scholarly journals Bond strength of glass-ceramic cemented to a zirconia structure: influence of adhesive cementation strategy

2016 ◽  
Vol 64 (2) ◽  
pp. 140-147
Author(s):  
Gilvan Cutrim TAVARES ◽  
Renan Macedo Cutrim TAVARES ◽  
Milton Edson MIRANDA ◽  
Cecilia Pedroso TURSSI ◽  
Roberta Tarkany BASTING ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Adhesive System ◽  
Resin Cement ◽  
The Other ◽  
Universal Testing ◽  
Adhesive Cementation ◽  
Adhesive Cement ◽  
One Way Anova

ABSTRACT Objective This study evaluated the shear bond strength (SBS) of lithium disilicate glass (LDG) ceramic bonded to a zirconia (Y-TZP), using different cementation strategies. Methods LDG ceramic cylinders were cemented to Y-TZP structure according to the following adhesive system (AS)/resin cement (RC) (n = 15): U- self-adhesive dual-cure RC; AMBAR- AS containing phosphate monomers (PM) + dual-cure RC; group SBU: PM+Silane/AS + light-cure RC; group ALLB: PM/AS + dual-cure RC. Specimens were subjected to SBS in a universal testing machine (0.5 mm/min). Data (MPa) were subjected to one-way ANOVA and Tukey's test (α = 0,05). Results The groups SBU and ALLB had significantly higher SBS than those provided by the group U, in which the lowest values were observed. For the AMBAR group, intermediate SBS values were found, which did not differ significantly from the values observed in the other groups. Conclusion Regardless of resins cement, the use of adhesives containing phosphate monomers provided superior bond strength than self-adhesive cement.

Ceramic Bonding to Biocompatible Titanium Alloys Obtained by Powder Metallurgy

2006 ◽  
Vol 530-531 ◽  
pp. 605-611
Author(s):  
M.C. Bottino ◽  
D.K. Oyafuso ◽  
Paulo Guilherme Coelho ◽  
Elisa B. Taddei ◽  
Vinicius André Rodrigues Henriques ◽  
...  
Keyword(s):  
Bond Strength ◽  
Titanium Alloys ◽  
Shear Bond Strength ◽  
Microstructural Analysis ◽  
Testing Machine ◽  
Phase Identification ◽  
Base Metals ◽  
Blended Elemental ◽  
Universal Testing ◽  
One Way Anova

The shear bond strength between a ceramic material (Titankeramik®, Vita Zahnfabrik, Germany) and two biocompatible titanium alloys was investigated. Ti-13%Nb-13%Zr (TNZ) and Ti-35%Nb-7%Zr-5%Ta (TNZT) alloys were obtained based on the blended elemental technique followed by a sequence of cold uniaxial and isostatic pressing and sintering. Characterization involved microstructural analysis (SEM) and crystalline phase identification (XRD). Subsequently, samples were machined to 4 x 4 mm with a base of 5 x 1 mm. The base metals were blasted with Al2O3 particles followed by the application of a coupling agent and opaque ceramic. After ceramic firing, the specimens were loaded in a universal testing machine (0,5mm/min). XRD revealed the presence of α and β-phases for TNZ, and peaks related to β phases and Nb and Ta for the TNZT alloy. SEM evaluation (TNZ) depicted remaining pores and biphasic microstructure formation. SEM micrographs of the TNZT alloy revealed good densification and a homogeneous β structure. Shear bond strength data (MPa) were statistically analyzed (one-way ANOVA and Tukey test, α=.05) revealing that TNZT (37.6 ± 2.91) presented significant higher values (p=0.0002) compared to TNZ (26.03 ± 2.92). In conclusion, it seems that Ti alloy composition plays a significant role on ceramic bonding.

scholarly journals Shear Bond Strengths and Morphological Evaluation of Filled and Unfilled Adhesive Interfaces to Enamel and Dentine

2012 ◽  
Vol 2012 ◽  
pp. 1-9 ◽  
Author(s):  
Vajihesadat Mortazavi ◽  
Mohammadhosein Fathi ◽  
Ebrahim Ataei ◽  
Niloufar Khodaeian ◽  
Navid Askari
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Testing Machine ◽  
The Other ◽  
Adhesive Systems ◽  
Morphological Evaluation ◽  
Bond Strengths ◽  
Post Hoc ◽  
One Way Anova

In this laboratory study shear bond strengths of three filled and one unfilled adhesive systems to enamel and dentine were compared. Forty-eight extracted intact noncarious human mandibular molars were randomly assigned to two groups of 24 one for bonding to enamel and the other for bonding to dentine. Buccal and lingual surfaces of each tooth were randomly assigned for application of each one of filled (Prime & Bond NT (PBNT), Optibond Solo Plus (OBSP), and Clearfil SE Bond (CSEB)) and unfilled (Single Bond (SB)) adhesive systems (n=12). A universal resin composite was placed into the translucent plastic cylinders (3 mm in diameter and 2 mm in length) and seated against the enamel and dentine surfaces and polymerized for 40 seconds. Shear bond strength was determined using a universal testing machine, and the results were statistically analyzed using two-way ANOVA, one-way ANOVA,t-test, and Tukey HSD post hoc test with a 5% level of significance.There were no statistically significant differences in bond strength between the adhesive systems in enamel, but CSEB and SB exhibited significantly higher and lower bond strength to dentine, respectively, than the other tested adhesive systems while there were no statistically significant differences between PBNT and OBSP.

Effect of Steam Autoclaving on the Tensile Strength of Resin Cements Used for Bonding Two-Piece Zirconia Abutments

2017 ◽  
Vol 43 (2) ◽  
pp. 87-93 ◽  
Author(s):  
Marcos Alexandre Fadanelli ◽  
Flávia Lucisano Botelho do Amaral ◽  
Roberta Tarkany Basting ◽  
Cecilia Pedroso Turssi ◽  
Bruno Salles Sotto-Maior ◽  
...  
Keyword(s):  
Tensile Strength ◽  
Testing Machine ◽  
Resin Cement ◽  
The Other ◽  
Strength Testing ◽  
Resin Cements ◽  
Universal Testing ◽  
Cad Cam ◽  
The Mean ◽  
Adhesive Cement

The purpose of this study was to evaluate the effects of steam autoclave sterilization on the tensile strength of two types of resin cements used to bond customized CAD/CAM zirconia abutments onto titanium bases. Forty sets of zirconia abutments cemented to screwed titanium bases of implants analogs were divided into 4 groups (n = 10). Two groups were treated with a conventional chemically activated resin cement (ML, Multilink Ivoclar Vivadent) and the other two groups with a self-adhesive dual resin cement (RelyX U200, 3M ESPE). One group from each cement was submitted to steam autoclaving. The autoclave sterilization cycle was performed after 72 hours of cementation for 15 minutes at 121°C and 2.1 Kgf/cm2. The samples were subjected to tensile strength testing in a universal testing machine (200 Kgf, 0.5 mm/min), from which the means and standard deviations were obtained in Newtons. Results showed (via ANOVA and Tukey's test; α = 0.05) that in the absence of steam autoclaving, no difference was observed in tensile strength between the cements tested: ML: 344.87 (93.79) and U200: 280 (92.42) (P = .314). Steam autoclaving, however, significantly increased tensile strength for the ML: 465.42 (87.87) compared to U200: 289.10 (49.02) (P < .001). Despite the significant increase in the ML samples (P = .013), autoclaving did not affect the tensile strength of the U200 samples (P > 0.05). The authors concluded that steam autoclaving increases the mean tensile strength of the chemically activated cement compared to the dual-cure self-adhesive cement. The performance of both cements evaluated was similar if the sterilization step was disconsidered.

scholarly journals Shear bond strength of metallic and ceramic brackets using color change adhesives

2013 ◽  
Vol 18 (2) ◽  
pp. 76-80 ◽  
Author(s):  
Aisha de Souza Gomes Stumpf ◽  
Carlos Bergmann ◽  
José Renato Prietsch ◽  
Juliane Vicenzi
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Color Change ◽  
Testing Machine ◽  
Adhesive System ◽  
Bonding Material ◽  
Universal Testing ◽  
Adhesive Remnant Index ◽  
Ceramic Brackets ◽  
The Mean

OBJECTIVE: To determine the shear bond strength of orthodontic brackets using color change adhesives that are supposed to aid in removing excess of bonding material and compare them to a traditional adhesive. METHODS: Ninety metallic and ninety ceramic brackets were bonded to bovine incisors using two color change adhesives and a regular one. A tensile stress was applied by a universal testing machine. The teeth were observed in a microscope after debonding in order to determine the Adhesive Remnant Index (ARI). RESULTS: The statistical analysis (ANOVA, Tukey, and Kruskall-Wallis tests) demonstrated that the mean bond strength presented no difference when metallic and ceramic brackets were compared but the bond resistance values were significantly different for the three adhesives used. The most common ARI outcome was the entire adhesive remaining on the enamel. CONCLUSIONS: The bond strength was similar for metallic and ceramic brackets when the same adhesive system was used. ARI scores demonstrated that bonding with these adhesives is safe even when ceramic brackets were used. On the other hand, bond strength was too low for orthodontic purposes when Ortho Lite Cure was used.

scholarly journals Shear bond strength of brackets to demineralize enamel after different pretreatment methods

2011 ◽  
Vol 82 (1) ◽  
pp. 56-61 ◽  
Author(s):  
Rengin Attin ◽  
Bogna Stawarczyk ◽  
Defne Keçik ◽  
Michael Knösel ◽  
Dirk Wiechmann ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Resin Cement ◽  
The Other ◽  
Control Group ◽  
Demineralized Enamel ◽  
Group 5 ◽  
Group 2 ◽  
Group 1

Abstract Objective: To compare the influence of demineralized and variously pretreated demineralized enamel on the shear bond strength of orthodontic brackets. Materials and Methods: Sixty bovine enamel specimens were allocated to five groups (n  =  12). Specimens of group 1 were not demineralized and were not pretreated, but served as controls. The other specimens were demineralized to form artificial carious lesions. Samples from group 2 were only demineralized and were kept untreated in artificial saliva. The other samples were pretreated with highly concentrated fluoride preparations (group 3: Elmex Gelee, 1.23% F; group 4: Clinpro White Varnish, 2.23% F) or with an infiltrating resin (group 5: Icon). After respective pretreatments, brackets were adhesively fixed on all specimens with an adhesive system after etching with 35% phosphoric acid and application of a primer and bracket resin cement (Transbond XT). Bracket shear bond strength was evaluated with a universal testing machine. Statistical analysis was performed by one-way analysis of variance followed by a post-hoc Scheffé test. Results: Shear bond strength in control group 1 was statistically significantly greater compared with that in all other groups. Application of the infiltrating resin Icon (group 5) as pretreatment resulted in statistically significantly greater bond strength as compared with pretreatments with fluoride compounds (groups 3 and 4) and treatment provided without pretreatment (group 2). Groups 2, 3, and 4 did not significantly differ from each other. Conclusion: Pretreatment with the infiltrating resin is a beneficial approach to increasing the shear bond strength of brackets to demineralized enamel.

scholarly journals Effects of 10-MDP Based Primer on Shear Bond Strength between Zirconia and New Experimental Resin Cement

Materials ◽  
2020 ◽  
Vol 13 (1) ◽  
pp. 235 ◽  
Author(s):  
Francesco Valente ◽  
Luan Mavriqi ◽  
Tonino Traini
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Maximum Load ◽  
Load Resistance ◽  
Resin Cement ◽  
Dihydrogen Phosphate ◽  
Zirconia Ceramics ◽  
Adhesive Cementation ◽  
Composite Cylinders ◽  
One Way Anova

To date, numerous materials in the dental field are marketed to ensure stable adhesive cementation of zirconia ceramics (Y-TZP). The aims of this study were to assess the shear bond strength of the new experimental cement Surgi Dual Flo’ Zr to Y-TZP compared to Panavia V5 cement, and to evaluate the effect of 10-MDP (10-methacryloyloxydecyl dihydrogen phosphate) containing primer on their bond strength. Twenty composite cylinders and Y-TZP disks were adhesively luted and divided into four groups based on cement type used and application or not of 10-MDP. The groups (n = 5 each) were S 10MDP (Surgi Dual Flo’ Zr with 10-MDP); S no 10MDP (Surgi Dual Flo’ Zr without 10-MDP); P 10MDP (Panavia V5 with 10-MDP); P no 10MDP (Panavia V5 without 10-MDP). Maximum load resistance (ML) and shear bond strength (SBS) were tested and mode of failure qualitative documented via scanning electron microscopy. The data were analyzed with one-way ANOVA, Holm-Sidak method, and Bayesian analysis. ML and SBS were significantly higher in S 10MDP than in S no 10MDP; and in P 10MDP than in P no 10MDP (p < 0.05). No significant differences were found between S 10MDP and P 10MDP; S no 10MDP and P no 10MDP (p > 0.05). Cohesive, adhesive, and mixed failure occurred among the groups. Bond strength between the experimental resin-based cement and Y-TZP was adequate for clinical application when 10-MDP was added. 10-MDP containing primer was effective improving the bond strength to Y-TZP more than the different type of resinous cement.

scholarly journals Effect of previous desensitizer and rewetting agent application on shear bond strength of bonding

2010 ◽  
Vol 9 (4) ◽  
Author(s):  
Carlos José Soares ◽  
Paulo César F. Santos Filho ◽  
Bruno C. F. Barreto ◽  
Adérito S. Mota
Keyword(s):  
Bond Strength ◽  
Mechanical Testing ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Adhesive System ◽  
Single Bond ◽  
Crosshead Speed ◽  
Tukey Test ◽  
One Step ◽  
One Way Anova

This study evaluated the effect of desensitizer and rewetting agent on dentin shear bond strength. One hundred thirty five bovine incisive teeth had their buccal surfaces ground down to produce a fl at superficial dentin surfaces and received the following treatments: G1- One Step Plus (OSP) and resin cylinder adhesive fi xation (RI); G2- Gluma One Bond (GOB) and RI; G3- Single Bond (SB) and RI; G4- Aqua-Prep (AP) + OSP and RI; G5- Gluma Desensitizer (GD) + GOB and RI; G6- GD + SB and RI; G7- GD + OSP and RI; G8- AP + GOB and RI; G9- AP + SB and RI. The specimens were stored at 37°C and 100% humidity for 24 hours and a shear bond test was performed with a mechanical testing machine, at a crosshead speed of 0.5 mm⁄min. The data were submitted to one-way ANOVA followed by the Tukey test (p<0.05). The results (MPa) were: G1: 10.75(2.64)a; G2: 10.28(2.58)a; G3: 11.63(4.59)a; G4: 10.93(4.88)a; G5: 10.15(3.95)a; G6: 11.82(4.14)a; G7: 9.85(2.15)a; G8: 5.48(1.94)b; G9: 10.62(2.83)a. The resistance of the GOB adhesive system was negatively affected by AP application. The use of desensitizer and rewetting agent does not compromise the bond strength when they are compatible with the adhesive system used.

scholarly journals Repair bond strength and degradation of glass ionomer cements after mechanical and chemical challenges

2020 ◽  
Vol 19 ◽  
pp. e201715
Author(s):  
Leandro Rahal Mestrener ◽  
Sandra Rahal Mestrener ◽  
Cleidiel Aparecido Araujo Lemos ◽  
André Luiz Fraga Briso ◽  
Renato Herman Sundfeld ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
The Other ◽  
Acid Solutions ◽  
Glass Ionomer Cements ◽  
Glass Ionomer ◽  
Universal Testing ◽  
Before And After ◽  
Bond Strengths

Aim: Little is known about the reparability of glass ionomer cements (GICs) after storage in acid environments. The aim of this study was to evaluate the solubility and repairability of GICs immersed in acid solutions and subjected to brushing. Methods: Thirty discs of each GIC (Vitremer, VitroFil LC, VitroFil, and Maxxion R) were divided into three immersion groups: distilled water, Coca-Cola, or hydrochloric acid (HCl), then subjected to brushing. The weight of discs was measured before and after the immersions to determine mass alteration. Each disc was repaired, by adding the same brand of GIC over its surface. After immersing the repaired specimens in same solutions, shear bond strengths using universal testing machine were measured. Two-way ANOVA and Tukey’s test was used (α=0.05). Results: Resin-modified GICs degrade after HCl immersion followed by brushing (p<0.05), while self-cured GICs were negatively affected by all challenges (p<0.05). The challenges decreased the repair strength for VitroFil LC (p<0.05), which had higher repair shear bond strength than the other GICs (p<0.05), exhibiting most cohesive failures. Conclusion: Self-cured GICs degraded when immersed in all acid solutions with brushing while resin-modified GICs only degraded following HCl immersion with brushing. Despite exhibiting the best repair results, VitroFil LC was the only GIC that was influenced by all the acid challenges.

Evaluation of Bond Strength and Microleakage of a Novel Metal-titanate Antibacterial Agent

2016 ◽  
Vol 41 (3) ◽  
pp. E48-E56 ◽  
Author(s):  
S Deng ◽  
KH Chung ◽  
DCN Chan ◽  
C Spiekerman
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Adhesive System ◽  
Class V ◽  
Bonding Agents ◽  
Dental Adhesive ◽  
Universal Testing ◽  
The Mean ◽  
Post Hoc

SUMMARY Objectives: To evaluate the effect on both bond strength and microleakage of incorporation of a novel antibacterial nanoparticulate metal-titanate complex (nMT) into a dental adhesive system. Materials and Methods: Eighty extracted human molars were prepared to determine whether incorporation of nMT into bonding agents can affect shear bond strength (SBS) and adhesive strength fatigue. SBS was measured with a universal testing machine, and the peak force at failure was recorded. An electromechanical fatigue machine was used for cyclic loading treatment of specimens. Differences in the SBS values among groups were identified using analysis of variance and Tukey post hoc analyses (α=0.05). Twenty standard Class V cavities were restored to examine microleakage when the primer/bonding resin was modified with 10 wt% nMT. Microleakage at the enamel and dentin margins was calculated as a percentage of the full length of the cavity. Results of the microleakage experiment were analyzed with paired and independent sample t-tests (α=0.05). Results: The mean (± standard deviation) shear bond strength values of before fatigue and after fatigue ranged from 21.9 (2.5) MPa to 23.9 (3.8) MPa and from 17.1 (2.5) MPa to 17.7 (2.5) MPa respectively. No statistically significant differences in failure force were observed among groups (p=0.70). Microleakage under all conditions was significantly greater in the dentin margins than in the enamel margins (p&lt;0.05). There was no evidence that microleakage differed between the experimental groups with modified primer and bonding resin. Conclusions: Incorporating nMT into a dental adhesive system will not compromise the resin composite's tooth bonding and sealing ability.

scholarly journals Water and Saliva Contamination Effect on Shear Bond Strength of Brackets Bonded with a Moisture-Tolerant Light Cure System

2009 ◽  
Vol 79 (1) ◽  
pp. 127-132 ◽  
Author(s):  
Ascensión Vicente ◽  
Ana Mena ◽  
Antonio José Ortiz ◽  
Luis Alberto Bravo
Keyword(s):  
Bond Strength ◽  
Water Contamination ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
The Other ◽  
Universal Testing ◽  
Contamination Effect ◽  
Bond Strengths ◽  
Saliva Contamination ◽  
Lower Incisors

Abstract Objective: To evaluate the effects of water and saliva contamination on shear bond strength of brackets bonded with a moisture-tolerant light cure system. Materials and Methods: Brackets were bonded to 240 bovine lower incisors divided into 12 groups. Four bonding procedures were evaluated, including (1) TSEP/Transbond XT, (2) TMIP/ Transbond XT, (3) TSEP/Transbond PLUS, and (4) TMIP/Transbond PLUS, each under three different bonding conditions: without contamination, with water contamination, and with saliva contamination. Shear bond strength was measured with a universal testing machine. The adhesive remnant on the teeth was quantified with the use of image analyzing equipment. Results: Without contamination, bond strengths for the four procedures were similar (P &gt; .05). TSEP/Tranbond PLUS and TMIP/Transbond PLUS left significantly less adhesive on the teeth after debonding than TSEP/Transbond XT and TMIP/Transbond XT (P &lt; .008). Bond strength and adhesive remaining for TMIP/Transbond XT contaminated with water or saliva showed significantly worse performance than the other procedures evaluated (P &lt; .008). Contamination (with water or saliva) did not affect either bond strength or adhesive remaining on the teeth for TSEP/ Transbond XT, TSEP/Transbond PLUS, or TMIP/Transbond PLUS (P &gt; .017), although for TMIP/ Transbond XT, both variables showed significant reductions after contamination (P &lt; .017). Conclusion: TSEP/Transbond PLUS, TMIP/Transbond PLUS, and TSEP/Transbond XT showed greater tolerance to wet conditions than was shown by TMIP/Transbond XT.

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