High-Temperature Mechanical Behavior and Phase Morphology of Poly(Tetrafluoroethylene)/Siloxane Nanocomposites Used as Ultra Low-k Dielectrics

2000 ◽  
Vol 612 ◽  
Author(s):  
Ping Xu ◽  
Shichun Qu ◽  
Tom Rosenmayer ◽  
Min Y. Lin
Keyword(s):  
High Temperature ◽  
Mechanical Behavior ◽  
Small Angle Neutron Scattering ◽  
Single Phase ◽  
Phase Morphology ◽  
Phase Separations ◽  
High Temperature Mechanical Properties ◽  
Mechanical Study ◽  
Molecular Composites ◽  
Low K

AbstractPoly(tetrafluoroethylene) (PTFE)/siloxane nanocomposites have been prepared as ultra low-k dielectrics. These new nanocomposites show excellent high-temperature mechanical properties compared to unfilled PTFE while their dielectric constant almost remains unchanged. Specifically, the data from the dynamic mechanical study indicates that these nanocomposites have the mechanical behavior similar to that of crosslinked polymers. Small-angle neutron scattering (SANS) has been carried out to characterize the phase morphology of the PTFE/siloxane nanocomposites and the size of the inorganic networks. It has been shown that no phase separations or orientations appear in these nanocomposites in the range of 12 to 469 nm. These SANS results suggest that these materials are single-phase nanocomposites that are very homogeneous and isotropic. They are basically PTFE-based molecular composites.

High Temperature Mechanical Behavior of Some Advanced Ni3Al

1986 ◽  
Vol 81 ◽  
Author(s):  
S. E. Hsu ◽  
N. N. Hsu ◽  
C. H. Tong ◽  
C. Y. Ma ◽  
S. Y. Lee
Keyword(s):  
Mechanical Properties ◽  
High Temperature ◽  
Yield Strength ◽  
Mechanical Behavior ◽  
Single Phase ◽  
Rupture Strength ◽  
Strengthening Mechanisms ◽  
High Temperature Mechanical Properties ◽  
Higher Temperature

AbstractHigh temperature mechanical properties of various Zr and Cr strengthened single phase Ni3Al are investigated, with emphasis on the ability of each element to elevate Tp, the temperature corresponding to the peak yield strength. It is observed that Zr is a very effective strengthener, more so below Tp than above it, while a combination of Cr and Zr is capable of shifting Tp to a higher temperature. The combination results in an effective improvement of the rupture strength of Ni3Al. The strengthening mechanisms of each element will be discussed in this paper.

Application of TEM to Deformation, Wear, and Fracture of Ceramics

1974 ◽  
Vol 32 ◽  
pp. 472-473
Author(s):  
B. J. Hockey
Keyword(s):  
Wear Resistance ◽  
High Temperature ◽  
Mechanical Behavior ◽  
Brittle Materials ◽  
High Temperature Strength ◽  
Wide Range ◽  
Corrosive Environments ◽  
Further Development

Ceramics, such as Al2O3 and SiC have numerous current and potential uses in applications where high temperature strength, hardness, and wear resistance are required often in corrosive environments. These materials are, however, highly anisotropic and brittle, so that their mechanical behavior is often unpredictable. The further development of these materials will require a better understanding of the basic mechanisms controlling deformation, wear, and fracture.The purpose of this talk is to describe applications of TEM to the study of the deformation, wear, and fracture of Al2O3. Similar studies are currently being conducted on SiC and the techniques involved should be applicable to a wide range of hard, brittle materials.

TEM Studies of Grain Boundary Films in Si3N4 Ceramics

1991 ◽  
Vol 49 ◽  
pp. 930-931
Author(s):  
H.-J. Kleebe ◽  
J.S. Vetrano ◽  
J. Bruley ◽  
M. Rühle
Keyword(s):  
Mechanical Properties ◽  
High Temperature ◽  
Silicon Nitride ◽  
Hot Isostatic Pressing ◽  
Amorphous Film ◽  
Liquid Phase Sintering ◽  
Second Phase ◽  
High Temperature Mechanical Properties ◽  
Triple Points ◽  
Boundary Films

It is expected that silicon nitride based ceramics will be used as high-temperature structural components. Though much progress has been made in both processing techniques and microstructural control, the mechanical properties required have not yet been achieved. It is thought that the high-temperature mechanical properties of Si3N4 are limited largely by the secondary glassy phases present at triple points. These are due to various oxide additives used to promote liquid-phase sintering. Therefore, many attempts have been performed to crystallize these second phase glassy pockets in order to improve high temperature properties. In addition to the glassy or crystallized second phases at triple points a thin amorphous film exists at two-grain junctions. This thin film is found even in silicon nitride formed by hot isostatic pressing (HIPing) without additives. It has been proposed by Clarke that an amorphous film can exist at two-grain junctions with an equilibrium thickness.

Precipitate coarsening during hot-compression testing of NiAl + 2 at.% Nb

1986 ◽  
Vol 44 ◽  
pp. 598-599
Author(s):  
W. M. Sherman ◽  
K. M. Vedula
Keyword(s):  
High Temperature ◽  
Flow Stress ◽  
Weight Ratio ◽  
Constant Strain Rate ◽  
Hot Compression ◽  
Compression Testing ◽  
Second Phase ◽  
Precipitate Coarsening ◽  
High Temperature Mechanical Properties ◽  
Ordered Intermetallic

The strength to weight ratio and oxidation resistance of NiAl make this ordered intermetallic, with some modifications, an attractive candidate to compete with many superalloys for high temperature applications. Recent studies have shown that the inherent brittleness of many polycrystalline intermetallics can be overcome by micro and macroalloying. It has also been found that the high temperature mechanical properties of NiAl can be enhanced through the addition of Nb by powder metallurgical techniques forming a dispersed second phase through interdiffusion in a polycrystalline matrix. A drop in the flow stress is observed however in a NiAl-2 at.% Nb alloy after 0.2 % strain during constant strain rate hot compression testing at 1025°C. The object of this investigation was to identify the second phase and to determine the cause of the flow stress drop.

BERYLCO NICKEL ALLOY 440

Alloy Digest ◽  
1975 ◽  
Vol 24 (9) ◽  
Keyword(s):  
Mechanical Properties ◽  
High Temperature ◽  
Nickel Alloy ◽  
High Strength ◽  
Heat Treating ◽  
Electronic Components ◽  
High Temperature Mechanical Properties ◽  
Temperature Performance ◽  
Solution Treated ◽  
Complex Shapes

Abstract BERYLCO NICKEL ALLOY 440 is an age-hardenable nickel-beryllium-titanium alloy that offers high strength, excellent spring properties outstanding formability, good high-temperature mechanical properties, and resistance to corrosion and fatigue. Complex shapes can be produced in the solution-treated (soft) condition and then aged to a minimum tensile strength of 215,500 psi. It is used for mechanical and electrical/electronic components in the temperature range -320 to 800 F. This datasheet provides information on composition, physical properties, hardness, elasticity, and tensile properties as well as fracture toughness. It also includes information on high temperature performance and corrosion resistance as well as forming, heat treating, machining, joining, and surface treatment. Filing Code: Ni-94. Producer or source: Kawecki Berylco Industries Inc.. Originally published September 1964, revised September 1975.

COPPER ALLOY No. 230

Alloy Digest ◽  
1972 ◽  
Vol 21 (3) ◽  
Keyword(s):  
Fracture Toughness ◽  
Corrosion Resistance ◽  
Shear Strength ◽  
High Temperature ◽  
Physical Properties ◽  
Tensile Properties ◽  
Copper Alloy ◽  
Single Phase ◽  
Heat Treating ◽  
Temperature Performance

Abstract COPPER ALLOY No. 230 is a single-phase brass containing 15% zinc which is the most widely used of the low zinc brasses. This datasheet provides information on composition, physical properties, hardness, elasticity, tensile properties, and shear strength as well as fracture toughness and creep. It also includes information on low and high temperature performance, and corrosion resistance as well as forming, heat treating, machining, and joining. Filing Code: Cu-252. Producer or source: Brass mills.

HASTELLOY ALLOY S

Alloy Digest ◽  
1973 ◽  
Vol 22 (1) ◽  
Keyword(s):  
Mechanical Properties ◽  
High Temperature ◽  
Heat Treating ◽  
High Temperature Alloy ◽  
Excellent Thermal Stability ◽  
Cabot Corporation ◽  
High Temperature Mechanical Properties ◽  
Temperature Performance ◽  
Resistance To Oxidation ◽  
Nickel Base

Abstract HASTELLOY alloy S is a nickel-base high-temperature alloy having excellent thermal stability, good high-temperature mechanical properties and excellent resistance to oxidation up to 2000 F. This datasheet provides information on composition, physical properties, elasticity, and tensile properties as well as creep. It also includes information on high temperature performance and corrosion resistance as well as forming, heat treating, machining, and joining. Filing Code: Ni-184. Producer or source: Stellite Division, Cabot Corporation.

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