scholarly journals Numerical investigations on solute transport and freckle formation during directional solidification of nickle-based superalloy ingot

2021 ◽  
pp. 339-339
Author(s):  
Jiajun Cui ◽  
Baokuan Li ◽  
Zhongqiu Liu ◽  
Fengsheng Qi ◽  
Beijiang Zhang

In order to investigate the solute distribution and freckles formation during directional solidification of superalloy ingots, a mathematical model with coupled solution of flow field, solute and temperature distribution was developed. Meanwhile, the reliability of this model was verified by the experimental and simulation results in relevant literatures. The three-dimensional directional solidification process of Ni-5.8wt%Al-15.2wt%Ta superalloy ingot was simulated, and then the dynamic growth of solute enrichment channels was demonstrated inside the ingot. Freckles formation under different cooling rates was studied, and the local segregation degree inside the ingot was obtained innovatively after solidification. The results show that the number of freckles formed at the top gradually decreases, and so do the degree of solute enrichment at these freckles with the increase of cooling rate. Moreover, the relative and volume-averaged segregation ratio is defined to describe the segregation degree inside the ingot. The span of relative segregation ratio for positive segregation is wider than that for negative segregation, but it accounts for less of total volume. As the cooling rate increases from 0.1 K/s to 1.0 K/s, the proportion of weak segregation (-20%~20%) increases significantly from 26% to 41%, so that the segregation degree is weakened in general. By analyzing the freckles formation and segregation degree inside the ingot, the numerical simulation results can provide a theoretical basis for optimizing the actual production process to suppress the freckle defects.

2010 ◽  
Vol 145 ◽  
pp. 326-331 ◽  
Author(s):  
Shao Jun Zhang ◽  
Dong Mei Zhu ◽  
Guo Yong Liu

The three dimensional unsteady cooling process of flat steel is simulated by the numerical simulation calculation method of Finite Element Coupling Field. Then, the influential rules, which about layout parameters of the controlled cooling nozzle such as the distance and number of nozzle rows on the cooling effect, are analyzed separately. The results show that the distance of nozzle has a little effect on cooling rate. Relatively the number of nozzle rows affects cooling rate of flat steel greatly. Different layout parameters of the controlled cooling nozzle will be used by considering different factors. The numerical simulation results provide references for the layout of steel nozzle and controlled cooling device.


2015 ◽  
Vol 723 ◽  
pp. 561-564
Author(s):  
Zhi Hong Jia ◽  
Liang Xu ◽  
Ran Tao ◽  
Ming Zhe Ma ◽  
Dao Cun Xie ◽  
...  

A three-dimensional model of CMSX-6 superalloy coupons was built in the paper, temperature field was calculated with software ProCAST. The temperature values of coupons were indicated from the measurement at the rate of 3 mm min-1 withdrawal velocity during directional solidification process, and the temperature gradient of different location of the coupons were calculated. It turned out that: the simulated results and the measured results are in good agreement; due to the different medial and lateral affected by radiation, isotherms showed sloped distributions in the process of the withdrawal; the temperature gradient of the measured positions in the coupons which are 10 mm, 50 mm, 100 mm, 150 mm far from the copper chill, are 8.0 Kmm-1, 3.0 Kmm-1, 2.5 Kmm-1, 1.8 Kmm-1 respectively.


2016 ◽  
Vol 869 ◽  
pp. 452-457 ◽  
Author(s):  
André Santos Barros ◽  
Maria Adrina Paixão de Souza da Silva ◽  
Otávio Fernandes Lima da Rocha ◽  
Antonio Luciano Seabra Moreira

The main purpose of this paper is to evaluate both tertiary dendritic arm growth and microhardness of Al-3wt%Cu alloy during horizontal directional solidification under transient heat flow conditions. Experimental thermal profiles recorded during solidification process allowed to determine growth rate and cooling rate values which are associated with both tertiary dendritic arm spacings and microhardness. The results show that initial tertiary branches growth only occurs when a cooling rate value of 1.14 K/s is reached. Variation of tertiary spacings is expressed as-1.1 and-0.55 power law functions of growth rate and cooling rate, respectively. A comparative analysis with other studies published in the literature that analyze tertiary dendritic growth of Al-Cu alloys considering transient directional solidification is carried out. Dependence of microhardness on dendritic arrangement is evaluated by experimental laws of power and Hall-Petch types with a view to permitting the applicability of the resulting expressions.


Author(s):  
J. J. Laidler

The presence of three-dimensional voids in quenched metals has long been suspected, and voids have indeed been observed directly in a number of metals. These include aluminum, platinum, and copper, silver and gold. Attempts at the production of observable quenched-in defects in nickel have been generally unsuccessful, so the present work was initiated in order to establish the conditions under which such defects may be formed.Electron beam zone-melted polycrystalline nickel foils, 99.997% pure, were quenched from 1420°C in an evacuated chamber into a bath containing a silicone diffusion pump fluid . The pressure in the chamber at the quenching temperature was less than 10-5 Torr . With an oil quench such as this, the cooling rate is approximately 5,000°C/second above 400°C; below 400°C, the cooling curve has a long tail. Therefore, the quenched specimens are aged in place for several seconds at a temperature which continuously approaches the ambient temperature of the system.


Author(s):  
H.J. Zuo ◽  
M.W. Price ◽  
R.D. Griffin ◽  
R.A. Andrews ◽  
G.M. Janowski

The II-VI semiconducting alloys, such as mercury zinc telluride (MZT), have become the materials of choice for numerous infrared detection applications. However, compositional inhomogeneities and crystallographic imperfections adversly affect the performance of MZT infrared detectors. One source of imperfections in MZT is gravity-induced convection during directional solidification. Crystal growth experiments conducted in space should minimize gravity-induced convection and thereby the density of related crystallographic defects. The limited amount of time available during Space Shuttle experiments and the need for a sample of uniform composition requires the elimination of the initial composition transient which occurs in directionally solidified alloys. One method of eluding this initial transient involves directionally solidifying a portion of the sample and then quenching the remainder prior to the space experiment. During the space experiment, the MZT sample is back-melted to exactly the point at which directional solidification was stopped on earth. The directional solidification process then continues.


Author(s):  
Chenqi Zhu

In order to improve the guiding accuracy in intercepting the hypersonic vehicle, this article presents a finite-time guidance law based on the observer and head-pursuit theory. First, based on a two-dimensional model between the interceptor and target, this study applies the fast power reaching law to head-pursuit guidance law so that it can alleviate the chattering phenomenon and ensure the convergence speed. Second, target maneuvers are considered as system disturbances, and the head-pursuit guidance law based on an observer is proposed. Furthermore, this method is extended to a three-dimensional case. Finally, comparative simulation results further verify the superiority of the guidance laws designed in this article.


2021 ◽  
Vol 40 (1) ◽  
pp. 178-192
Author(s):  
Wen-Qiang Ren ◽  
Lu Wang ◽  
Zheng-Liang Xue ◽  
Cheng-Zhi Li ◽  
Hang-Yu Zhu ◽  
...  

Abstract Thermodynamic analysis of the precipitation behavior, growth kinetic, and control mechanism of MnS inclusion in U75V heavy rail steel was conducted in this study. The results showed that solute element S had a much higher segregation ratio than that of Mn, and MnS would only precipitate in the solid–liquid (two-phase) regions at the late stage during the solidification process at the solid fraction of 0.9518. Increasing the cooling rate had no obvious influence on the precipitation time of MnS inclusion; however, its particle size would be decreased greatly. The results also suggested that increasing the concentration of Mn would lead to an earlier precipitation time of MnS, while it had little effect on the final particle size; as to S, it was found that increasing its concentration could not only make the precipitation time earlier but also make the particle size larger. Adding a certain amount of Ti additive could improve the mechanical properties of U75V heavy rail steel due to the formation of TiO x –MnS or MnS–TiS complex inclusions. The precipitation sequences of Ti3O5 → Ti2O3 → TiO2 → TiO → MnS → TiS for Ti treatment were determined based on the thermodynamic calculation.


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