Simulation of Miscible Displacement in Full-Diameter Carbonate Cores

1982 ◽  
Vol 22 (05) ◽  
pp. 647-657 ◽  
Author(s):  
J.P. Batycky ◽  
B.B. Maini ◽  
D.B. Fisher

Abstract Miscible gas displacement data obtained from full-diameter carbonate reservoir cores have been fitted to a modified miscible flow dispersion-capacitance model. Starting with earlier approaches, we have synthesized an algorithm that provides rapid and accurate determination of the three parameters included in the model: the dispersion coefficient, the flowing fraction of displaceable volume, and the rate constant for mass transfer between flowing and stagnant volumes. Quality of fit is verified with a finite-difference simulation. The dependencies of the three parameters have been evaluated as functions of the displacement velocity and of the water saturation within four carbonate cores composed of various amounts of matrix, vug, and fracture porosity. Numerical simulation of a composite core made by stacking three of the individual cores has been compared with the experimental data. For comparison, an analysis of Berea sandstone gas displacement also has been provided. Although the sandstone displays a minor dependence of gas recovery on water saturation, we found that the carbonate cores are strongly affected by water content. Such behavior would not be measurable if small carbonate samples that can reflect only matrix properties were used. This study therefore represents a significant assessment of the dispersion-capacitance model for carbonate cores and its ability to reflect changes in pore interconnectivity that accompany water saturation alteration. Introduction Miscible displacement processes are used widely in various aspects of oil recovery. A solvent slug injected into a reservoir can be used to displace miscibly either oil or gas. The necessary slug size is determined by the rate at which deterioration can occur as the slug is Another commonly used miscible process involves addition of a small slug within the injected fluids or gases to determine the nature and extent of inter well communication. The quantity of tracer material used is dictated by analytical detection capabilities and by an understanding of the miscible displacement properties of the reservoir. We can develop such understanding by performing one-dimensional (1D) step-change miscible displacement experiments within the laboratory with selected reservoir core material. The effluent profiles derived from the experiments then are fitted to a suitable mathematical model to express the behavior of each rock type through the use of a relatively small number of parameters. This paper illustrates the efficient application of the three-parameter, dispersion-capacitance model. Its application previously has been limited to use with small homogeneous plugs normally composed of intergranular and intencrystalline porosity, and its suitability for use with cores displaying macroscopic heterogeneity has been questioned. Consequently, in addition to illustrating its use with a homogeneous sandstone, we fit data derived from previously reported full-diameter carbonate cores. As noted earlier, these cores were heterogeneous, and each of them displayed different dual or multiple types of porosity characteristic of vugular and fractured carbonate rocks. Dispersion-Capacitance Model The displacement efficiency of one fluid by a second immiscible fluid within a porous medium depends on the complexity of rock and fluid properties. SPEJ P. 647^

2021 ◽  
Author(s):  
Nicolas Gaillard ◽  
Matthieu Olivaud ◽  
Alain Zaitoun ◽  
Mahmoud Ould-Metidji ◽  
Guillaume Dupuis ◽  
...  

Abstract Polymer flooding is one of the most mature EOR technology applied successfully in a broad range of reservoir conditions. The last developments made in polymer chemistries allowed pushing the boundaries of applicability towards higher temperature and salinity carbonate reservoirs. Specifically designed sulfonated acrylamide-based copolymers (SPAM) have been proven to be stable for more than one year at 120°C and are the best candidates to comply with Middle East carbonate reservoir conditions. Numerous studies have shown good injectivity and propagation properties of SPAM in carbonate cores with permeabilities ranging from 70 to 150 mD in presence of oil. This study aims at providing new insights on the propagation of SPAM in carbonate reservoir cores having permeabilities ranging between 10 and 40 mD. Polymer screening was performed in the conditions of ADNOC onshore carbonate reservoir using a 260 g/L TDS synthetic formation brine together with oil and core material from the reservoir. All the experiments were performed at residual oil saturation (Sor). The experimental approach aimed at reproducing the transport of the polymer entering the reservoir from the sand face up to a certain depth. Three reservoir coreflood experiments were performed in series at increasing temperatures and decreasing rates to mimic the progression of the polymer in the reservoir with a radial velocity profile. A polymer solution at 2000 ppm was injected in the first core at 100 mL/h and 40°C. Effluents were collected and injected in the second core at 20 mL/h and 70°C. Effluents were collected again and injected in the third core at 4 mL/h and 120°C. A further innovative approach using reservoir minicores (6 mm length disks) was also implemented to screen the impact of different parameters such as Sor, molecular weight and prefiltration step on the injectivity of the polymer solutions. According to minicores data, shearing of the polymer should help to ensure good propagation and avoid pressure build-up at the core inlet. This result was confirmed through an injection in a larger core at Sor and at 120°C. When comparing the injection of sheared and unsheared polymer at the same concentration, core inlet impairment was suppressed with the sheared polymer and the same range of mobility reduction (Rm) was achieved in the internal section of the core although viscosity was lower for the sheared polymer. Such result indicates that shearing is an efficient way to improve injectivity while maximizing the mobility reduction by suppressing the loss of product by filtration/retention at the core inlet. This paper gives new insights concerning SPAM rheology in low permeability carbonate cores. Additionally, it provides an innovative and easier approach for screening polymer solutions to anticipate their propagation in more advanced coreflooding experiments.


2021 ◽  
Author(s):  
Yuri Mikhailovich Trushin ◽  
Anton Sergeevich Aleshchenko ◽  
Oleg Nikolaevich Zoshchenko ◽  
Mark Suleimanovich Arsamakov ◽  
Ivan Vasilevich Tkachev ◽  
...  

Abstract The paper considers the use of a surfactant-polymer composition for the mobilization of light paraffinic oil from the D3-III carbonate reservoir at a reservoir temperature of 62°C, as well as the results of its tests in field conditions. Earlier, the composition showed its effectiveness on model carbonate cores with salinity from current (50-80 g/l) to reservoir (up to 170 g/l), in the presence of surfactants, type III microemulsions according to Winsor with oil were obtained. Based on the results of the filtration experiments performed on our own core from the productive formation D3-III, an increase in the displacement efficiency of surfactant-polymer compositions compared to water was obtained 11–14% (with a total surfactant concentration of 1%), irreversible surfactant losses in water-saturated rock–up to 0, 38 mg/g. Displacement efficiency after water and surfactant-polymer composition flooding was also estimated in the field conditions using SWCTT; its results were interpreted by various methods (analytical, in a hydrodynamic simulator), and also compared with laboratory results. Within a single-well tracer test, an assessment of the residual saturation after water filtration and injection of a surfactant-polymer composition was carried out under the following conditions: the target research radius is 3.5 m; porosity 10%, effective reservoir thickness 38 m. Based on the results of SWCTT, an increase in the displacement efficiency of 16.7% was obtained in comparison with water displacement (total surfactant concentration 1%) using an analytical method of interpretation. The adaptation of the SWCTT results on the hydrodynamic model was carried out, the most influencing parameters on the quality of adaptation were determined. The selection and justification of a pilot area for a multi-well pilot project was carried out, a sector hydrodynamic model of the site was built, and calculations were made to assess additional oil production.


2017 ◽  
Vol 140 (5) ◽  
Author(s):  
Wu Zhengbin ◽  
Liu Huiqing ◽  
Wang Xue

Thermal–chemical flooding (TCF) is an effective alternative to enhance heavy oil recovery after steam injection. In this paper, single and parallel sand-pack flooding experiments were carried out to investigate the oil displacement ability of thermal–chemical composed of steam, nitrogen (N2), and viscosity breaker (VB), considering multiple factors such as residual oil saturation (Sorw) postwater flood, scheme switch time, and permeability contrast. The results of single sand-pack experiments indicated that compared with steam flooding (SF), steam-nitrogen flooding, and steam-VB flooding, TCF had the best displacement efficiency, which was 11.7% higher than that of pure SF. The more serious of water-flooded degree, the poorer of TCF effect. The improvement effect of TCF almost lost as water saturation reached 80%. Moreover, the earlier TCF was transferred from steam injection, the higher oil recovery was obtained. The parallel sand-pack experiments suggested that TCF had good adaptability to reservoir heterogeneity. Emulsions generated after thermal–chemical injection diverted the following compound fluid turning to the low-permeable tube (LPT) due to its capturing and blocking ability. The expansion of N2 and the disturbance of VB promoted oil recovery in both tubes. As reservoir heterogeneity became more serious, namely, permeability contrast was more than 6 in this study, the improvement effect became weaker due to earlier steam channeling in the high-permeable tube (HPT).


2017 ◽  
Vol 11 (12) ◽  
pp. 58
Author(s):  
Wicaksono Wicaksono ◽  
Pudji Permadi ◽  
Utjok W.R. Siagian ◽  
Tjokorde Walmiki Samadhi

Carbon dioxide (CO2) injection is the most promising technique to enhance the recovery of high gravity oil with the existing oil price situation. Even though, challenges still exist for thick and heterogeneous reservoirs at very high temperature. The problems faced in such reservoirs are low displacement efficiency and very high injection pressure requirement for a miscible displacement. The effort being done by researchers to overcome the situations is the use of silica nanoparticle as an agent to form CO2-silica nanoparticle foam. Currently, the related literature shows that CO2 miscible displacement is rarely performed at very high temperature and consequently no relevant effort has been made to investigate the stability of CO2-silica nanoparticle foam, while there are many oil reservoirs with temperature of higher than 250 oF. Therefore, related studies on such situations are needed. The present work consists of two stages. First, slimtube and coreflood experiments of CO2 injection are conducted at about 270 oF, respectively, to both determine the Minimum Miscibility Pressure (MMP) of the selected live oil system and the oil recovery. Secondly, CO2-silica nanoparticle foam stability in various brine salinity at such high temperature will be investigated and effectiveness of the selected stable foam will be tested through an oil displacement using native cores.In this paper, the results of both slimtube and coreflood experiments are first presented. A live paraffinic oil with 34 oAPI is used. The standard slimtube apparatus is employed. Stacked core composing of three native core plugs of different permeability ranging from 75 to 503 milidarcies are used to represent rock heterogeneity. At a temperature of 270 oF, MMP of the oil obtained from the slimtube experiment is 2960 psi, about 100 psi higher than that obtained from the coreflood experiment. The slimtube test gives oil recovery 94.2% and the coreflood as expected yields lower recovery, 84% of the initial oil in place. The importance of the tests is two folds that the MMP of the oil system is firmly known while the existing empirical correlations estimate the values ranging from 2718 to 5578 psi and a relatively low coreflood oil recovery suggests further investigation of stability of CO2-silica nanoparticle foam at that temperature in an attempt for enhancing the oil recovery. 


2014 ◽  
Vol 18 (01) ◽  
pp. 39-52 ◽  
Author(s):  
Yousef Hamedi Shokrlu ◽  
Tayfun Babadagli

Summary Flow of three phases, of which one is miscible with another, in porous media may commonly be encountered during enhanced-oil-recovery (EOR) applications in oil reservoirs. Typical examples include solvent (miscible-gas) injection alternated with water and coinjection or alternate injection of steam (or hot water) and solvent in heavy-oil/bitumen reservoirs. Oil, water, and solvent flow together under immiscible (water/oil and water/solvent) and miscible (oil/solvent) conditions at the same time, and the distribution of phases and removal of residual oil in those types of processes depend on many parameters. This paper reports microscale experimental investigations on this complex flow process and provides an extensive parametric analysis on the microscopic displacement efficiency of oil recovery using miscible solvent. For this purpose, micromodels created by use of a replica of sandstones were used. Waterflood residual-oil displacement requires contact of the injected solvent with the blocked oil. The efficiency of this process depends on several parameters, including matrix wettability, oil viscosity, initial water saturation, and reservoir heterogeneity. On the other hand, the sequence of injection of solvent and water is considered as another parameter by which oil recovery can be affected significantly. The results of the micromodel-visualization experiments showed that injection of solvent before the introduction of any water to the reservoir can increase the recovery factor significantly. Existence of the water phase in the reservoir creates capillary barriers that prevent oil/solvent contact. The matrix wettability and oil viscosity were observed to be critically important to the amount of oil recovery.


SPE Journal ◽  
2018 ◽  
Vol 24 (01) ◽  
pp. 129-139 ◽  
Author(s):  
J. L. Juárez-Morejón ◽  
H.. Bertin ◽  
A.. Omari ◽  
G.. Hamon ◽  
C.. Cottin ◽  
...  

Summary An experimental study of polymer flooding is presented here, focusing on the influence of initial core wettability and flood maturity (volume of water injected before polymer injection) on final oil recovery. Experiments were performed using homogeneous Bentheimer Sandstone samples of similar properties. The cores were oilflooded using mineral oil for water-wet conditions and crude oil (after an aging period) for intermediate-wet conditions; the viscosity ratio between oil and polymer was kept constant in all experiments. Polymer, which is a partially hydrolyzed polyacrylamide (HPAM), was used at a concentration of 2,500 ppm in a moderate-salinity brine. The polymer solution was injected in the core at different waterflood-maturity times [breakthrough (BT) and 0, 1, 1.75, 2.5, 4, and 6.5 pore volumes (PV)]. Coreflood results show that the maturity of polymer injection plays an important role in final oil recovery, regardless of wettability. The waterflood-maturity time 0 PV (polymer injection without initial waterflooding) leads to the best sweep efficiency, whereas final oil production decreases when the polymer-flood maturity is high (late polymer injection after waterflooding). A difference of 15% in recovery is observed between early polymer flooding (0 PV) and late maturity (6.5 PV). Concerning the effect of wettability, the recovery factor obtained with water-wet cores is always lower (from 10 to 20%, depending on maturity) than the values obtained with intermediate-wet cores, raising the importance of correctly restoring core wettability to obtain representative values of polymer incremental recovery. The influence of wettability can be explained by the oil-phase distribution at the pore scale. Considering that the waterflooding period leads to different values of the oil saturation at which polymer flooding starts, we measured the core dispersivity using a tracer method at different states. The two-phase dispersivity decreases when water saturation increases, which is favorable for polymer sweep. This study shows that in addition to wettability, the maturity of polymer flooding plays a dominant role in oil-displacement efficiency. Final recovery is correlated to the dispersion value at which polymer flooding starts. The highest oil recovery is obtained when the polymer is injected early.


2021 ◽  
Vol 36 (3) ◽  
pp. 143-156
Author(s):  
Yousef Shiri ◽  
Alireza Shiri

Quadrant geometry with permeability and wettability contrast occurs in different events, such as faults, wellbore damage, and perforation zones. In these events, understanding the dynamics of immiscible fluid displacement is vital for enhanced oil recovery. Fluid flow studies showed that viscous fingering occurs due to viscous instabilities that depend on the mobility of fluids and capillary forces. Besides, the porous domain heterogeneity is also effective on the formation of fingering. So, the purpose of the current research is to numerically investigate the effect of heterogeneity in wettability and permeability, and flow properties in Saffmann-Taylor instabilities. Numerical simulations with different flow rates in the permeability contrast model illustrated the nodal crossflow, growth of viscous fingering in the nodal part, and bypass flow in the second zone. In the wettability contrast model, a capillary fingering pattern is observed and fluid patches are isolated because of capillary force and the end effects are trapped within the quadrant. Moreover, the consequences of wettability on apparent wettability that alters the fluid-front pattern and displacement efficiency are shown.


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