close to the natural color values.


2014 ◽  
Vol 2 ◽  
pp. 345-352 ◽  
Author(s):  
Cristina Marinela Olarescu ◽  
Mihaela Campean

Heat treatment is renowned as the most environmentally friendly process of dimensional stabilization that can be applied to wood, in order to make it suitable for outdoor uses. It also darkens wood color and improves wood durability. The intensity of heat treatment can be appreciated by means of two parameters: the color change occured in wood due to the high temperature, and the mass loss, which is a measure of the degree of thermal degradation. In order to find a mathematical correlation between these two parameters, an experimental study was conducted with four European wood species, which were heat-treated at 180°C and 200ºC, for 1-3 hours, under atmosheric pressure.The paper presents the results concerning the color changes and mass losses recorded for the heat-treated wood samples compared to untreated wood.  For all four species, the dependency between the color change and the mass loss was found to be best described by a logarithmic regression equation with R2 of 0.93 to 0.99 for the soft species (spruce, pine and lime), and R2 of 0.77 for beech. The results of this study envisage to simplify the assessment procedure of the heat treatment efficiency, by only measuring the color – a feature that is both convenient and cost-effective. 


Forests ◽  
2019 ◽  
Vol 10 (9) ◽  
pp. 791
Author(s):  
Xinjie Cui ◽  
Junji Matsumura

To quickly clarify the effect of heat treatment on weatherability of Cunninghamia lanceolate (Lamb.) Hook., we investigated the surface degradation under natural exposure. A comparison between heat-treated and untreated samples was taken based on surface color changes and structural decay at each interval. Over four weeks of natural exposure, multiple measurements were carried out. Results show that color change decreased in the order of 220 °C heat-treated > untreated > 190 °C heat-treated. The results also indicate that the wood surface color stability was improved via the proper temperature of thermal modification. Low vacuum scanning electron microscopy (LVSEM) results expressed that thermal modification itself had caused shrinking in the wood surface structure. From the beginning of the weathering process, the heat treatment affected the surface structural stability. After natural exposure, the degree of wood structure decay followed the pattern 220 °C heat-treated > 190 °C heat-treated > untreated. Therefore, when considering the impact on the structure, thermal modification treatment as a protective measure to prevent weathering was not an ideal approach and requires further improvement.


2007 ◽  
Vol 554 ◽  
pp. 107-112 ◽  
Author(s):  
V. Demir ◽  
Derek P. Thompson

Silicon nitride samples were pressureless sintered with up to 5 w/o MgO to give densities in the range 98-99% of theoretical. After pressureless sintering, selected samples were placed in a vacuum heat treatment furnace surrounded by a carbon bed in a carbon crucible at a pressure of less than 4x10-4 mbar, and vacuum heat treated at different temperatures and times to remove grainboundary glass. The results showed that this was substantially achieved at 1575oC for 3h and that increasing the time to 5 hours gave still further improvement. SEM images, EDX analysis and oxidation tests provided additional evidence for the removal of Mg from the samples.


2014 ◽  
Vol 9 (1-2) ◽  
Author(s):  
Dragan P Vujadinović ◽  
Božana V Odžaković ◽  
Radoslav D Grujić ◽  
Milija Perić

Abstract: A heat-treated beet is defined as a food that is subject to a temperature, high enough to destroy microorganisms and to preserve all the nutrients. The aim of the study presented in this paper was to investigate the effect by cooking on the properties of heat threated beetroot in the temperature range between 75 °C and 115 °C during the 40, 50 and 60 minutes of cooking. In order to determine the optimal conditions for the implementation of various heat treatment procedures consequently, was followed the influence of heat treatment conditions (temperature/time) on the composition, rheological properties, pH, color change (L*, a*, b*) and sensory characteristics during the development of the “pasteurized/sterilized” beet product. This study has shown that the optimum time and temperature for processing of beetroot is 105 °C at 50 minutes. Samples of beetroot, processed under these conditions had the best softness, the most acceptable taste and color (sensory and instrumentally determined).


BioResources ◽  
2020 ◽  
Vol 15 (2) ◽  
pp. 2708-2720 ◽  
Author(s):  
Ahmet Can

Heat treatment is an environmentally friendly and efficient way to improve the properties of wood species. These treatments alter the substrates and can influence the surface properties of the varnish coatings. This paper investigated the effects of heat treatment on the physical properties of open and close systems Scots pine (Pinus sylvestris L.) and poplar (Populus euramericana) wood, coated with water-based, polyurethane-based, and oil/wax-based varnishes. Heat treatment was applied at the temperatures of 190, 212 °C for pine and 180, 200 °C for poplar, respectively. Color, gloss, and roughness tests were carried out for each of the coatings. Higher mass loss occurred in pine samples with heat treatment as compared to vacuum-heat treatment. Gloss decreased in OIL+WAX treatment and color change increased after the heat treatment, but these results were inhibited with vacuum-heat treatment. Maximum roughness was obtained in PUR varnishes and minimum roughness in OIL + WAX samples. The low roughness values provide some advantages in application.


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