scholarly journals Research on the drying Mechanism of Astragali Radix during Processing

Author(s):  
Jie Peng ◽  
Meng-Mei Wu ◽  
Li-Fang Ye ◽  
Meng-Hua Wu ◽  
Zhi-Guo Ma ◽  
...  

Abstract Backgroundstragali Radix (Huangqi) is an important Chinese herbal medicine that is always processed into pieces for clinical use. There are many operations required after harvesting, among which drying of AR pieces is a key step. Unfortunately, research on the drying mechanism is still limited.MethodsLow-field nuclear magnetic resonance (LF-NMR) and magnetic resonance imaging (MRI) techniques were applied to study the water status and water distribution during the drying process. The contents of bioactive ingredients and texture changes were measured by HPLC and texture analyzer, respectively.ResultsDuring the drying process, the moisture content first decreased rapidly. After a particular time, the moisture content decreased slowly, and the equilibrium value was reached. The trends for changes in flavonoid glycoside and flavonoid aglycone contents in AR pieces were entirely opposite. The relaxation times T22 and T23 and the peak areas A22 and ATotal decreased significantly during drying. In addition, the intensity of the water signal decreased from the surface to the interior. The textural parameters hardness, adhesion and fracturability increased without an apparent change in springiness. The parameters of LF-NMR and the texture analyzer were correlated with water content.ConclusionsThis study indicated that HPLC, LF-NMR, MRI and texture analyzers provide a scientific basis for elucidating the principles for drying of AR pieces. The method is useful and shows potential for popularization and application; accordingly, it can easily be extended to other radix and/or rhizoma Traditional Chinese Medicinal materials.

Molecules ◽  
2019 ◽  
Vol 24 (2) ◽  
pp. 236 ◽  
Author(s):  
Yannan Chen ◽  
Hongjing Dong ◽  
Jingkun Li ◽  
Lanping Guo ◽  
Xiao Wang

Gastrodia elata Blume (G. elata) is a prominent traditional herb and its dry tuber is officially listed in the Chinese Pharmacopoeia. To ensure the quality of dried G. elata, the establishment of a nondestructive and convenient method to monitor the drying process is necessary. In this study, a nondestructive low-field nuclear magnetic resonance (LF-NMR) and magnetic resonance imaging (MRI) method was introduced to monitor the drying process of G. elata. Three water states (bound, immobilized, and free) in G. elata samples were investigated through multiexponential fitting and inversion of the NMR data. The variation and distribution of the three water states during drying were monitored by LF-NMR, and the spatial distribution of water and internal structural changes were analyzed by MRI. Linear analysis of the moisture content, L* (lightness), b* (yellowness), and NMR parameters showed good correlations among them. Furthermore, partial least squares regression (PLSR) model analysis, which takes into account all NMR parameters, also showed good correlations among these parameters. All results showed that LF-NMR was feasible and convenient for monitoring moisture content. Therefore, LF-NMR and MRI could be used to monitor the moisture content nondestructively in the drying process of Chinese traditional herbs.


2000 ◽  
Vol 3 (06) ◽  
pp. 498-508 ◽  
Author(s):  
Songhua Chen ◽  
D.T. Georgi ◽  
Oscar Olima ◽  
Hector Gamin ◽  
J.C. Minetto

Summary We report a case study of using nuclear magnetic resonance (NMR) multiple-te, dual wait-time (tw) log acquisitions for quantitative characterization of San Jorge Basin reservoir oil viscosity. Previously, dual-tw logs have been used to discern gas and oil from water, while dual-te logs have been used as a qualitative light oil indicator. Although theoretically simple, quantitative determination of viscosity from dual-te logs is complicated by several factors, including poor signal-to-noise ratio, difficulties in separating oil from water, and the uncertainty of internal gradient strength. In the present study, multiple-te acquisitions of dual-tq logs were used to isolate the oil from the water signal. The values of viscosity of the reservoir fluids can be estimated from either intrinsic T2 or T1. In estimation of the apparent T2, we used a model that does not explicitly require knowledge of the internal gradient, thereby minimizing the effects arising from the uncertainty of the internal and tool gradient strengths. Because T1 and intrinsic T2 are estimated independently, the degree of agreement between the two values provides an indication of the reliability of the two estimates. The main example in the study of four pay zones was thought to contain viscous oil. However, our analysis indicated that the viscosity values of the oil are less than 5 cP. The predictions have been substantiated by production of light hydrocarbons from the three zones that have been perforated. Further, a good agreement is obtained for the viscosity estimates based on NMR log data and laboratory pressure/volume/temperature (PVT) analysis. Introduction Hydrocarbon viscosity is an important reservoir fluid parameter that significantly affects oil recovery and economics. Fluid flow is inversely proportional to viscosity and the higher the viscosity the lower the flow rate and the slower the recovery. Further, when two or more fluids are flowing, the ratio of the viscosities, the mobility ratio, is one of the key parameters that affects sweep efficiency and ultimate recovery. In many reservoirs, it is uneconomical to produce heavy, viscous oil, and thus it is crucial to determine oil viscosity before completing the well. The problem is even more pressing when oil viscosities vary within a hydrocarbon column or from zone to zone when attempting to commingle multiple zones. Many laboratory procedures can determine viscosity. Samples for viscosity determination may be obtained from reservoir fluid samples recovered from well tests or drill stem tests, downhole fluid samplers, or reconstituted from separator samples. Sampling procedures are generally limited to a few depths; and, of course, samples reconstituted from separators are associated with the entire producing interval and may not be associated with a single depth. Further, there is always the concern that the fluid samples may not be representative of the in-situ reservoir fluids. Nuclear magnetic resonance (NMR) logging measurements have the potential to provide in-situ viscosity measurement because the NMR relaxation times, T1 and T2, correlate strongly with fluid viscosity. The difficulty with NMR-determined viscosity is that the measurement is relatively shallow. Thus, the hydrocarbon saturations may be significantly reduced (So or Sor), and hence, the sought NMR oil signal is small. Further, the interpretation may be complicated by NMR signals originating from the invading fluids. NMR response is controlled by both rock and fluid properties. In fact, NMR log interpretation is complicated because it is not always clear whether the T2 decay reflects hydrocarbon and/or rock properties. However, we are fortunate because two NMR experiment parameters, te and tw (Fig. 1), can be used to tailor the NMR data acquisition to separate the hydrocarbon and rock property effects. One of the first specialized NMR applications that took advantage of the ability to control NMR log acquisition parameters was hydrocarbon typing.1 NMR hydrocarbon typing in porous media relies on the difference in NMR response in either or both of the relaxation times (T1 and T2) or diffusivity of oil, water, and gas. By carefully designing the logging program and using combinations of pulse sequences, one can enhance the relaxation and diffusivity contrasts between the different fluid phases. The two commonly used approaches for magnetic resonance image log (MRIL®)** based hydrocarbon typing are dual-tq logging1,2 and dual-te logging.3,4 Dual-tw logging utilizes the T1 contrast between nonwetting light hydrocarbons and the wetting water for quantitative light hydrocarbon typing, while dual-te logging utilizes the viscosity (and thus diffusivity) contrast between reservoir fluids. The latter, to our knowledge, previously has been used mainly as a qualitative, or, at best semiquantitative, hydrocarbon indicator. Quantitative estimation of oil viscosity and saturation require solving problems related to uncertainty of internal magnetic-field gradient and separating oil from water signals. We combined the dual-tw and dual-te approaches to maximize the advantages of both T1 and T2 contrasts. With multiple-te passes of dual-tw logs, we are able to eliminate a majority of the water signal from dual-tw logs; the remaining signal is predominantly an oil signal. The characterization of oil viscosity is achieved by analyzing the relaxation times and diffusion effect on the isolated oil signal with the multiple-te data acquisition. This reduces uncertainties due to the interfering water signal originating from either the irreducible and bound water or from the invading mud filtrate present on conventional dual-te logs.


HortScience ◽  
1995 ◽  
Vol 30 (4) ◽  
pp. 898D-898 ◽  
Author(s):  
Anne Fennell ◽  
M.J. Line ◽  
M. Faust

Changes in water status have been associated with various stages of dormancy and freezing tolerance in woody perennials. Recent studies in apple indicate that changes in the state (bound vs. free) of bud water are strongly correlated with the end of dormancy. In this study nuclear magnetic resonance imaging (NMRI) was used to monitor changes in the state of bud water during the photoperiodic induction of endo-dormancy in Vitis riparia. Bud water status was monitored using proton relaxation times from T1 and T2 images determined at 2, 4, and 6 weeks of long (LD) or short (SD) photoperiod treatments. Bud dormancy was determined by monitoring budbreak in plants defoliated after photoperiod treatments. NMRI allowed nondestructive monitoring of changes in tissue water state. T1 and T2 maps indicated changes in the state of the water in bud and stem tissues during the 6 weeks of treatment. Differences in relaxation times for nondormant and dormancy-induced (reversible) buds were not clear. However, T2 relaxation times were lower in the dormant buds than in the nondormant buds.


Geophysics ◽  
2016 ◽  
Vol 81 (6) ◽  
pp. EN87-EN97 ◽  
Author(s):  
Emily L. Fay ◽  
Rosemary J. Knight

We have conducted proton nuclear magnetic resonance (NMR) measurements of relaxation times [Formula: see text] and [Formula: see text] as well as the diffusion coefficient [Formula: see text] to detect and quantify gasoline, diesel, crude oil, and trichloroethylene (TCE) in sediment samples containing water. The sediment samples were coarse sand, fine sand, and a sand-clay mixture. We found that water, gasoline, diesel, and crude oil all exhibited similar signal amplitudes per unit volume, whereas TCE exhibited one-tenth the signal. The ability to use [Formula: see text] measurements to distinguish the contaminant signal from the water signal depended on the bulk-fluid properties as well as the sediment texture and grain size. In the [Formula: see text] distributions for samples containing equal volumes of contaminant and water, the contaminant signal could be resolved for crude oil in sand and for gasoline and TCE in the sand-clay mixture. Adding the diffusion measurement, using either pulsed or static gradients, made it possible to distinguish diesel and crude oil in all of the samples due to the large differences between the [Formula: see text] of the contaminants and water. From the diffusion measurements, we were able to accurately quantify diesel and crude oil volumes ranging from 1% to 17% of the total sample volume. These methods could be applied in the field using NMR logging tools to quantify and monitor subsurface contamination.


2018 ◽  
Vol 13 (4) ◽  
pp. 477
Author(s):  
Rudney Amaral ◽  
Ednilton Tavares Andrade ◽  
Francisco Carlos Gomes ◽  
Flávio Meira Borém ◽  
Isabella Lemos ◽  
...  

<p>Drying is a fundamental step in post-harvest handling of coffee because moisture content at the end of drying affects several important aspects, such as sensory quality, storability, and color. Within this context, the aim of this study is to determine water distribution within the natural coffee fruit during and at the end of the drying process. For that purpose, simulations were made through finite elements using computational fluid dynamics. Experimental data on moisture content of coffee fruitin the “cherry” stage were collected during drying, which was carried out at a temperature of 40°C and relative humidity of 25% to 0.18 decimal(dry basis – d.b.)to compare the results of the experiment with the results of the simulations. Ten mathematical models of the drying process were developed for the collected data. The two-term exponential model best fit the data. The results of the simulations in computational fluid dynamics were compared to the results from experimental drying, and a satisfactory fit was obtained. The effective diffusivity coefficient (D<sub>eff</sub>) was developed for the model, obtaining the value of 2.87 x 10<sup>‑11</sup> m<sup>2</sup> s<sup>-1</sup>. At the end of drying, the model exhibited 57.1% of the projection area of the coffee fruit with moisture content below 0.18 decimal (d.b.). Thus, the model can be used for other applications.</p>


2019 ◽  
Vol 2019 ◽  
pp. 1-7 ◽  
Author(s):  
Shengmei Gai ◽  
Zhonghui Zhang ◽  
Yufeng Zou ◽  
Dengyong Liu

This study investigated the effects of hydrocolloid injection on the eating quality of porcine meat based on low-field nuclear magnetic resonance (LF-NMR). The eating quality and water distribution of hydrocolloid-injected pork were compared with control, and the principle component analysis (PCA) was applied for the identification of hydrocolloid-injected pork. Total color difference (ΔE∗), cooking loss, and moisture content of hydrocolloid-injected pork were significantly increased compared with the control (p<0.05). LF-NMR indicated that significant differences in the relaxation time and peak area proportion of immobilized water (T21, P21) and free water (T22, P22) were detected among hydrocolloid-injected samples and the control (p<0.05). The first two principal components (PCs) of PCA accounted for 54.07% and 33.56% of the observed variation, respectively. Based on the two PCs, the hydrocolloid-injected pork could be differentiated from the control. Therefore, LF-NMR combined with PCA offers an effective method for the analysis and detection of hydrocolloid-injected pork.


2011 ◽  
Vol 704-705 ◽  
pp. 446-449
Author(s):  
Xiang Jun Wang ◽  
Ming Hui Zhang ◽  
Xi Ming Wang

the moisture distribution in untreated and esterified poplar with Maleic anhydride was studied in the present paper employed nuclear magnetic resonance (NMR). The results show that relaxation times decrease with the the fall of moisture content, and there is a linear equation between the moisture content and transverse relaxation time in esterified wood. The content of bonding water and free water in the esterified wood decreased simultaneously during the drying.


Author(s):  
Xiu Zang ◽  
Yinxue Zu ◽  
Tan Zhang ◽  
Kexin Xia ◽  
Yukun Song ◽  
...  

AbstractThe purpose of this study is to elucidate the water dynamics in sea cucumber (Stichopus japonicas) during drying processin situby the fast and non-destructive low field nuclear magnetic resonance (LF-NMR) and magnetic resonance imaging (MRI) methods.T2relaxation spectra in three-dimensional (3D) color map surface image from LF-NMR showed three main peaks assigned to bound water with relaxation time less than 2 ms, immobilized water in the range of 15–150 ms and extra-collagen fibrillar bulk water or free water adhered onto the sea cucumber with the longest relaxation time 200–1600 ms. The water dynamics in sea cucumber during drying process was clearly observed from the 3D color map surface image. Significant correlations between the LF-NMRT2parameters (ATotal, A23andT23) and TPA parameters were observed, demonstrating that LF-NMR might be a complementary technique in monitoring the textural properties of sea cucumber during drying process.


Author(s):  
M.J. Hennessy ◽  
E. Kwok

Much progress in nuclear magnetic resonance microscope has been made in the last few years as a result of improved instrumentation and techniques being made available through basic research in magnetic resonance imaging (MRI) technologies for medicine. Nuclear magnetic resonance (NMR) was first observed in the hydrogen nucleus in water by Bloch, Purcell and Pound over 40 years ago. Today, in medicine, virtually all commercial MRI scans are made of water bound in tissue. This is also true for NMR microscopy, which has focussed mainly on biological applications. The reason water is the favored molecule for NMR is because water is,the most abundant molecule in biology. It is also the most NMR sensitive having the largest nuclear magnetic moment and having reasonable room temperature relaxation times (from 10 ms to 3 sec). The contrast seen in magnetic resonance images is due mostly to distribution of water relaxation times in sample which are extremely sensitive to the local environment.


2012 ◽  
Vol 2 (1) ◽  
pp. 14-20
Author(s):  
Yuwana Yuwana

Experiment on catfish drying employing ‘Teko Bersayap’ solar dryer was conducted. The result of the experiment indicated that the dryer was able to increase ambient temperature up to 44% and decrease ambient relative humidity up to 103%. Fish drying process followed equations : KAu = 74,94 e-0,03t for unsplitted fish and KAb = 79,25 e-0,09t for splitted fish, where KAu = moisture content of unsplitted fish (%), KAb = moisture content of splitted fish (%), t = drying time. Drying of unsplitted fish finished in 43.995 hours while drying of split fish completed in 15.29 hours. Splitting the fish increased 2,877 times drying rate.


Sign in / Sign up

Export Citation Format

Share Document