scholarly journals Concentrations of manganese and iron in some woody and herbs plants

2011 ◽  
pp. 39-49 ◽  
Author(s):  
Dragica Stankovic ◽  
Borivoj Krstic ◽  
Mirjana Sijacic-Nikolic ◽  
Milan Knezevic
Keyword(s):  
Heavy Metals ◽  
Natural Environment ◽  
Atomic Absorption Spectrophotometry ◽  
Multidisciplinary Research ◽  
Flame Atomic Absorption ◽  
Term Basis ◽  
Level Of Significance ◽  
The City

Heavy metals are the substances that indicate environmental pollution. The plants polluted with heavy metals may endanger natural environment and cause health problems in humans. In our multidisciplinary research of the concentrations of pollutants in forest ecosystems and natural environment in Belgrade, we examined the contents of heavy metals essential for plants but harmful in greater concentrations on a long-term basis. The fact that heavy metals manganese and iron are accumulated in plants to the greatest extent focused our work on determination of the level of concentrations of Mn and Fe in the vegetative parts of 8 plant types on three locations on the Avala Mountain and one location in the centre of the city of Belgrade. The analyses of heavy metals contents in plants were performed by the method of flame atomic absorption spectrophotometry. The examination of the existence of important differences between the average values was performed by implementation of Duncan?s test for the level of significance of 95%. The current contents of heavy metals in plants in the area of the protected natural resource Avala do not represent danger that would presently cause notable damage to forests but show the tendency of the increase of concentrations. Therefore, this issue should be constantly monitored.

Co-precipitation of Ni, Cr, Mn, Pb and Zn in industrial wastewater and sediment samples with copper(II) cyclo-hexylmethyldithiocarbamate for their flame atomic absorption spectrometric determination

2012 ◽  
Vol 66 (1) ◽  
pp. 105-112 ◽  
Author(s):  
Ayodele Rotimi Ipeaiyeda ◽  
Adekunle Johnson Odola
Keyword(s):  
Heavy Metals ◽  
Atomic Absorption ◽  
Industrial Wastewater ◽  
Atomic Absorption Spectrophotometry ◽  
Sample Volume ◽  
Sediment Samples ◽  
Flame Atomic Absorption ◽  
Precipitation Procedure ◽  
Co Precipitation

A co-precipitation technique for nickel(II), chromium(II), manganese(II), lead(II) and zinc(II) with the aid of copper(II) cyclo-hexylmethyldithiocarbamate was established. The influences of some analytical parameters such as pH, sample volume, amounts of cyclo-hexylmethyldithiocarbamate and copper(II) on the recovery of metal ions were investigated. The heavy metals in the precipitate were determined by flame atomic absorption spectrophotometry. The range of detection limits for the heavy metals was 0.003–0.005 mg/L. The atomic spectrometric technique with co-precipitation procedure was successfully applied for the determination of Ni, Cr, Mn, Pb and Zn in industrial wastewater and sediment samples from Ladipo stream in Lagos, Nigeria. The mean concentrations for these metals using co-precipitation procedure were not significantly different from corresponding concentrations obtained using spectrometric techniques without co-precipitation procedure.

ANALISA LOGAM BESI (Fe) DI SUNGAI PASAR DAERAH BELANGWETAN KLATEN DENGAN METODE SPEKTROFOTOMETRI SERAPAN ATOM

2017 ◽  
Vol 2 (1) ◽  
pp. 39
Author(s):  
Rahmi Nurhaini ◽  
Arief Affandi
Keyword(s):  
Heavy Metals ◽  
Sampling Method ◽  
Research Result ◽  
The Body ◽  
Clean Water ◽  
Observational Method ◽  
The Mean ◽  
The Republic

Iron (Fe) is one of many heavy metals that is corrosive resistant, dense, and has a low melting point. If accumulated in the body, the metal can cause some medical conditions, such as irritation to skin and eyes, breathing problems, and in the long term, cancer. This research aims to know generally the spread of metallic iron (Fe) in the river Pasar in Belangwetan, Klaten. This study was conducted using an observational method in which researchers did not examine the effects of interventions. Sampling was done using purposive sampling method taken from three points, namely the upper, middle, lower. Determination of iron levels by Atomic Absorption Spectrophotometer (AAS) obtained a positive result, and the data was processed using SPSS to determine the Mean and Standard Deviation. Of the research result, it could be known the Mean score was 2.33 ppm and SD was 0.0352. The result of this research indicated that the levels of iron in the river Pasar in Belangwetan were 2.33 ppm. It means that the levels violate the regulation of the Minister of Health of the Republic of Indonesia, which is not more than 1mg/L (1ppm) in the clean water

scholarly journals Cost-effective Method of Analysis for the Determination of Cadmium, Copper, Nickel and Zinc in Cocoa Beans and Chocolates

2014 ◽  
Vol 4 (1) ◽  
pp. 193 ◽  
Author(s):  
Gideon Ramtahal ◽  
Ivan Chang Yen ◽  
Isaac Bekele ◽  
Frances Bekele ◽  
Lawrence Wilson ◽  
...  
Keyword(s):  
Heavy Metals ◽  
Heavy Metal ◽  
Reference Materials ◽  
Certified Reference Materials ◽  
Control Sample ◽  
Cost Effective ◽  
Cocoa Beans ◽  
Copper Nickel ◽  
Flame Atomic Absorption

<p>The determination of heavy metals in cocoa beans and chocolates is of great importance, due to increasingly stringent regulations being implemented by international legislative bodies and chocolate manufacturers, to protect the health of their consumers. While various techniques exist for heavy metal analyses in cocoa, this study developed a cost-effective, accurate and precise method capable of processing up to 120 samples per batch for the determination of cadmium, copper, nickel and zinc. For sample extractions, a normal laboratory hot plate and locally fabricated high-capacity digestion blocks were used, instead of dedicated block digestion or microwave digestion systems. In addition, only concentrated nitric acid was used, instead of mixed reagents used in standardized methods, for metal extractions from samples, with a sample: extractant ratio of 0.5 g : 10 mL, digestion at 130 ºC, followed by filtration and analysis by flame atomic absorption spectrophotometry. The method was validated with Certified Reference Materials, with heavy metal recoveries generally &gt;95%. Additionally, an in-house quality control sample of ground cocoa nib analyzed together with the Certified Reference Materials was used to monitor the consistency of analyses of heavy metals in cocoa bean samples.</p>

scholarly journals Determination of heavy metals (Pb and Cd) in guava pulps (psidium guajava) obtained in the city of Cartagena

2019 ◽  
Vol 17 (2) ◽  
pp. 137
Author(s):  
Diana Gómez-Marrugo ◽  
Glicerio León-Méndez ◽  
Jorge Puello-Silva ◽  
Miladys Torrenegra-Alarcon ◽  
Deisy León-Méndez ◽  
...  
Keyword(s):  
Heavy Metals ◽  
Psidium Guajava ◽  
The City

 El objetivo de este estudio fue determinar los niveles de acumulación de metales pesados como el cadmio (Cd) y el plomo (Pb) derivados de actividades antropogénicas, como los humos metálicos de la soldadura y el tráfico de vehículos, en la pulpa de guayaba (Psidium guajava) en la ciudad de Cartagena. -Bolívar. Las muestras se dividieron en tres (3) grupos según la proximidad de las fuentes de contaminación. En el grupo 1, menos de 100 m de industrias metalúrgicas, las concentraciones de Cd en el rango de 0.0400 ± 0.33 mg / Kg y 0.0483 ± 0.15 mg / Kg, mientras que los valores de Pb oscilaron entre 0.036 ± 0.22 mg / kg y 0.060 ± 0.01 mg / kg . Para el grupo 2, se tomaron muestras en 3 lugares donde no se identificó claramente ninguna fuente de contaminación, lo que resultó en concentraciones de Cd 0.0215 ± 0.05 mg / Kg y 0.0260 ± 0.10 mg / Kg, mientras que para el Pb solo se encontró en una de las muestras cuyo valor fue 0.035 ± 0.15 mg / Kg. Finalmente, para el grupo 3, se tomaron muestras en 2 ubicaciones ubicadas a menos de 100 m de avenidas de alto tráfico, resultando en valores muy similares para Cd (0.0220 ± 0.13 mg / Kg y 0.0311 ± 0. 22 mg / Kg), mientras que para Pb el los valores fueron muy precisos (0.032 ± 0.35 mg / Kg y 0.029 ± 0.20 mg / Kg). Estas mediciones muestran cómo, en sitios cercanos a las actividades humanas, las concentraciones de estos metales pesados están en niveles más altos, lo que representa un peligro para su consumo debido a la bioacumulación en diferentes tejidos humanos.Palabras clave: metales pesados, humo metálico, contaminación, tráfico vehicular.

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