Effect of Steam Autoclaving on the Tensile Strength of Resin Cements Used for Bonding Two-Piece Zirconia Abutments

2017 ◽  
Vol 43 (2) ◽  
pp. 87-93 ◽  
Author(s):  
Marcos Alexandre Fadanelli ◽  
Flávia Lucisano Botelho do Amaral ◽  
Roberta Tarkany Basting ◽  
Cecilia Pedroso Turssi ◽  
Bruno Salles Sotto-Maior ◽  
...  
Keyword(s):  
Tensile Strength ◽  
Testing Machine ◽  
Resin Cement ◽  
The Other ◽  
Strength Testing ◽  
Resin Cements ◽  
Universal Testing ◽  
Cad Cam ◽  
The Mean ◽  
Adhesive Cement

The purpose of this study was to evaluate the effects of steam autoclave sterilization on the tensile strength of two types of resin cements used to bond customized CAD/CAM zirconia abutments onto titanium bases. Forty sets of zirconia abutments cemented to screwed titanium bases of implants analogs were divided into 4 groups (n = 10). Two groups were treated with a conventional chemically activated resin cement (ML, Multilink Ivoclar Vivadent) and the other two groups with a self-adhesive dual resin cement (RelyX U200, 3M ESPE). One group from each cement was submitted to steam autoclaving. The autoclave sterilization cycle was performed after 72 hours of cementation for 15 minutes at 121°C and 2.1 Kgf/cm2. The samples were subjected to tensile strength testing in a universal testing machine (200 Kgf, 0.5 mm/min), from which the means and standard deviations were obtained in Newtons. Results showed (via ANOVA and Tukey's test; α = 0.05) that in the absence of steam autoclaving, no difference was observed in tensile strength between the cements tested: ML: 344.87 (93.79) and U200: 280 (92.42) (P = .314). Steam autoclaving, however, significantly increased tensile strength for the ML: 465.42 (87.87) compared to U200: 289.10 (49.02) (P < .001). Despite the significant increase in the ML samples (P = .013), autoclaving did not affect the tensile strength of the U200 samples (P > 0.05). The authors concluded that steam autoclaving increases the mean tensile strength of the chemically activated cement compared to the dual-cure self-adhesive cement. The performance of both cements evaluated was similar if the sterilization step was disconsidered.

scholarly journals Bond strength of glass-ceramic cemented to a zirconia structure: influence of adhesive cementation strategy

2016 ◽  
Vol 64 (2) ◽  
pp. 140-147
Author(s):  
Gilvan Cutrim TAVARES ◽  
Renan Macedo Cutrim TAVARES ◽  
Milton Edson MIRANDA ◽  
Cecilia Pedroso TURSSI ◽  
Roberta Tarkany BASTING ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Adhesive System ◽  
Resin Cement ◽  
The Other ◽  
Universal Testing ◽  
Adhesive Cementation ◽  
Adhesive Cement ◽  
One Way Anova

ABSTRACT Objective This study evaluated the shear bond strength (SBS) of lithium disilicate glass (LDG) ceramic bonded to a zirconia (Y-TZP), using different cementation strategies. Methods LDG ceramic cylinders were cemented to Y-TZP structure according to the following adhesive system (AS)/resin cement (RC) (n = 15): U- self-adhesive dual-cure RC; AMBAR- AS containing phosphate monomers (PM) + dual-cure RC; group SBU: PM+Silane/AS + light-cure RC; group ALLB: PM/AS + dual-cure RC. Specimens were subjected to SBS in a universal testing machine (0.5 mm/min). Data (MPa) were subjected to one-way ANOVA and Tukey's test (α = 0,05). Results The groups SBU and ALLB had significantly higher SBS than those provided by the group U, in which the lowest values were observed. For the AMBAR group, intermediate SBS values were found, which did not differ significantly from the values observed in the other groups. Conclusion Regardless of resins cement, the use of adhesives containing phosphate monomers provided superior bond strength than self-adhesive cement.

scholarly journals Influence of temporary cement in the tensile strenght of full crowns cemented with resin cement

2015 ◽  
Vol 18 (3) ◽  
pp. 52
Author(s):  
Daniela Ribon Galazi ◽  
Leticia Ferreira de Freitas Brianezzi ◽  
Adriana Regina Cruz Grando De Góes ◽  
Rafael Francisco Lia Mondelli ◽  
Áquira Ishikiriama ◽  
...  
Keyword(s):  
Tensile Strength ◽  
Testing Machine ◽  
Negative Influence ◽  
Resin Cement ◽  
Distilled Water ◽  
Third Molars ◽  
Tukey Test ◽  
Universal Testing ◽  
Adhesive Cementation ◽  
Traction Test

<p>This study evaluated the influence of residual eugenol on the tensile strength in the ceromer crowns cementation, using resin cement. Thirty-nine third molars were prepared for a full crown. For each prepared tooth one provisional and one ceromer crown were made. The teeth were divided into three groups according the temporary cement (n=13): GTB: Temp Bond; GTBNE: Temp Bond NE and GDY: Dycal. After temporary cementation, the teeth were kept in distilled water for one week and then submitted to traction test in a universal testing machine (EMIC DL 500), using a 200Kgf load cell at 0.5mm/min speed. After the test, the teeth were cleaned and received the final adhesive cementation of ceromer crowns. Next, the specimens were kept in distilled water (37<sup>0</sup>C) for a week and then the traction test was performed, also at 0,5mm/min. The comparison among groups was carried out by variance analysis (ANOVA) followed by the Tukey test (p≤0.05). The results (Kgf) of provisional cementation for groups GTB, GTBNE and GDY were respectively: 2.75 ± 1.35b, 3.43 ± 1.66ab, and 4.48 ± 1.11a. The results of the adhesive cementation (Kgf) were respectively: 42.71 ± 15.33b, 57.59 ± 15.66a, and 54.75 ± 15.28ab. It was concluded that the temporary cement containing eugenol shows negative influence on the removal resistance of crowns cemented with resin cement. </p>

Effect of Artificial Aging and Surface Treatment on Bond Strengths to Dental Zirconia

2013 ◽  
Vol 38 (2) ◽  
pp. 168-176 ◽  
Author(s):  
J Perdigão ◽  
SD Fernandes ◽  
AM Pinto ◽  
FA Oliveira
Keyword(s):  
Surface Treatment ◽  
Artificial Aging ◽  
Testing Machine ◽  
Significance Level ◽  
Diamond Blade ◽  
Universal Testing ◽  
Bond Strengths ◽  
The Mean ◽  
Post Hoc ◽  
Adhesive Cement

SUMMARY The objective of this project was to study the influence of artificial aging and surface treatment on the microtensile bond strengths (μTBS) between zirconia and a phosphate monomer–based self-adhesive cement. Thirty zirconia disks (IPS e.max ZirCAD, Ivoclar Vivadent) were randomly assigned to two aging regimens: AR, used as received, which served as a control, and AG, artificial aging to simulate low-temperature degradation. Subsequently, the disks of each aging regimen were assigned to three surface treatments: NT, no surface treatment; CO, surface silicatization with CoJet sand (3M ESPE); and ZP, zirconia surface treated with Z-Prime Plus (Bisco Inc). Thirty discs were made of Filtek Z250 (3M ESPE) composite resin and luted to the zirconia discs using RelyX Unicem (3M ESPE). The specimens were sectioned with a diamond blade in X and Y directions to obtain bonded beams with a cross-section of 1.0 ± 0.2 mm. The beams were tested in tensile mode in a universal testing machine at a speed of 0.5 mm/min to measure μTBS. Selected beams were selected for fractographic analysis under the SEM. Statistical analysis was carried out with two-way analysis of variance and Dunnett T3 post hoc test at a significance level of 95%. The mean μTBS for the three AR subgroups (AR-NT, AR-CO, and AR-ZP) were significantly higher than those of the corresponding AG groups (p&lt;0.0001). Both AR-CO and AR-ZP resulted in statistically significant higher mean bond strengths than the group AR-NT (p&lt;0.006 and p&lt;0.0001, respectively). Both AG-CO and AG-ZP resulted in statistically significant higher mean bond strengths than the group AG-NT (both at p&lt;0.0001). Overall, AG decreased mean μTBS. Under the SEM, mixed failures showed residual cement attached to the zirconia side of the beams. CO resulted in a characteristic roughness of the zirconia surface. AR-ZP was the only group for which the amount of residual cement occupied at least 50% of the interface in mixed failures.

scholarly journals Influence of activation modes on diametral tensile strength of dual-curing resin cements

2005 ◽  
Vol 19 (4) ◽  
pp. 267-271 ◽  
Author(s):  
Renata Garcia Fonseca ◽  
Juliana Gomes dos Santos ◽  
Gelson Luis Adabo
Keyword(s):  
Tensile Strength ◽  
Zinc Phosphate ◽  
Chemical Activation ◽  
Testing Machine ◽  
Resin Cement ◽  
The Self ◽  
Resin Cements ◽  
Significant Difference ◽  
Dual Curing ◽  
Diametral Tensile Strength

In metallic restorations, the polymerization of dual-curing resin cements depends exclusively on chemical activation. The effect of the lack of photoactivation on the strength of these cements has been rarely studied. This study evaluated the influence of activation modes on the diametral tensile strength (DTS) of dual-curing resin cements. Base and catalyst pastes of Panavia F, Variolink II, Scotchbond Resin Cement, Rely X and Enforce were mixed and inserted into cylindrical metal moulds (4 x 2 mm). Cements were either: 1) not exposed to light (chemical activation = self-cured groups) or 2) photoactivated through mylar strips (chemical and photo-activation = dual-cured groups) (n = 10). After a 24 h storage in 37ºC distilled water, specimens were subjected to compressive load in a testing machine. A self-curing resin cement (Cement-It) and a zinc phosphate cement served as controls. Comparative analyses were performed: 1) between the activation modes for each dual-curing resin cement, using Student’s t test; 2) among the self-cured groups of the dual-curing resin cements and the control groups, using one-way ANOVA and Tukey’s test (alpha = 0.05). The dual-cured groups of Scotchbond Resin Cement (53.3 MPa), Variolink II (48.4 MPa) and Rely X (51.6 MPa) showed higher DTS than that of self-cured groups (44.6, 40.4 and 44.5 MPa respectively) (p < 0.05). For Enforce (48.5 and 47.8 MPa) and Panavia F (44.0 and 43.3 MPa), no significant difference was found between the activation modes (p > 0.05). The self-cured groups of all the dual-curing resin cements presented statistically the same DTS as that of Cement-It (44.1 MPa) (p > 0.05), and higher DTS than that of zinc phosphate (4.2 MPa). Scotchbond Resin Cement, Variolink II and Rely X depended on photoactivation to achieve maximum DTS. In the absence of light, all the dual-curing resin cements presented higher DTS than that of zinc phosphate and statistically the same as that of Cement-It (p > 0.05).

scholarly journals Effect of beverages on surface properties of resin-based sealants

2017 ◽  
Vol 16 ◽  
pp. 1-7
Author(s):  
Bruna Genari ◽  
Vicente Castelo Branco Leitune ◽  
João Henrique Macedo Saucedo ◽  
Susana Maria Werner Samuel ◽  
Fabrício Mezzomo Collares
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Resin Cement ◽  
Control Group ◽  
Resin Cements ◽  
Universal Testing ◽  
Halogen Light ◽  
Significant Difference ◽  
Tooth Surfaces ◽  
Light Curing

Self-adhesive, dual-polymerizing resin cements require no treatment to the prepared tooth surfaces before cementation. Aim: The aim of this study was to evaluate the influence of curing mode on bond strength (BS) of three cementing systems to bovine dentin. Methods: The buccal enamel surfaces of 50 bovine incisors were removed to expose dentin and to flat the surface. The teeth were divided into five groups (n=10), which consisted of two resin cements (Multilink and Clearfil SA Cement) that were tested in dual- (halogen light for 40 s) and self-cured modes, and a control (RelyX ARC). Two cylinders of resin cements (1.0 mm X 0.75 mm) were prepared on each bonded dentin surface. After 24h at 37oC, resin cylinders were subjected to micro-shear testing in a universal testing machine (4411/Instron - 0.5 mm/min). Data were statistically analyzed by two-way ANOVA, Tukey and Dunnett`s test (5%). Results: Multilink showed higher BS than those observed on Clearfil SA. Light-curing resulted in higher BS for both Multilink and Clearfil SA. When Multilink was light-cured, no significant difference on BS was demonstrated between it and RelyX ARC. Conclusions: The highest BS values were obtained in control group and light-cured Multilink resin cement.

scholarly journals Evaluation of physical-mechanical properties of self-adhesive versus conventional resin cements

2020 ◽  
Vol 19 ◽  
pp. e208204
Author(s):  
Maria Helena Rossy Borges ◽  
Carmen Gilda Tavares Dias ◽  
Cristiane de Melo Alencar ◽  
Cecy Martins Silva ◽  
Renata Antunes Esteves
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Compressive Strength ◽  
Testing Machine ◽  
Strength Test ◽  
Resin Cement ◽  
Resin Cements ◽  
Tensile Strength Test ◽  
Diametral Tensile Strength ◽  
One Way Anova

Aim: The purpose of this study was to compare the microhardness, diametral tensile strength, compressive strength and the rheological properties of self-adhesive versus conventional resin cements. Methods: Specimens of a conventional (RelyX ARC) and 3 self-adhesive (RelyX U200, Maxcem Elite, Bifix SE) types of resin cements were prepared. The Knoop test was used to assess the microhardness, using a Microhardness Tester FM 700. For the diametral tensile strength test, a tensile strength was applied at a speed of 0.6 mm/minute. A universal testing machine was used for the analysis of compressive strength and a thermo-controlled oscillating rheometer was used for the Rheology test. One-way ANOVA and Tukey’s test (α=0.05) were used for data analysis. Results: According to microhardness analysis, all the cements were statistically similar (p>0.05), except for Maxcem that presented lower hardness compared with the other cements in relation to the top surface (p<0.05). In the diametral tensile strength test, Relyx U200 and RelyX ARC cements were statistically similar (p>0.05), presented higher value when compared to the Maxcem and Bifix cements (p<0.05). The compressive strength of RelyX ARC and Maxcem Elite cements was statistically higher than RelyX U200 and Bifix cements (p<0.05). Regarding the rheology test, Maxcem Elite and RelyX ARC cements showed a high modulus of elasticity. Conclusions: The self-adhesive cements presented poorer mechanical properties than conventional resin cement. Chemical structure and types of monomers employed interfere directly in the mechanical properties of resin cements.

scholarly journals Retention of provisional crowns cemented with eight temporary cements: comparative study

2004 ◽  
Vol 12 (3) ◽  
pp. 209-212 ◽  
Author(s):  
Mariana Ribeiro de Moraes Rego ◽  
Luiz Carlos Santiago
Keyword(s):  
Tensile Strength ◽  
Comparative Study ◽  
Testing Machine ◽  
Strength Test ◽  
The Other ◽  
Universal Testing Machine ◽  
Tensile Strength Test ◽  
Universal Testing ◽  
Significant Difference ◽  
Crown Preparation

Many temporary cements are commercially available; therefore, it is necessary to indicate them for each clinical requirement with regard to the tensile strength of prosthetic retainers. Thus, the purpose of this study was to compare the retention of provisional crowns cemented with eight temporary cements, over full crown preparations with standardized mechanical principles as height, taper, and length. For that purpose, eighty human first premolars received full crown preparation with standardized height and taper. Provisional crowns were fabricated and luted with eight brands of temporary cements. Twenty four hours after cementation, the restorations were submitted to tensile strength test in a universal testing machine and the data submitted to ANOVA and Bonferroni tests. Mean tensile strength values ranged from 20.1N for Nogenol cement to 67.5N for Hydro C cement. Statistically significant difference (p<0.05) was found between Hydro C and the other groups, except for Temp Bond and Rely X Temp, which presented statistically significant difference when compared to Freegenol and Nogenol temporary cements. The crowns cemented with Hydro C cement were more retentive that than those cemented with the other cements, except for Rely X Temp and Temp Bond. The less retentive crowns were those cemented with Nogenol and Freegenol temporary cements.

scholarly journals Effect of thermocycling on the bond strength of a glass-infiltrated ceramic and a resin luting cement

2003 ◽  
Vol 11 (1) ◽  
pp. 61-67 ◽  
Author(s):  
Osvaldo Daniel Andreatta Filho ◽  
Marco Antonio Bottino ◽  
Renato Sussumu Nishioka ◽  
Luiz Felipe Valandro ◽  
Fabíola Pessoa Pereira Leite
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Silica Coating ◽  
Deionized Water ◽  
Resin Cement ◽  
P Value ◽  
Universal Testing ◽  
Adhesive Surface ◽  
Luting Cement ◽  
The Mean

The aim of the present study was to evaluate the effect of thermocycling on the bond strength between the surface of the glass-infiltrated alumina ceramic In-Ceram (VITA) and the Panavia F resin cement (Kuraray CO.). Four 5x6x6mm In-Ceram blocks were obtained. One of the 6x6mm faces of each block was conditioned with Cojet - System (tribochemical silica coating, ESPE-3M) and then luted under a constant 750g pressure with Panavia F cement to another identical face of a resin composit block (Clearfil AP-X, Kuraray) obtained by reproduction of the ceramic one from Express (3M) addition curing silicone impressions. The four sets so formed by ceramic, luting cement and resin have been each one serially sectioned in 20 sticks so that the adhesive surface in each presented 1mm² of area. The samples were divided in 2 groups (n=10): G1- stored for 7 days in deionized water at 36 ± 2ºC; G2 - thermocycled 1500 times between 5 and 55ºC dwell times. The microtensile tests were accomplished in an universal testing machine (EMIC) at a crosshead speed of 0,5 mm/min. The results showed that the mean tensile bond strength values (MPa) for the group G2: (22,815 ± 5,254) had not statistically differ of the values of group G1: (25,628 ± 3,353) (t = 1,427; gl = 18; p-value = 0,171), at the level of a= 5%. It can be concluded that the thermocycling technique used in the present experiment had not produced statistically significant differences between the bond strength results of the specimens obtained by the two used techniques.

scholarly journals Effect of Adhesive Gap Setting on Fracture Resistance of All-ceramic Crowns

2020 ◽  
Vol 14 (1) ◽  
pp. 600-607
Author(s):  
Mohammed Zahran
Keyword(s):  
Fracture Strength ◽  
Fracture Resistance ◽  
Testing Machine ◽  
Resin Cement ◽  
All Ceramic ◽  
Complete Failure ◽  
Ceramic Crowns ◽  
The Mean ◽  
Adhesive Cement ◽  
Cerec 3D

Background: Several factors might affect the fracture resistance of all-ceramic crowns, including cement thickness. Aim: To evaluate the influence of cement thickness on the fracture resistance. Objective: To determine the effect of varying the adhesive gap thickness on the fracture loads of all-ceramic CEREC 3D molar crowns. Methods: Standardized prepared epoxy resin molar dies (Viade Inc.) were fabricated. A standard molar crown was designed using a CEREC 3D machine (Sirona Dental Systems). Twenty-four crowns were milled from Vita Mark II blocks (Vita Zahnfabrik), using adhesive gap settings of 30, 60 and 90 µm (n=8). A dual-cure resin cement (PanaviaF 2.0, Kuraray) was used to cement the crowns to their respective dies, following manufacturer's recommendation. After 1 week of storage in distilled water at 37°C, each crown was loaded in compression until complete failure in a universal testing machine (Instron 8501) and fracture loads (N) were recorded. Fractured specimens were sectioned to determine cement thickness. Sections were examined using a traveling light microscope to measure cement thickness. Data were statistically analyzed using one-way ANOVA test and Pearson's correlation at (α=0.05). Results: The mean fracture loads and standard deviation values in N were 1,267.57 (122.82), 1,225.20 (179.46) and 1,180.76 (161.77) for the crowns with 30, 60 and 90µm, respectively. ANOVA indicated no significant differences among mean fracture strength values (p = 0.55). All crowns failed in a catastrophic mode and were not repairable. Conclusions: Adhesive cement gap as achieved with three CEREC 3D settings from 30 to 90µm had no significant effect on fracture strength of crowns made from Vita Mark II blocks.

scholarly journals Compressive and diametral tensile strength of glass ionomer cements

2004 ◽  
Vol 12 (4) ◽  
pp. 344-348 ◽  
Author(s):  
Eduardo Bresciani ◽  
Terezinha de Jesus Esteves Barata ◽  
Ticiane Cestari Fagundes ◽  
Akimi Adachi ◽  
Marina Martins Terrin ◽  
...  
Keyword(s):  
Tensile Strength ◽  
Testing Machine ◽  
Glass Ionomer Cement ◽  
Mean Value ◽  
Atraumatic Restorative Treatment ◽  
Glass Ionomer ◽  
Restorative Treatment ◽  
Significant Difference ◽  
The Mean ◽  
Diametral Tensile Strength

The aim of this study was to compare, in different periods of time, the compressive and diametral tensile strength of a traditional high viscous glass ionomer cement: Fuji IX (GC Corporation), with two new Brazilian GIC's: Vitro-Molar (DFL) and Bioglass R (Biodinamica), all indicated for the Atraumatic Restorative Treatment (ART) technique. Fifteen disk specimens (6.0mm diameter x 3.0mm height) for the diametral tensile strength (DTS) test and fifteen cylindrical specimens (6.0mm diameter x 12.0mm height) for the compressive strength (CS) test were made of each GIC. Specimens were stored in deionized water at 37º C and 100% of humidity in a stove until testing. Five specimens of each GIC were submitted to CS and DTS test in each period, namely 1 hour, 24 hours and 7 days. The specimens were tested in a testing machine (Emic) at a crosshead speed of 1.0mm/min for CS and 0.5mm/min for the DTS test until failure occurred. The data were submitted to two-way ANOVA and Tukey tests (alpha=0.05). The mean CS values ranged from 42.03 to 155.47MPa and means DTS from 5.54 to 13.72 MPa, with test periods from 1h to 7 days. The CS and DTS tests showed no statistically significant difference between Fuji IX and Vitro Molar, except for CS test at 1-hour period. Bioglass R had lowest mean value for CS of the cements tested. In DTS test Bioglass R presented no statistically significant differences when compared with all others tested GICs at 1-hour period and Bioglass R presented no difference at 24-hour and 7-day periods when compared to Vitro-Molar. Further studies to investigate other physical properties such as fracture toughness and wear resistance, as well as chemical composition and biocompatibility, are now needed to better understand the properties of these new Brazilian GIC's.

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