scholarly journals COMPARATIVE STUDY OF THE SHEAR BOND STRENGTH OF COMPOSITE RESIN TO DENTAL ENAMEL CONDITIONED WITH PHOSPHORIC ACID OR Nd: YAG LASER

1997 ◽  
Vol 11 (4) ◽  
pp. 245-248 ◽  
Author(s):  
Carlos de Paula EDUARDO ◽  
Wilson Tavares de OLIVEIRA JUNIOR ◽  
Silvio Issáo MYAKI ◽  
Denise Maria ZEZELL

This study has been focused on a comparison between the shear bond strength of a composite resin attached to dental enamel surface, after a 35% phosphoric acid etching and after a Nd:YAG laser irradiation with 165.8 J/cm2 of energy density per pulse. After etching and attaching resin to these surfaces, the specimens were thermocycled and then underwent the shearing bond strength tests at a speed of 5 mm/min. The results achieved, after statistical analysis with Student's t-test, showed that the adhesion was significantly greater in the 35% phosphoric acid treated group than in the group treated with the Nd:YAG laser, thus demonstrating the need for developing new studies to reach the ideal parameters for an effective enamel surface conditioning as well as specific adhesives and composite resins when Nd:YAG laser is used

2014 ◽  
Vol 25 (6) ◽  
pp. 519-523 ◽  
Author(s):  
Erica Moreno Zanconato-Carvalho ◽  
João Felipe Bruniera ◽  
Natália Spadini de Faria ◽  
Vivian Colucci ◽  
Danielle Cristine Messias

Surface treatment of dentin before the bleaching procedure may affect its permeability and influence the bond strength of restorative materials. This study evaluated the influence of surface treatment before the bleaching on shear bond strength (SBT) of restorative materials to intracoronal dentin. Dentin slabs were subjected to surface treatment: no bleaching (control - CON), no surface treatment + bleaching (HP), 37% phosphoric acid + bleaching (PA) and Er:YAG laser + bleaching (L). After the bleaching procedure, specimens (n=10) were restored with: microhybrid composite resin (MH), flowable composite resin (F), and resin-modified glass-ionomer cement (RMGIC). The shear test was carried out. ANOVA and Tukey's test (α=0.05) showed significant difference for surface treatment and restorative materials (p<0.05). CON presented higher STB and was statistically different from HP (p<0.05). PA and L showed intermediate values and were statistically similar to CON and HP (p>0.05). STB for MH and F were higher than RMGIC (p<0.05), and did not differ from each other (p>0.05). The surface treatments with phosphoric acid and Er:YAG laser before the bleaching procedure provided shear bond strength at the same level of unbleached dentin and the composite resins presented superior bond strength to the intracoronal dentin.


2002 ◽  
Vol 13 (3) ◽  
pp. 175-178 ◽  
Author(s):  
Maria Cristina Borsatto ◽  
Alma Blásida Elisaur Benitez Catirse ◽  
Regina Guenka Palma Dibb ◽  
Telma Nunes do Nascimento ◽  
Renata Andréa Salvitti de Sá Rocha ◽  
...  

The aim of this study was to evaluate the shear bond strength of a composite resin to dental enamel, using three different surface treatments. Fifteen sound third molars were randomly assigned to three groups. The mesial and distal surfaces were flattened and covered using adhesive tape with a central orifice delimiting the adhesion area (7.07 mm²). Group I, the enamel surface was conditioned with 37% phosphoric acid for 15 s; group II, the surface was treated using air abrasion with aluminum oxide; group III, the enamel surface was treated using an association of air abrasion with aluminum oxide and 37% phosphoric acid. The Single Bond (3M) adhesive system was applied and a Teflon matrix was placed and filled with composite resin Z-100 (3M) and light-cured. The shear bond strength test was performed with a universal testing machine. The acid etching technique and air abrasion with aluminum oxide associated with acid etching had the highest shear bond strength values. Data were subjected to statistical analysis using ANOVA and the Tukey test, and no statistically significant difference in shear bond strength was observed between group I (12.49 ± 2.85 MPa) and group III (12.59 ± 2.68 MPa). In contrast, both groups had statistically better shear bond strengths compared to group II (0.29 ± 0.56 MPa; p<0.05). Air abrasion with aluminum oxide does not substitute acid etching. The association of these methods to obtain adequate adhesion to the substrate is necessary.


2018 ◽  
Vol 21 (4) ◽  
pp. 395
Author(s):  
Jaiane Bandoli Monteiro ◽  
Ricardo Toledo Abreu ◽  
Lívia Salgado ◽  
Thais Cachuté Paradella ◽  
Ivone De Oliveira Salgado ◽  
...  

<p><strong>Objective</strong>: The aim of this study was to evaluate the shear bond strength (SBS) of two materials for bonding orthodontic brackets on dental enamel before and after thermocycling. <strong>Material and Methods: </strong>Forty bovine incisors were divided into four groups (n=10). All teeth were etched with 35% phosphoric acid (3M Espe). For bonding of the brackets, G1 and G2 received orthodontic composite resin (Fill Magic Ortodôntico) and G3 and G4, an adhesive (ScotchBond) was used before the orthodontic resin Transbond XT (3M Unitek). G1 and G3 were kept at 37ºC for 24h and G2 and G4 were submitted to thermocycling (5000 cycles, at 5ºC - 55ºC) prior to SBS testing, performed by a universal machine (EMIC) at 1 mm/min, with a 50kgf load cell. Results were analyzed with two-way ANOVA, followed by Tukey's test (p=0.05). Adhesive surfaces were evaluated through stereomicroscopy and classified according to the type of failure presented. <strong>Results</strong>: Surface treatment with dental adhesive presented higher SBS values, regardless thermocycling (G3: 12.01 MPa; G4: 12.36 MPa) and the lowest values occurred in G2 (8.89 MPa). For groups without adhesive and with thermocycling, a higher number of completely adhesive failures between composite and enamel were present. For groups in which dental adhesive was used, regardless thermocycling, the failures were mainly adhesive between composite and the bracket. <strong>Conclusion</strong>: Surface etching of enamel with 35% phosphoric acid with or without adhesive showed a positive effect on SBS. The application of adhesive on enamel surface contributed to the maintenance of SBS values after thermocycling.</p><p> </p><p><strong>Keywords</strong></p><p>Aging; Orthodontic brackets; Composite resins; Shear strength.</p>


2014 ◽  
Vol 39 (3) ◽  
pp. 273-282 ◽  
Author(s):  
X Wen ◽  
L Zhang ◽  
R Liu ◽  
M Deng ◽  
Y Wang ◽  
...  

SUMMARY This study aims to evaluate the effects of pulsed Nd:YAG laser on the tensile bond strength (TBS) of resin to human enamel and caries resistance of human enamel. A total of 201 human premolars were used in this in vitro study. A flat enamel surface greater than 4 × 4 mm in area was prepared on each specimen using a low-speed cutting machine under a water coolant. Twenty-one specimens were divided into seven groups for morphology observations with no treatment, 35% phosphoric acid etching (30 seconds), and laser irradiation (30 seconds) of pulsed Nd:YAG laser with five different laser-parameter combinations. Another 100 specimens were used for TBS testing. They were embedded in self-cured acrylic resin and randomly divided into 10 groups. After enamel surface pretreatments according to the group design, resin was applied. The TBS values were tested using a universal testing machine. The other 80 specimens were randomly divided into eight groups for acid resistance evaluation. Scanning electron microscope (SEM) results showed that the enamel surfaces treated with 1.5 W/20 Hz and 2.0 W/20 Hz showed more etching-like appearance than those with other laser-parameter combinations. The laser-parameter combinations of 1.5 W/15 Hz and 1.5 W/20 Hz were found to be efficient for the TBS test. The mean TBS value of 14.45 ± 1.67 MPa in the laser irradiated group was significantly higher than that in the untreated group (3.48 ± 0.35 MPa) but lower than that in the 35% phosphoric acid group (21.50 ± 3.02 MPa). The highest mean TBS value of 26.64 ± 5.22 MPa was identified in the combination group (laser irradiation and then acid etching). Acid resistance evaluation showed that the pulsed Nd:YAG laser was efficient in preventing enamel demineralization. The SEM results of the fractured enamel surfaces, resin/enamel interfaces, and demineralization depths were consistent with those of the TBS test and the acid resistance evaluation. Pulsed Nd:YAG laser as an enamel surface pretreatment method presents a potential clinical application, especially for the caries-susceptible population or individuals with recently bleached teeth.


2017 ◽  
Vol 19 (4) ◽  
pp. 1-6
Author(s):  
Meghna Singh ◽  
Neerja Singh ◽  
Ashish Saini ◽  
Pranav Singh ◽  
Tanu Tewari ◽  
...  

2013 ◽  
Vol 14 (1) ◽  
pp. 21-25 ◽  
Author(s):  
T Praveen Kumar Reddy ◽  
Kolasani Srinivasa Rao ◽  
Garlapati Yugandhar ◽  
B Sunil Kumar ◽  
SN Chandrasekhar Reddy ◽  
...  

ABSTRACT The acid pretreatment and use of composite resins as the bonding medium has disadvantages like scratching and loss of surface enamel, decalcification, etc. To overcome disadvantages of composite resins, glass ionomers and its modifications are being used for bonding. The study was conducted to evaluate the efficiency of resin reinforced glass ionomer as a direct bonding system with conventional glass ionomer cement and composite resin. The study showed that shear bond strength of composite resin has the higher value than both resin reinforced glass ionomer and conventional glass ionomer cement in both 1 and 24 hours duration and it increased from 1 to 24 hours in all groups. The shear bond strength of resin reinforced glass ionomer cement was higher than the conventional glass ionomer cement in both 1 and 24 hours duration. Conditioning with polyacrylic acid improved the bond strength of resin reinforced glass ionomer cement significantly but not statistically significant in the case of conventional glass ionomer cement. How to cite this article Rao KS, Reddy TPK, Yugandhar G, Kumar BS, Reddy SNC, Babu DA. Comparison of Shear Bond Strength of Resin Reinforced Chemical Cure Glass Ionomer, Conventional Chemical Cure Glass Ionomer and Chemical Cure Composite Resin in Direct Bonding Systems: An in vitro Study. J Contemp Dent Pract 2013;14(1):21-25.


2012 ◽  
Vol 19 (2) ◽  
pp. 102
Author(s):  
Endang Wahyuningtyas ◽  
Suparyono Saleh ◽  
Sri Budi Barunawati

Latar Belakang. Resin komposit merupakan bahan pilihan untuk reparasi Gigi Tiruan Cekat porcelain fused to metal (PFM) Karena estetis baik dan manipulasi mudah. Tujuan penelitian ini adalah mengetahui perbedaan kekuatan geser perlekatan resin komposit pada permukaan logam Gigi Tiruan Cekat dengan menggunakan resin komposit jenis packable dan jenis flowable. Metode penelitian. Subjek penelitian berupa logam NiCr (Noritake, Japan) berbentuk silinder dengan diameter 10 mm dan tinggi 3 mm. Penelitian dibagi menjadi dua kelompok, masing-masing terdiri dari 10 subjek. Kelompok pertama reparasi dengan resin komposit packable (Z250™ 3M ESPE, USA) dan kelompok kedua reparasi dengan resin komposit flowable (Dyad flow, Kerr, USA). Permukaan subjek dikasari dengan wheel diamond bur, dietsa dengan asam fosfat 37 % (Scotchbond™, 3M ESPE, USA) kemudian dicuci dan dikeringkan, selanjutnya diaplikasikan silan (Rely X™ Ceramic Primer, 3M ESPE, USA) dan bonding (Adper™ Single Bond, 3M ESPE, USA). Permukaan kemudian dilapisi dengan resin komposit packable dan flowable, disinari selama 40 detik. Subjek penelitian direndam di dalam distilled water dan dimasukkan ke dalam incubator dengan suhu 37°C selama 7 hari. Uji kekuatan geser dilakukan dengan menggunakan Universal Testing Machine. Data dianalisis dengan uji t. hasil uji t menunjukkan terdapat perbedaan bermakna kekuatan geser reparasi gigi tiruan cekat pada permukaan logam (p<0,05). Kesimpulan penelitian ini adalah kekuatan geser reparasi pada permukaan logam dengan menggunakan resin komposit flowable yang mengandung bahan coupling agent lebih tinggi dibandingkan reparasi pada permukaan porselen dengan menggunakan resin komposit packable. Background. One of selected material by repairing the fixed partial denture was composite resin because of its good aesthetics and low manipulation. The aim. This research was aimed at identifying the differences of shear bond strength of composite resin on metal surface by using different composite resins, namely packable and flowable composite resins. Method. The research subjects were cylinders with 10 mm in diameter and 3 mm in height. The research subjects with metal material of NiCr (Noritke, Japan) involved two groups. The first group comprising 10 repair subjects with composite packable (Z250™, 3M ESPE, USA) and 10 repair subjects with flowable composite (Dyad flow, Kerr, USA). The surface of the subjects were roughned with wheel diamond bur and etched with 37% phosphate acid (Scotbond™, 3M ESPE, USA) were applied. The surface was then coated with packable and flowable composite resins and light-cured for 40 seconds. The research subjects were immersed in distilled water and put into the incubator at temperature of 37°C for 7 days. The shear bond strength test was conducted using the Universal Testing Machine. Data were analyzed using t-test. The result. The research result showed that there were differences of shear bond strength of repair between packable and flowable composite resins. The result of t-test indicated significant diffrences on metal surface (p<0,05). The conclusion of this research is that shear bond strength of repair with flowable composite which contain coupling agent has higher shear bond strength than that of packable composite resin.


2010 ◽  
Vol 35 (2) ◽  
pp. 187-193 ◽  
Author(s):  
M. Khoroushi ◽  
M. Tavasoli

Clinical Relevance TCA gel etches enamel surfaces and produces surface morphological characteristics and bond strength similar to that produced by phosphoric acid. When TCA is used as a hemostatic agent on marginal gingiva, its inadvertent contact with enamel improves the immediate bond strength of resin composite to enamel. However, when using phosphoric acid and 50% TCA, an erosive enamel surface is produced.


2015 ◽  
Vol 40 (3) ◽  
pp. E112-E121 ◽  
Author(s):  
HA St Germain ◽  
TH St Germain

SUMMARY In this laboratory research, shear bond strength (SBS) and mode of failure of veneers rebonded to enamel in shear compression were determined. Three groups (A, B, and C; n=10 each) of mounted molar teeth were finished flat using wet 600-grit silicon carbide paper, and 30 leucite-reinforced porcelain veneers (5.0 × 0.75 mm) were air abraded on the internal surface with 50 μm aluminum oxide, etched with 9.5% hydrofluoric acid, and silanated. The control group (A) veneer specimens were bonded to enamel after etching with 37% phosphoric acid using bonding resin and a dual cure resin composite cement. Groups B and C were prepared similarly to group A with the exception that a release agent was placed before the veneer was positioned on the prepared enamel surface and the resin cement was subsequently light activated. The debonded veneers from groups B and C were placed in a casting burnout oven and heated to 454°C/850°F for 10 minutes to completely carbonize the resin cement and stay below the glass transition temperature (Tg) of the leucite-reinforced porcelain. The recovered veneers were then prepared for bonding. The previously bonded enamel surfaces in group B were air abraded using 50 μm aluminum oxide followed by 37% phosphoric acid etching, while group C enamel specimens were acid etched only. All specimens were thermocycled between 5°C and 55°C for 2000 cycles using a 30-second dwell time and stored in 37°C deionized water for 2 weeks. SBS was determined at a crosshead speed of 1.0 mm/min. SBS results in MPa for the groups were (A) = 20.6±5.1, (B) = 18.1±5.5, and (C) = 17.2±6.1. One-way analysis of variance indicated that there were no significant interactions (α=0.05), and Tukey-Kramer post hoc comparisons (α=0.05) detected no significant pairwise differences. An adhesive mode of failure at the enamel interface was observed to occur more often in the experimental groups (B = 40%, C = 50%). Rebonding the veneers produced SBS values that were not significantly different from the control group. Also, no significant difference in SBS values were observed whether the debonded enamel surface was air abraded and acid etched or acid etched only.


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