Preparation of Metal Nanosuspensions by High-Pressure DC-Sputtering on Running Liquids

1996 ◽  
Vol 457 ◽  
Author(s):  
M. Wagener ◽  
B. S. Murty ◽  
B. Günther
Keyword(s):  
Particle Size ◽  
High Pressure ◽  
Particle Size Distribution ◽  
Pressure Range ◽  
Narrow Particle Size Distribution ◽  
Descriptive Model ◽  
Mean Particle Size ◽  
Dc Sputtering ◽  
The Mean ◽  
Argon Sputtering

ABSTRACTA modified VERL-process (Vacuum evaporation on running liquids) employing high pressure magnetron sputtering has been used for the preparation of suspensions with metal nanoparticles. The method has been tested for Ag- and Fe-suspensions by varying the pressure of the Argon sputtering atmosphere in the range of 1 to 30 Pa. A narrow particle size distribution with a mean particle size ranging from 5–18 nm has been found. The mean particle size increases with increasing Argon pressure in the pressure range under investigation. A descriptive model for the process of particle formation as a function of sputtering gas pressure is given.

Super Fine Powderization of Korean Ginseng Using Low Temperature Turbo Mill

2006 ◽  
Vol 326-328 ◽  
pp. 445-448 ◽  
Author(s):  
Beom Goo Lee ◽  
Yeon Ho Jeong ◽  
Dong Ha Cho ◽  
Kang Yol Lee ◽  
Wie Soo Kang
Keyword(s):  
Particle Size ◽  
Low Temperature ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Particle Diameter ◽  
Fine Powder ◽  
Narrow Particle Size Distribution ◽  
Volume Distribution ◽  
The Mean ◽  
Korean Ginseng

It is investigated whether ginseng can be milled into super fine powder below 50μm, changing the circumferential velocity of impeller of a turbo mill(100, 110 and 120m/s). The mean particle size is 113.3μm in control but is decreased abruptly into 11.9μm at 120m/s. The largest particle diameter at 97% of volume distribution is reduced into below 32μm at 120m/s from below 725μm at control. The particle size distribution between d(0.1) and d(0.9) is 334μm at control, but is decreased into less than 26μm in all conditions after milling. It shows that ginseng can be milled into super fine powder by the turbo mill, which has the narrow particle size distribution.

Investigation of the crystallization of zeolite A from hydrogels aged under high pressure

CrystEngComm ◽  
2014 ◽  
Vol 16 (36) ◽  
pp. 8563-8569
Author(s):  
Fei Tong ◽  
Weiwei Ji ◽  
Ming Li ◽  
Changfeng Zeng ◽  
Lixiong Zhang
Keyword(s):  
Particle Size ◽  
High Pressure ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Small Particle ◽  
Narrow Particle Size Distribution ◽  
Particle Sizes ◽  
Zeolite A

Aging of hydrogels under high pressure can result in the formation of zeolites with small particle sizes and narrow particle size distribution.

Batch Precipitation of Lead Iodide

1994 ◽  
Vol 59 (6) ◽  
pp. 1301-1304
Author(s):  
Jaroslav Nývlt ◽  
Stanislav Žáček
Keyword(s):  
Aqueous Solution ◽  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Crystal Size ◽  
Lead Nitrate ◽  
Lead Iodide ◽  
Constant Rate ◽  
Mean Size ◽  
The Mean

Lead iodide was precipitated by a procedure in which an aqueous solution of potassium iodide at a concentration of 0.03, 0.10 or 0.20 mol l-1 was stirred while an aqueous solution of lead nitrate at one-half concentration was added at a constant rate. The mean size of the PbI2 crystals was determined by evaluating the particle size distribution, which was measured sedimentometrically. The dependence of the mean crystal size on the duration of the experiment exhibited a minimum for any of the concentrations applied. The reason for this is discussed.

scholarly journals Particle Size Effects on Selectivity in Confined Bed Comminution

Minerals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 342
Author(s):  
Holger Lieberwirth ◽  
Lisa Kühnel
Keyword(s):  
Particle Size ◽  
High Pressure ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Size Effects ◽  
Experimental Investigations ◽  
Ore Processing ◽  
Tumbling Mills ◽  
Particle Bed ◽  
Vertical Roller

Confined bed comminution in high-pressure grinding rollers (HPGRs) and vertical roller mills (VRMs) was previously used preferably for grinding comparably homogeneous materials such as coal or clinker. Meanwhile, it started to complement or even replace tumbling mills in ore beneficiation with ore and gangue particles of rather different breakage behaviors. The selectivity in the comminution of a mixture of particles with different strengths but similar particle size distribution (PSD) of the constituents in a particle bed was investigated earlier. The strength of a material is, however, also a function of particle size. Finer particles tend to be more competent than coarser ones of the same material. In industrial ore processing using confined bed comminution, this effect cannot be neglected but even be exploited to increase efficiency. This paper presents research results on this topic based on experimental investigations with model materials and with natural particles, which were stressed in a piston–die press. It appeared that the comminution result substantially depends on the material characteristics, the composition of the mixture and the PSD of the constituents. Conclusions will be drawn for the future applications of selective comminution in mineral processing.

Green synthesis of submicron copper powder with narrow particle size distribution via a simple methanol thermal reduction

2021 ◽  
Author(s):  
Xiaoping Chen ◽  
Jiaqi Fu ◽  
Jiangang Li ◽  
Bohong Chen ◽  
Lei Yang ◽  
...  
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Green Synthesis ◽  
Size Distribution ◽  
Copper Powder ◽  
Reduction Method ◽  
Particle Distribution ◽  
Thermal Reduction ◽  
Narrow Particle Size Distribution

In this work, submicron copper powder with narrow particle distribution was synthesized via a simple methanol thermal reduction method without using any surfactants. Smaller copper powder with narrower particle size...

A SIMULATION STUDY ON THE EFFECT OF PARTICLE SIZE DISTRIBUTION ON THE PRINTED GEOMETRY IN SELECTIVE LASER MELTING

2021 ◽  
pp. 1-14
Author(s):  
Vaishak Ramesh Sagar ◽  
Samuel Lorin ◽  
Johan Göhl ◽  
Johannes Quist ◽  
Christoffer Cromvik ◽  
...  
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Layer Thickness ◽  
Selective Laser Melting ◽  
Laser Melting ◽  
Powder Bed ◽  
Mean Particle Size ◽  
Final Layer ◽  
Effect Of Particle Size

Abstract Selective laser melting (SLM) process is a powder bed fusion additive manufacturing process that finds applications in aerospace and medical industries for its ability to produce complex geometry parts. As the raw material used is in powder form, particle size distribution (PSD) is a significant characteristic that influences the build quality in turn affecting the functionality and aesthetics aspects of the product. This paper investigates the effect of PSD on the printed geometry for 316L stainless steel powder, where three coupled in-house simulation tools based on Discrete Element Method (DEM), Computational Fluid Dynamics (CFD), and Structural Mechanics are employed. DEM is used for simulating the powder bed distribution based on the different powder PSD. The CFD is used as a virtual testbed to determine thermal parameters such as heat capacity and thermal conductivity of the powder bed viewed as a continuum. The values found as a stochastic function of the powder distribution is used to analyse the effect on the melted zone and deformation using Structural Mechanics. Results showed that mean particle size and PSD had a significant effect on the packing density, melt pool layer thickness, and the final layer thickness after deformation. Specifically, a narrow particle size distribution with smaller mean particle size and standard deviation produced solidified final layer thickness closest to nominal layer thickness. The proposed simulation approach and the results will catalyze in development of geometry assurance strategies to minimize the effect of particle size distribution on the geometric quality of the printed part.

Organosilicon Comb-Shaped Surfactants for the Synthesis of Polymer Suspensions with a Narrow Particle Size Distribution

2021 ◽  
Vol 63 (3) ◽  
pp. 209-217
Author(s):  
A. A. Ezhova ◽  
I. A. Gritskova ◽  
S. A. Gusev ◽  
S. A. Milenin ◽  
V. V. Gorodov ◽  
...  
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Narrow Particle Size Distribution

Dropwise cooling crystallization of ammonium perchlorate in gas–liquid two-phase suspension systems

CrystEngComm ◽  
2018 ◽  
Vol 20 (43) ◽  
pp. 6932-6939 ◽  
Author(s):  
Wei Liu ◽  
Yong Xie ◽  
Qiang Xie ◽  
Kexiong Fang ◽  
Xuan Zhang ◽  
...  
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Crystal Engineering ◽  
Smooth Surface ◽  
Narrow Particle Size Distribution ◽  
Two Phase ◽  
Crystalline Materials ◽  
Suspension Systems ◽  
Crystallization Method ◽  
Cooling Crystallization

A dropwise cooling crystallization method was proposed to prepare AP crystals with a uniform shape, a narrow particle size distribution and a smooth surface, which is also a reference for the crystallization of other crystalline materials in crystal engineering.

scholarly journals MINERAL ABUNDANCE AND PARTICLE SIZE DISTRIBUTION DERIVED FROM IN-SITU SPECTRA MEASUREMENTS OF YUTU ROVER OF CHANG’E-3

2017 ◽  
Vol XLII-3/W1 ◽  
pp. 85-89
Author(s):  
H. Lin ◽  
X. Zhang ◽  
Y. Yang ◽  
X. Wu ◽  
D. Guo
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Landing Site ◽  
Radiative Transfer Model ◽  
Transfer Model ◽  
Particle Sizes ◽  
The Mean ◽  
The Difference ◽  
Yutu Rover

From geologic perspective, understanding the types, abundance, and size distributions of minerals allows us to address what geologic processes have been active on the lunar and planetary surface. The imaging spectrometer which was carried by the Yutu Rover of Chinese Chang’E-3 mission collected the reflectance at four different sites at the height of ~ 1 m, providing a new insight to understand the lunar surface. The mineral composition and Particle Size Distribution (PSD) of these four sites were derived in this study using a Radiative Transfer Model (RTM) and Sparse Unmixing (SU) algorithm. The endmembers used were clinopyroxene, orthopyroxene, olivine, plagioclase and agglutinate collected from the lunar sample spectral dataset in RELAB. The results show that the agglutinate, clinopyroxene and olivine are the dominant minerals around the landing site. In location Node E, the abundance of agglutinate can reach up to 70 %, and the abundances of clinopyroxene and olivine are around 10 %. The mean particle sizes and the deviations of these endmembers were retrieved. PSDs of all these endmembers are close to normal distribution, and differences exist in the mean particle sizes, indicating the difference of space weathering rate of these endmembers.

Effect of Ag addition in Sn on growth of SnTe compound during reaction between molten solder and tellurium

2010 ◽  
Vol 25 (2) ◽  
pp. 391-395 ◽  
Author(s):  
Chien-Neng Liao ◽  
Yen-Chun Huang
Keyword(s):  
Particle Size ◽  
Reaction Time ◽  
Electrical Properties ◽  
Bismuth Telluride ◽  
Molten Solder ◽  
Thermoelectric Modules ◽  
Ag Addition ◽  
Mean Particle Size ◽  
Mechanical And Electrical Properties ◽  
The Mean

SnTe is the most common compound formed at the bismuth telluride/metal soldered junction of thermoelectric modules. It affects the mechanical and electrical properties of the soldered junction. In the study we investigate the growth of SnTe compound during reaction between molten Sn–3.5Ag solder and tellurium at 250 °C. We found that the growth of SnTe is suppressed by Ag–Te bilayer compounds that block further reaction between liquid Sn and Te. With increasing reaction time, the SnTe morphology becomes rough as a result of coarsening of SnTe grains. The growth of SnTe grains follows the conservative ripening kinetics with the mean particle size proportional to one-third power of reaction time.

Sign in / Sign up

Export Citation Format

Share Document